# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2020
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
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# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
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data_v18433
_database_code_depnum_ccdc_archive 'CCDC 1985597'
loop_
_audit_author_name
_audit_author_address
'Manar Shoshani'
;California Institute of Technology
United States of America
;
_audit_update_record
;
2020-07-16 deposited with the CCDC. 2020-07-20 downloaded from the CCDC.
;
_audit_creation_method SHELXL-2018/3
_shelx_SHELXL_version_number 2018/3
_chemical_name_common ?
_chemical_name_systematic ?
_chemical_formula_moiety ?
_chemical_formula_sum 'C93.64 H148.93 K2 N2 Ni3 O8 P2 Si4'
_chemical_formula_weight 1859.40
_chemical_melting_point ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system monoclinic
_space_group_IT_number 15
_space_group_name_H-M_alt 'C 2/c'
_space_group_name_Hall '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
_cell_length_a 28.067(6)
_cell_length_b 20.574(4)
_cell_length_c 18.052(4)
_cell_angle_alpha 90
_cell_angle_beta 97.215(7)
_cell_angle_gamma 90
_cell_volume 10341(4)
_cell_formula_units_Z 4
_cell_measurement_reflns_used 14000
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 29.14
_cell_measurement_theta_min 2.408
_shelx_estimated_absorpt_T_max 0.916
_shelx_estimated_absorpt_T_min 0.841
_exptl_absorpt_coefficient_mu 0.748
_exptl_absorpt_correction_T_max 1.0000
_exptl_absorpt_correction_T_min 0.8816
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0917 before and 0.0631 after correction. The Ratio of minimum to maximum transmission is 0.8816. The \l/2 correction factor is Not present.'
_exptl_absorpt_special_details SADABS-2016/2
_exptl_crystal_colour yellow
_exptl_crystal_density_diffrn 1.194
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_description block
_exptl_crystal_F_000 3987
_exptl_crystal_size_max 0.240
_exptl_crystal_size_mid 0.160
_exptl_crystal_size_min 0.120
_exptl_transmission_factor_max ?
_exptl_transmission_factor_min ?
_diffrn_reflns_av_R_equivalents 0.0627
_diffrn_reflns_av_unetI/netI 0.0395
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max 38
_diffrn_reflns_limit_h_min -38
_diffrn_reflns_limit_k_max 28
_diffrn_reflns_limit_k_min -28
_diffrn_reflns_limit_l_max 24
_diffrn_reflns_limit_l_min -24
_diffrn_reflns_number 107191
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 29.243
_diffrn_reflns_theta_min 2.283
_diffrn_ambient_temperature 100(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type 'Bruker APEX-II CCD'
_diffrn_measurement_method ?
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_source ?
_reflns_Friedel_coverage 0.000
_reflns_Friedel_fraction_full .
_reflns_Friedel_fraction_max .
_reflns_number_gt 10488
_reflns_number_total 14000
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_reflns_threshold_expression 'I > 2\s(I)'
_computing_cell_refinement 'SAINT V8.38A (?, 2016)'
_computing_data_collection 'APEX2 v2014.11-0 (Bruker-AXS, 2014)'
_computing_data_reduction 'SAINT V8.38A (?, 2016)'
_computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution 'XS (Sheldrick, 2008)'
_refine_diff_density_max 1.015
_refine_diff_density_min -0.550
_refine_diff_density_rms 0.098
_refine_ls_extinction_coef .
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.101
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 696
_refine_ls_number_reflns 14000
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.0850
_refine_ls_R_factor_gt 0.0562
_refine_ls_restrained_S_all 1.101
_refine_ls_shift/su_max 0.143
_refine_ls_shift/su_mean 0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0824P)^2^+29.1488P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1475
_refine_ls_wR_factor_ref 0.1755
_refine_special_details ?
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary ?
_atom_sites_solution_secondary ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni1 Ni 0.54766(2) 0.18693(2) 0.25786(2) 0.02189(10) Uani 1 1 d . . . . .
Ni2 Ni 0.500000 0.29414(2) 0.250000 0.02289(12) Uani 1 2 d S T P A .
P1 P 0.50306(2) 0.22176(4) 0.40004(4) 0.02358(15) Uani 1 1 d . . . . .
O2 O 0.50559(8) 0.35816(10) 0.32590(11) 0.0318(4) Uani 1 1 d . . . . .
O3 O 0.40696(7) 0.17000(10) 0.30792(10) 0.0278(4) Uani 1 1 d . . . . .
O1 O 0.59058(7) 0.16002(11) 0.34226(10) 0.0285(4) Uani 1 1 d . . . . .
N1 N 0.50086(8) 0.22064(11) 0.31063(11) 0.0226(4) Uani 1 1 d . . . . .
C33 C 0.58929(11) 0.34152(15) 0.53491(15) 0.0299(6) Uani 1 1 d . . . . .
C39 C 0.62173(11) 0.33758(15) 0.60939(16) 0.0327(6) Uani 1 1 d . . . . .
C34 C 0.56392(10) 0.28886(15) 0.50355(14) 0.0270(5) Uani 1 1 d . . . . .
H34 H 0.566227 0.248416 0.529147 0.032 Uiso 1 1 calc R U . . .
C19 C 0.55354(11) 0.08071(15) 0.54257(15) 0.0304(6) Uani 1 1 d . . . . .
C30 C 0.53047(10) 0.35247(14) 0.39281(15) 0.0273(6) Uani 1 1 d . . . . .
C15 C 0.53735(10) 0.15458(14) 0.43800(14) 0.0255(5) Uani 1 1 d . . . . .
C17 C 0.60660(10) 0.08343(14) 0.44277(15) 0.0264(5) Uani 1 1 d . . . . .
C3 C 0.36001(10) 0.18330(16) 0.40712(16) 0.0310(6) Uani 1 1 d . . . . .
C29 C 0.53460(10) 0.29364(14) 0.43436(14) 0.0250(5) Uani 1 1 d . . . . .
C20 C 0.52561(11) 0.12757(15) 0.50500(15) 0.0285(6) Uani 1 1 d . . . . .
H20 H 0.497628 0.142222 0.524590 0.034 Uiso 1 1 calc R U . . .
C7 C 0.31581(11) 0.15299(17) 0.36012(18) 0.0363(7) Uani 1 1 d . . . . .
C16 C 0.57798(10) 0.13385(14) 0.40479(14) 0.0253(5) Uani 1 1 d . . . . .
C21 C 0.65008(11) 0.05545(16) 0.40939(16) 0.0325(6) Uani 1 1 d . . . . .
C31 C 0.55588(11) 0.40808(14) 0.42610(16) 0.0305(6) Uani 1 1 d . . . . .
C25 C 0.54188(13) 0.05392(18) 0.61795(17) 0.0395(7) Uani 1 1 d . . . . .
C32 C 0.58379(11) 0.40042(15) 0.49522(16) 0.0333(6) Uani 1 1 d . . . . .
H32 H 0.600185 0.437521 0.516912 0.040 Uiso 1 1 calc R U . . .
C35 C 0.55266(13) 0.47418(16) 0.38632(19) 0.0412(8) Uani 1 1 d . . . . .
C18 C 0.59367(11) 0.05977(14) 0.51000(15) 0.0293(6) Uani 1 1 d . . . . .
H18 H 0.613443 0.027242 0.535419 0.035 Uiso 1 1 calc R U . . .
C40 C 0.67321(12) 0.35742(18) 0.59762(19) 0.0419(8) Uani 1 1 d . . . . .
H40A H 0.685193 0.327914 0.561549 0.063 Uiso 1 1 calc R U . . .
H40B H 0.694118 0.354926 0.645280 0.063 Uiso 1 1 calc R U . . .
H40C H 0.673052 0.402022 0.578538 0.063 Uiso 1 1 calc R U . . .
C2 C 0.40481(10) 0.18994(15) 0.37645(15) 0.0275(6) Uani 1 1 d . . . . .
C1 C 0.44356(10) 0.21848(14) 0.42414(14) 0.0264(5) Uani 1 1 d . . . . .
C36 C 0.57221(16) 0.46774(18) 0.3104(2) 0.0450(8) Uani 1 1 d . . . . .
H36A H 0.6108(18) 0.455(2) 0.317(3) 0.068 Uiso 1 1 d . U . . .
H36B H 0.5714(17) 0.515(2) 0.286(3) 0.068 Uiso 1 1 d . U . . .
H36C H 0.5561(18) 0.441(3) 0.285(3) 0.068 Uiso 1 1 d . U . . .
C41 C 0.60257(13) 0.38378(18) 0.66577(17) 0.0401(7) Uani 1 1 d . . . . .
H41A H 0.601723 0.428257 0.646212 0.060 Uiso 1 1 calc R U . . .
H41B H 0.623697 0.382070 0.713268 0.060 Uiso 1 1 calc R U . . .
H41C H 0.570080 0.370452 0.673746 0.060 Uiso 1 1 calc R U . . .
C22 C 0.63340(13) 0.0265(2) 0.33262(18) 0.0438(8) Uani 1 1 d . . . . .
H22A H 0.610620 -0.008819 0.337707 0.066 Uiso 1 1 calc R U . . .
H22B H 0.661182 0.009470 0.310944 0.066 Uiso 1 1 calc R U . . .
H22C H 0.617707 0.060299 0.299921 0.066 Uiso 1 1 calc R U . . .
C14 C 0.43608(13) 0.27757(19) 0.64995(18) 0.0437(8) Uani 1 1 d . . . . .
H14A H 0.445489 0.316464 0.624012 0.066 Uiso 1 1 calc R U . . .
H14B H 0.461772 0.245113 0.652002 0.066 Uiso 1 1 calc R U . . .
H14C H 0.430517 0.289149 0.700818 0.066 Uiso 1 1 calc R U . . .
C9 C 0.30289(12) 0.1907(2) 0.2871(2) 0.0430(8) Uani 1 1 d . . . . .
H9A H 0.298161 0.236655 0.298431 0.064 Uiso 1 1 calc R U . . .
H9B H 0.273247 0.172976 0.260174 0.064 Uiso 1 1 calc R U . . .
H9C H 0.329010 0.186539 0.256159 0.064 Uiso 1 1 calc R U . . .
C38 C 0.58212(17) 0.52676(18) 0.4308(2) 0.0546(10) Uani 1 1 d . . . . .
H38A H 0.569796 0.533273 0.478721 0.082 Uiso 1 1 calc R U . . .
H38B H 0.579632 0.567514 0.402499 0.082 Uiso 1 1 calc R U . . .
H38C H 0.615827 0.513224 0.439794 0.082 Uiso 1 1 calc R U . . .
C12 C 0.35053(16) 0.2998(3) 0.6076(3) 0.0680(14) Uani 1 1 d . . . . .
H12A H 0.346699 0.311514 0.659187 0.102 Uiso 1 1 calc R U . . .
H12B H 0.320303 0.281833 0.582919 0.102 Uiso 1 1 calc R U . . .
H12C H 0.359089 0.338592 0.580726 0.102 Uiso 1 1 calc R U . . .
C13 C 0.37670(19) 0.1873(2) 0.6491(2) 0.0631(12) Uani 1 1 d . . . . .
H13A H 0.402276 0.154958 0.648362 0.095 Uiso 1 1 calc R U . . .
H13B H 0.346487 0.169518 0.624098 0.095 Uiso 1 1 calc R U . . .
H13C H 0.372948 0.198096 0.700907 0.095 Uiso 1 1 calc R U . . .
C23 C 0.68775(11) 0.1088(2) 0.4039(2) 0.0442(8) Uani 1 1 d . . . . .
H23A H 0.673248 0.144605 0.373096 0.066 Uiso 1 1 calc R U . . .
H23B H 0.714789 0.090850 0.381081 0.066 Uiso 1 1 calc R U . . .
H23C H 0.699265 0.125015 0.454007 0.066 Uiso 1 1 calc R U . . .
C5 C 0.39596(11) 0.23124(17) 0.52683(16) 0.0346(6) Uani 1 1 d . . . . .
C10 C 0.27173(13) 0.1522(2) 0.4026(2) 0.0523(10) Uani 1 1 d . . . . .
H10A H 0.279033 0.126928 0.448615 0.078 Uiso 1 1 calc R U . . .
H10B H 0.244577 0.132279 0.371194 0.078 Uiso 1 1 calc R U . . .
H10C H 0.263429 0.196803 0.414946 0.078 Uiso 1 1 calc R U . . .
C11 C 0.38997(13) 0.24943(19) 0.60782(18) 0.0429(8) Uani 1 1 d . . . . .
C42 C 0.62327(15) 0.26886(18) 0.64228(19) 0.0456(9) Uani 1 1 d . . . . .
H42A H 0.591154 0.256653 0.653314 0.068 Uiso 1 1 calc R U . . .
H42B H 0.645790 0.267812 0.688383 0.068 Uiso 1 1 calc R U . . .
H42C H 0.633857 0.238160 0.606187 0.068 Uiso 1 1 calc R U . . .
C37 C 0.50044(16) 0.4978(2) 0.3749(2) 0.0501(10) Uani 1 1 d . . . . .
H37A H 0.4785(19) 0.466(3) 0.352(3) 0.075 Uiso 1 1 d . U . . .
H37B H 0.4981(18) 0.539(3) 0.342(3) 0.075 Uiso 1 1 d . U . . .
H37C H 0.4824(18) 0.502(3) 0.419(3) 0.075 Uiso 1 1 d . U . . .
C24 C 0.67452(14) 0.00043(19) 0.45771(19) 0.0454(8) Uani 1 1 d . . . . .
H24A H 0.686582 0.017433 0.507242 0.068 Uiso 1 1 calc R U . . .
H24B H 0.701350 -0.016966 0.433946 0.068 Uiso 1 1 calc R U . . .
H24C H 0.651210 -0.034250 0.462751 0.068 Uiso 1 1 calc R U . . .
C8 C 0.32631(14) 0.08251(18) 0.3420(2) 0.0453(8) Uani 1 1 d . . . . .
H8A H 0.354018 0.080769 0.313946 0.068 Uiso 1 1 calc R U . . .
H8B H 0.298246 0.063619 0.311798 0.068 Uiso 1 1 calc R U . . .
H8C H 0.333431 0.057816 0.388454 0.068 Uiso 1 1 calc R U . . .
C6 C 0.43825(11) 0.23962(15) 0.49724(15) 0.0303(6) Uani 1 1 d . . . . .
H6 H 0.464547 0.260067 0.526485 0.036 Uiso 1 1 calc R U . . .
C4 C 0.35759(11) 0.20329(17) 0.48028(18) 0.0357(7) Uani 1 1 d . . . . .
H4 H 0.328026 0.197618 0.499955 0.043 Uiso 1 1 calc R U . . .
K1A K 0.61988(3) 0.28749(5) 0.31848(6) 0.0422(3) Uani 0.797(2) 1 d . . P A 1
Si2A Si 0.68744(6) 0.39480(8) 0.19053(9) 0.0447(3) Uani 0.797(2) 1 d . . P A 1
Si1A Si 0.73379(4) 0.37070(6) 0.35155(8) 0.0397(3) Uani 0.797(2) 1 d . . P A 1
O4A O 0.69460(18) 0.3625(3) 0.2761(3) 0.0358(10) Uani 0.797(2) 1 d . . P A 1
C26 C 0.5411(3) -0.0206(4) 0.6147(4) 0.0447(18) Uani 0.610(15) 1 d . . P B 1
H26A H 0.515442 -0.034900 0.576287 0.067 Uiso 0.610(15) 1 calc R U P B 1
H26B H 0.535307 -0.037967 0.663282 0.067 Uiso 0.610(15) 1 calc R U P B 1
H26C H 0.572076 -0.036460 0.602346 0.067 Uiso 0.610(15) 1 calc R U P B 1
C27 C 0.4977(5) 0.0798(7) 0.6395(6) 0.085(5) Uani 0.610(15) 1 d . . P B 1
H27A H 0.502078 0.125952 0.652077 0.127 Uiso 0.610(15) 1 calc R U P B 1
H27B H 0.489344 0.056047 0.683144 0.127 Uiso 0.610(15) 1 calc R U P B 1
H27C H 0.471901 0.074963 0.598064 0.127 Uiso 0.610(15) 1 calc R U P B 1
C28 C 0.5844(5) 0.0735(4) 0.6772(3) 0.060(3) Uani 0.610(15) 1 d . . P B 1
H28A H 0.614325 0.055716 0.662996 0.090 Uiso 0.610(15) 1 calc R U P B 1
H28B H 0.578988 0.056271 0.726009 0.090 Uiso 0.610(15) 1 calc R U P B 1
H28C H 0.586651 0.121034 0.679847 0.090 Uiso 0.610(15) 1 calc R U P B 1
C43 C 0.7326(2) 0.2929(2) 0.4045(3) 0.0516(12) Uani 0.797(2) 1 d . . P A 1
H43A H 0.701899 0.289011 0.424675 0.077 Uiso 0.797(2) 1 calc R U P A 1
H43B H 0.758951 0.292649 0.445707 0.077 Uiso 0.797(2) 1 calc R U P A 1
H43C H 0.736384 0.256279 0.371090 0.077 Uiso 0.797(2) 1 calc R U P A 1
C44 C 0.7121(3) 0.4377(3) 0.4079(5) 0.0511(18) Uani 0.797(2) 1 d . . P A 1
H44A H 0.714993 0.479212 0.382136 0.077 Uiso 0.797(2) 1 calc R U P A 1
H44B H 0.731512 0.439170 0.456968 0.077 Uiso 0.797(2) 1 calc R U P A 1
H44C H 0.678396 0.430161 0.414328 0.077 Uiso 0.797(2) 1 calc R U P A 1
C48 C 0.6256(2) 0.3724(3) 0.1480(3) 0.0538(12) Uani 0.797(2) 1 d . . P A 1
H48A H 0.619(2) 0.328(4) 0.134(4) 0.081 Uiso 0.797(2) 1 d . U P A 1
H48B H 0.615(3) 0.393(4) 0.101(4) 0.081 Uiso 0.797(2) 1 d . U P A 1
H48C H 0.600(3) 0.388(3) 0.172(4) 0.081 Uiso 0.797(2) 1 d . U P A 1
C45 C 0.79500(16) 0.3861(3) 0.3282(4) 0.0575(13) Uani 0.797(2) 1 d . . P A 1
H45A H 0.804538 0.350735 0.296840 0.086 Uiso 0.797(2) 1 calc R U P A 1
H45B H 0.817493 0.388503 0.374251 0.086 Uiso 0.797(2) 1 calc R U P A 1
H45C H 0.795448 0.427359 0.301085 0.086 Uiso 0.797(2) 1 calc R U P A 1
C47 C 0.7320(3) 0.3614(4) 0.1317(4) 0.063(3) Uani 0.74(2) 1 d . . . A 1
H47A H 0.764645 0.371135 0.155254 0.094 Uiso 0.797(2) 1 calc R U P A 1
H47B H 0.726921 0.381396 0.082035 0.094 Uiso 0.797(2) 1 calc R U P A 1
H47C H 0.727936 0.314235 0.126931 0.094 Uiso 0.797(2) 1 calc R U P A 1
C46 C 0.6953(3) 0.4840(4) 0.1991(5) 0.064(3) Uani 0.72(2) 1 d . . . A 1
H46A H 0.671908 0.501654 0.229706 0.096 Uiso 0.797(2) 1 calc R U P A 1
H46B H 0.690256 0.503767 0.149310 0.096 Uiso 0.797(2) 1 calc R U P A 1
H46C H 0.727883 0.493704 0.222681 0.096 Uiso 0.797(2) 1 calc R U P A 1
K1B K 0.59919(14) 0.3172(2) 0.2016(3) 0.0472(11) Uani 0.203(2) 1 d . . P A 2
Si1B Si 0.70141(19) 0.3565(3) 0.3429(3) 0.0441(13) Uani 0.203(2) 1 d . . P A 2
Si2B Si 0.7078(3) 0.4101(4) 0.1828(5) 0.072(2) Uani 0.203(2) 1 d . . P A 2
O4B O 0.6888(10) 0.3714(13) 0.2514(10) 0.048(5) Uani 0.203(2) 1 d . . P A 2
C28B C 0.5559(6) 0.1070(9) 0.6790(5) 0.062(5) Uani 0.390(15) 1 d . . P B 2
H28D H 0.590850 0.112449 0.686396 0.094 Uiso 0.390(15) 1 calc R U P B 2
H28E H 0.544902 0.093485 0.726097 0.094 Uiso 0.390(15) 1 calc R U P B 2
H28F H 0.540663 0.148368 0.662788 0.094 Uiso 0.390(15) 1 calc R U P B 2
C27B C 0.4867(4) 0.0464(8) 0.6169(7) 0.046(3) Uani 0.390(15) 1 d . . P B 2
H27D H 0.471545 0.089395 0.612122 0.069 Uiso 0.390(15) 1 calc R U P B 2
H27E H 0.479901 0.025956 0.663407 0.069 Uiso 0.390(15) 1 calc R U P B 2
H27F H 0.473911 0.019269 0.574397 0.069 Uiso 0.390(15) 1 calc R U P B 2
C26B C 0.5643(7) -0.0082(9) 0.6404(10) 0.072(5) Uani 0.390(15) 1 d . . P B 2
H26D H 0.558939 -0.038929 0.598681 0.108 Uiso 0.390(15) 1 calc R U P B 2
H26E H 0.550105 -0.025483 0.683205 0.108 Uiso 0.390(15) 1 calc R U P B 2
H26F H 0.598858 -0.001865 0.654261 0.108 Uiso 0.390(15) 1 calc R U P B 2
C1AA C 0.7612(9) 0.3170(14) 0.3595(15) 0.072(7) Uani 0.203(2) 1 d . . P A 2
H1AA H 0.761380 0.278293 0.327909 0.108 Uiso 0.203(2) 1 calc R U P A 2
H1AB H 0.767890 0.304310 0.412121 0.108 Uiso 0.203(2) 1 calc R U P A 2
H1AC H 0.785848 0.347499 0.347297 0.108 Uiso 0.203(2) 1 calc R U P A 2
C0AA C 0.708(2) 0.431(3) 0.394(3) 0.16(3) Uani 0.203(2) 1 d . . P A 2
H0AA H 0.738950 0.450915 0.388237 0.240 Uiso 0.203(2) 1 calc R U P A 2
H0AB H 0.705766 0.422911 0.446725 0.240 Uiso 0.203(2) 1 calc R U P A 2
H0AC H 0.682016 0.461237 0.374197 0.240 Uiso 0.203(2) 1 calc R U P A 2
C4AA C 0.662(2) 0.405(3) 0.104(3) 0.160(19) Uiso 0.203(2) 1 d . . P A 2
H4AA H 0.677133 0.405507 0.058077 0.241 Uiso 0.203(2) 1 calc R U P A 2
H4AB H 0.640126 0.441516 0.104856 0.241 Uiso 0.203(2) 1 calc R U P A 2
H4AC H 0.644332 0.363948 0.106953 0.241 Uiso 0.203(2) 1 calc R U P A 2
C47A C 0.753(2) 0.375(3) 0.156(3) 0.14(2) Uiso 0.203(2) 1 d . . P A 2
H47D H 0.779429 0.375440 0.196336 0.211 Uiso 0.203(2) 1 calc R U P A 2
H47E H 0.761841 0.397027 0.112168 0.211 Uiso 0.203(2) 1 calc R U P A 2
H47F H 0.744123 0.329463 0.143100 0.211 Uiso 0.203(2) 1 calc R U P A 2
C46A C 0.720(2) 0.4971(13) 0.212(3) 0.111(16) Uani 0.203(2) 1 d . . P A 2
H46D H 0.693889 0.513187 0.238078 0.166 Uiso 0.203(2) 1 calc R U P A 2
H46E H 0.721976 0.523823 0.167172 0.166 Uiso 0.203(2) 1 calc R U P A 2
H46F H 0.750420 0.499705 0.244689 0.166 Uiso 0.203(2) 1 calc R U P A 2
C2AA C 0.6522(9) 0.3019(14) 0.3747(13) 0.069(6) Uani 0.203(2) 1 d . . P A 2
H2AA H 0.621607 0.325421 0.368988 0.103 Uiso 0.203(2) 1 calc R U P A 2
H2AB H 0.660916 0.290070 0.427256 0.103 Uiso 0.203(2) 1 calc R U P A 2
H2AC H 0.649057 0.262440 0.344113 0.103 Uiso 0.203(2) 1 calc R U P A 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ni1 0.01939(16) 0.03284(19) 0.01350(15) 0.00143(12) 0.00231(11) -0.00038(13)
Ni2 0.0218(2) 0.0322(3) 0.0140(2) 0.000 -0.00017(16) 0.000
P1 0.0220(3) 0.0356(4) 0.0131(3) 0.0004(2) 0.0022(2) -0.0001(3)
O2 0.0404(12) 0.0355(11) 0.0172(9) -0.0028(8) -0.0055(8) 0.0094(9)
O3 0.0257(9) 0.0410(11) 0.0176(8) -0.0036(8) 0.0059(7) -0.0037(8)
O1 0.0213(9) 0.0474(12) 0.0167(8) 0.0082(8) 0.0014(7) 0.0000(8)
N1 0.0203(10) 0.0340(12) 0.0133(9) -0.0010(8) 0.0020(8) 0.0004(8)
C33 0.0306(14) 0.0386(15) 0.0190(12) -0.0030(11) -0.0028(10) 0.0073(12)
C39 0.0368(15) 0.0377(15) 0.0206(13) -0.0035(11) -0.0083(11) 0.0050(12)
C34 0.0271(13) 0.0369(14) 0.0165(11) 0.0005(10) 0.0002(10) 0.0029(11)
C19 0.0346(15) 0.0397(16) 0.0171(12) 0.0043(11) 0.0036(10) -0.0020(12)
C30 0.0253(13) 0.0373(15) 0.0180(12) -0.0036(10) -0.0022(10) 0.0076(11)
C15 0.0240(12) 0.0358(14) 0.0162(11) 0.0035(10) 0.0008(9) -0.0018(10)
C17 0.0236(12) 0.0359(14) 0.0189(12) 0.0033(10) -0.0005(9) -0.0024(11)
C3 0.0245(13) 0.0433(16) 0.0266(14) -0.0041(12) 0.0082(11) -0.0011(12)
C29 0.0238(12) 0.0348(14) 0.0160(11) -0.0021(10) 0.0005(9) 0.0024(10)
C20 0.0300(14) 0.0374(15) 0.0188(12) 0.0015(10) 0.0054(10) -0.0016(11)
C7 0.0261(14) 0.0499(19) 0.0341(15) -0.0063(13) 0.0087(12) -0.0052(13)
C16 0.0230(12) 0.0356(14) 0.0169(11) 0.0044(10) 0.0003(9) -0.0051(10)
C21 0.0287(14) 0.0453(17) 0.0234(13) 0.0074(12) 0.0025(11) 0.0049(12)
C31 0.0349(15) 0.0326(14) 0.0225(13) -0.0038(11) -0.0024(11) 0.0069(12)
C25 0.0444(18) 0.0524(19) 0.0225(14) 0.0126(13) 0.0067(12) -0.0010(15)
C32 0.0376(16) 0.0335(15) 0.0262(14) -0.0058(11) -0.0063(12) 0.0067(12)
C35 0.053(2) 0.0313(15) 0.0336(16) -0.0025(12) -0.0150(14) 0.0060(14)
C18 0.0318(14) 0.0343(14) 0.0209(12) 0.0044(10) -0.0010(10) 0.0002(11)
C40 0.0374(17) 0.0498(19) 0.0351(17) -0.0055(14) -0.0084(13) 0.0059(14)
C2 0.0236(13) 0.0409(15) 0.0185(12) -0.0007(10) 0.0055(10) 0.0009(11)
C1 0.0237(12) 0.0393(15) 0.0169(11) -0.0016(10) 0.0048(10) 0.0002(11)
C36 0.060(2) 0.0354(17) 0.0363(18) 0.0067(14) -0.0075(16) -0.0026(16)
C41 0.0466(19) 0.0484(19) 0.0227(14) -0.0032(13) -0.0057(13) 0.0081(15)
C22 0.0474(19) 0.059(2) 0.0255(15) -0.0004(14) 0.0084(14) 0.0105(16)
C14 0.050(2) 0.060(2) 0.0217(14) -0.0114(14) 0.0090(13) 0.0014(16)
C9 0.0274(15) 0.064(2) 0.0369(17) -0.0058(15) -0.0001(13) -0.0066(14)
C38 0.075(3) 0.0331(17) 0.049(2) -0.0022(15) -0.0210(19) 0.0037(17)
C12 0.046(2) 0.108(4) 0.050(2) -0.039(2) 0.0070(18) 0.017(2)
C13 0.080(3) 0.084(3) 0.0298(18) -0.0092(18) 0.0261(19) -0.022(2)
C23 0.0249(15) 0.067(2) 0.0402(18) 0.0159(16) 0.0011(13) 0.0017(15)
C5 0.0350(16) 0.0485(18) 0.0219(13) -0.0061(12) 0.0103(11) 0.0019(13)
C10 0.0286(16) 0.083(3) 0.047(2) -0.0170(19) 0.0135(15) -0.0136(17)
C11 0.0433(19) 0.062(2) 0.0262(15) -0.0110(14) 0.0142(13) -0.0026(16)
C42 0.059(2) 0.0440(18) 0.0284(16) 0.0008(13) -0.0172(15) 0.0056(16)
C37 0.058(2) 0.0407(19) 0.045(2) -0.0099(16) -0.0173(17) 0.0196(17)
C24 0.0466(19) 0.056(2) 0.0338(17) 0.0101(15) 0.0068(14) 0.0188(16)
C8 0.050(2) 0.049(2) 0.0395(18) -0.0043(15) 0.0177(15) -0.0148(16)
C6 0.0279(14) 0.0436(16) 0.0197(12) -0.0031(11) 0.0046(10) 0.0015(12)
C4 0.0288(15) 0.0489(18) 0.0322(15) -0.0065(13) 0.0143(12) -0.0021(13)
K1A 0.0297(4) 0.0449(5) 0.0512(6) 0.0048(4) 0.0013(4) -0.0111(4)
Si2A 0.0370(8) 0.0462(8) 0.0509(8) 0.0186(6) 0.0058(6) 0.0023(6)
Si1A 0.0275(7) 0.0354(6) 0.0537(7) 0.0061(5) -0.0044(5) -0.0015(5)
O4A 0.0314(17) 0.039(2) 0.036(3) 0.011(2) 0.001(2) -0.0079(13)
C26 0.054(5) 0.047(3) 0.033(3) 0.010(3) 0.005(3) -0.011(3)
C27 0.124(10) 0.094(8) 0.045(5) 0.036(5) 0.042(6) 0.062(8)
C28 0.111(8) 0.048(4) 0.019(3) 0.007(2) -0.001(3) -0.010(4)
C43 0.053(3) 0.044(2) 0.053(3) 0.009(2) -0.013(2) -0.004(2)
C44 0.046(3) 0.042(3) 0.061(4) -0.010(3) -0.008(3) 0.014(3)
C48 0.045(3) 0.074(4) 0.041(3) 0.007(2) -0.003(2) 0.000(2)
C45 0.030(2) 0.060(3) 0.080(4) 0.008(3) -0.004(2) -0.004(2)
C47 0.055(4) 0.074(5) 0.063(4) 0.026(3) 0.025(3) 0.002(3)
C46 0.060(5) 0.046(4) 0.082(5) 0.030(4) -0.007(4) -0.003(3)
K1B 0.0335(19) 0.051(2) 0.057(2) -0.0018(17) 0.0030(16) -0.0087(15)
Si1B 0.032(3) 0.047(3) 0.051(3) -0.003(2) -0.004(2) -0.003(2)
Si2B 0.065(5) 0.077(5) 0.077(5) 0.038(4) 0.022(4) -0.007(4)
O4B 0.067(12) 0.057(12) 0.017(9) 0.012(7) -0.003(8) -0.019(8)
C28B 0.068(9) 0.104(12) 0.016(4) 0.001(5) 0.007(4) -0.048(8)
C27B 0.029(4) 0.082(10) 0.030(5) 0.017(5) 0.017(4) -0.005(5)
C26B 0.084(12) 0.089(11) 0.050(9) 0.035(8) 0.037(8) 0.014(9)
C1AA 0.059(14) 0.084(17) 0.067(15) 0.000(13) -0.016(12) 0.021(12)
C0AA 0.13(4) 0.23(7) 0.12(4) 0.09(4) -0.01(3) -0.10(4)
C46A 0.16(4) 0.020(11) 0.14(3) 0.023(14) -0.04(3) -0.010(17)
C2AA 0.068(15) 0.092(18) 0.049(12) 0.006(11) 0.017(11) 0.016(13)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ni1 Ni1 2.6548(9) 2_655 ?
Ni1 Ni2 2.5744(7) . ?
Ni1 O3 1.8797(19) 2_655 ?
Ni1 O1 1.9021(19) . ?
Ni1 N1 1.855(2) 2_655 ?
Ni1 N1 1.852(2) . ?
Ni1 K1A 3.0048(10) . ?
Ni1 K1B 3.268(4) . ?
Ni2 O2 1.893(2) 2_655 ?
Ni2 O2 1.893(2) . ?
Ni2 N1 1.865(2) . ?
Ni2 N1 1.865(2) 2_655 ?
Ni2 K1A 3.4384(12) . ?
Ni2 K1A 3.4384(12) 2_655 ?
Ni2 K1B 3.058(4) 2_655 ?
Ni2 K1B 3.058(4) . ?
P1 N1 1.608(2) . ?
P1 C15 1.772(3) . ?
P1 C29 1.794(3) . ?
P1 C1 1.779(3) . ?
P1 K1B 3.760(4) 2_655 ?
O2 C30 1.322(3) . ?
O2 K1B 3.039(5) 2_655 ?
O3 C2 1.312(3) . ?
O3 K1A 3.344(2) 2_655 ?
O3 K1B 3.038(5) 2_655 ?
O1 C16 1.338(3) . ?
O1 K1A 2.797(2) . ?
N1 K1B 3.424(4) 2_655 ?
C33 C39 1.528(4) . ?
C33 C34 1.379(4) . ?
C33 C32 1.406(4) . ?
C39 C40 1.542(5) . ?
C39 C41 1.538(4) . ?
C39 C42 1.532(5) . ?
C34 H34 0.9500 . ?
C34 C29 1.410(4) . ?
C19 C20 1.368(4) . ?
C19 C25 1.541(4) . ?
C19 C18 1.402(4) . ?
C30 C29 1.421(4) . ?
C30 C31 1.439(4) . ?
C30 K1A 3.276(3) . ?
C15 C20 1.407(4) . ?
C15 C16 1.419(4) . ?
C17 C16 1.433(4) . ?
C17 C21 1.539(4) . ?
C17 C18 1.397(4) . ?
C3 C7 1.544(4) . ?
C3 C2 1.443(4) . ?
C3 C4 1.393(4) . ?
C29 K1A 3.373(3) . ?
C20 H20 0.9500 . ?
C7 C9 1.532(5) . ?
C7 C10 1.535(4) . ?
C7 C8 1.523(5) . ?
C21 C22 1.527(4) . ?
C21 C23 1.536(5) . ?
C21 C24 1.537(4) . ?
C31 C32 1.396(4) . ?
C31 C35 1.535(4) . ?
C25 C26 1.534(8) . ?
C25 C27 1.446(10) . ?
C25 C28 1.552(9) . ?
C25 C28B 1.567(14) . ?
C25 C27B 1.553(10) . ?
C25 C26B 1.459(15) . ?
C32 H32 0.9500 . ?
C35 C36 1.544(5) . ?
C35 C38 1.527(5) . ?
C35 C37 1.533(5) . ?
C18 H18 0.9500 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C2 C1 1.426(4) . ?
C2 K1B 2.969(5) 2_655 ?
C1 C6 1.415(4) . ?
C1 K1B 3.168(5) 2_655 ?
C36 H36A 1.11(5) . ?
C36 H36B 1.07(5) . ?
C36 H36C 0.82(5) . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C14 C11 1.530(5) . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C12 C11 1.516(6) . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 H13C 0.9800 . ?
C13 C11 1.548(6) . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C5 C11 1.539(4) . ?
C5 C6 1.372(4) . ?
C5 C4 1.403(5) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C37 H37A 0.96(5) . ?
C37 H37B 1.03(5) . ?
C37 H37C 1.00(5) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C6 H6 0.9500 . ?
C4 H4 0.9500 . ?
K1A O4A 2.788(5) . ?
Si2A O4A 1.670(4) . ?
Si2A C48 1.865(6) . ?
Si2A C47 1.871(7) . ?
Si2A C46 1.852(9) . ?
Si1A O4A 1.648(5) . ?
Si1A C43 1.867(5) . ?
Si1A C44 1.861(7) . ?
Si1A C45 1.847(5) . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C43 H43A 0.9800 . ?
C43 H43B 0.9800 . ?
C43 H43C 0.9800 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C48 H48A 0.97(8) . ?
C48 H48B 0.96(8) . ?
C48 H48C 0.95(7) . ?
C45 H45A 0.9800 . ?
C45 H45B 0.9800 . ?
C45 H45C 0.9800 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
K1B O4B 2.79(3) . ?
Si1B O4B 1.674(16) . ?
Si1B C1AA 1.85(2) . ?
Si1B C0AA 1.79(7) . ?
Si1B C2AA 1.92(3) . ?
Si2B O4B 1.62(2) . ?
Si2B C4AA 1.79(5) . ?
Si2B C47A 1.58(6) . ?
Si2B C46A 1.89(3) . ?
C28B H28D 0.9800 . ?
C28B H28E 0.9800 . ?
C28B H28F 0.9800 . ?
C27B H27D 0.9800 . ?
C27B H27E 0.9800 . ?
C27B H27F 0.9800 . ?
C26B H26D 0.9800 . ?
C26B H26E 0.9800 . ?
C26B H26F 0.9800 . ?
C1AA H1AA 0.9800 . ?
C1AA H1AB 0.9800 . ?
C1AA H1AC 0.9800 . ?
C0AA H0AA 0.9800 . ?
C0AA H0AB 0.9800 . ?
C0AA H0AC 0.9800 . ?
C4AA H4AA 0.9800 . ?
C4AA H4AB 0.9800 . ?
C4AA H4AC 0.9800 . ?
C47A H47D 0.9800 . ?
C47A H47E 0.9800 . ?
C47A H47F 0.9800 . ?
C46A H46D 0.9800 . ?
C46A H46E 0.9800 . ?
C46A H46F 0.9800 . ?
C2AA H2AA 0.9801 . ?
C2AA H2AB 0.9801 . ?
C2AA H2AC 0.9801 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ni1 Ni1 K1A 131.57(2) 2_655 . ?
Ni1 Ni1 K1B 116.50(7) 2_655 . ?
Ni2 Ni1 Ni1 58.963(12) . 2_655 ?
Ni2 Ni1 K1A 75.65(3) . . ?
Ni2 Ni1 K1B 61.78(7) . . ?
O3 Ni1 Ni1 133.33(6) 2_655 2_655 ?
O3 Ni1 Ni2 120.84(6) 2_655 . ?
O3 Ni1 O1 92.34(8) 2_655 . ?
O3 Ni1 K1A 83.00(7) 2_655 . ?
O3 Ni1 K1B 66.07(10) 2_655 . ?
O1 Ni1 Ni1 127.88(6) . 2_655 ?
O1 Ni1 Ni2 124.47(7) . . ?
O1 Ni1 K1A 65.06(7) . . ?
O1 Ni1 K1B 103.13(10) . . ?
N1 Ni1 Ni1 44.31(7) . 2_655 ?
N1 Ni1 Ni1 44.21(7) 2_655 2_655 ?
N1 Ni1 Ni2 46.37(7) 2_655 . ?
N1 Ni1 Ni2 46.38(7) . . ?
N1 Ni1 O3 167.21(9) . 2_655 ?
N1 Ni1 O3 98.47(9) 2_655 2_655 ?
N1 Ni1 O1 96.65(9) . . ?
N1 Ni1 O1 168.74(9) 2_655 . ?
N1 Ni1 N1 72.18(11) . 2_655 ?
N1 Ni1 K1A 112.98(8) 2_655 . ?
N1 Ni1 K1A 92.54(7) . . ?
N1 Ni1 K1B 78.62(10) 2_655 . ?
N1 Ni1 K1B 102.87(11) . . ?
Ni1 Ni2 Ni1 62.08(2) . 2_655 ?
Ni1 Ni2 K1A 117.64(2) 2_655 . ?
Ni1 Ni2 K1A 57.85(2) 2_655 2_655 ?
Ni1 Ni2 K1A 117.64(2) . 2_655 ?
Ni1 Ni2 K1A 57.85(2) . . ?
Ni1 Ni2 K1B 70.33(8) . . ?
Ni1 Ni2 K1B 70.33(8) 2_655 2_655 ?
Ni1 Ni2 K1B 127.07(8) 2_655 . ?
Ni1 Ni2 K1B 127.07(8) . 2_655 ?
O2 Ni2 Ni1 124.13(6) . . ?
O2 Ni2 Ni1 129.15(7) . 2_655 ?
O2 Ni2 Ni1 129.15(7) 2_655 . ?
O2 Ni2 Ni1 124.13(6) 2_655 2_655 ?
O2 Ni2 O2 91.81(13) 2_655 . ?
O2 Ni2 K1A 77.23(7) . . ?
O2 Ni2 K1A 106.05(7) 2_655 . ?
O2 Ni2 K1A 77.23(7) 2_655 2_655 ?
O2 Ni2 K1A 106.05(7) . 2_655 ?
O2 Ni2 K1B 95.91(11) . . ?
O2 Ni2 K1B 71.39(11) 2_655 . ?
O2 Ni2 K1B 95.91(11) 2_655 2_655 ?
O2 Ni2 K1B 71.39(11) . 2_655 ?
N1 Ni2 Ni1 46.05(7) 2_655 . ?
N1 Ni2 Ni1 46.05(7) . 2_655 ?
N1 Ni2 Ni1 45.94(7) 2_655 2_655 ?
N1 Ni2 Ni1 45.94(7) . . ?
N1 Ni2 O2 98.37(9) 2_655 2_655 ?
N1 Ni2 O2 98.37(9) . . ?
N1 Ni2 O2 169.35(9) 2_655 . ?
N1 Ni2 O2 169.35(9) . 2_655 ?
N1 Ni2 N1 71.66(13) . 2_655 ?
N1 Ni2 K1A 79.44(7) 2_655 2_655 ?
N1 Ni2 K1A 96.82(7) 2_655 . ?
N1 Ni2 K1A 96.82(7) . 2_655 ?
N1 Ni2 K1A 79.44(7) . . ?
N1 Ni2 K1B 110.39(11) . . ?
N1 Ni2 K1B 84.46(10) . 2_655 ?
N1 Ni2 K1B 84.46(10) 2_655 . ?
N1 Ni2 K1B 110.39(11) 2_655 2_655 ?
K1A Ni2 K1A 175.44(4) . 2_655 ?
K1B Ni2 K1B 162.12(16) . 2_655 ?
N1 P1 C15 109.13(12) . . ?
N1 P1 C29 108.27(12) . . ?
N1 P1 C1 109.03(12) . . ?
N1 P1 K1B 65.59(11) . 2_655 ?
C15 P1 C29 106.79(13) . . ?
C15 P1 C1 110.91(13) . . ?
C15 P1 K1B 160.10(12) . 2_655 ?
C29 P1 K1B 92.93(11) . 2_655 ?
C1 P1 C29 112.62(13) . . ?
C1 P1 K1B 57.10(11) . 2_655 ?
Ni2 O2 K1B 72.44(11) . 2_655 ?
C30 O2 Ni2 125.87(18) . . ?
C30 O2 K1B 120.9(2) . 2_655 ?
Ni1 O3 K1A 63.10(6) 2_655 2_655 ?
Ni1 O3 K1B 79.49(11) 2_655 2_655 ?
C2 O3 Ni1 130.76(18) . 2_655 ?
C2 O3 K1A 112.60(17) . 2_655 ?
C2 O3 K1B 74.49(18) . 2_655 ?
Ni1 O1 K1A 76.88(7) . . ?
C16 O1 Ni1 125.81(17) . . ?
C16 O1 K1A 128.37(18) . . ?
Ni1 N1 Ni1 91.48(10) . 2_655 ?
Ni1 N1 Ni2 87.58(9) 2_655 . ?
Ni1 N1 Ni2 87.68(9) . . ?
Ni1 N1 K1B 69.30(10) 2_655 2_655 ?
Ni1 N1 K1B 144.40(12) . 2_655 ?
Ni2 N1 K1B 62.71(10) . 2_655 ?
P1 N1 Ni1 125.57(13) . . ?
P1 N1 Ni1 127.36(13) . 2_655 ?
P1 N1 Ni2 125.01(14) . . ?
P1 N1 K1B 89.10(12) . 2_655 ?
C34 C33 C39 122.6(3) . . ?
C34 C33 C32 116.7(3) . . ?
C32 C33 C39 120.6(3) . . ?
C33 C39 C40 109.3(3) . . ?
C33 C39 C41 109.3(2) . . ?
C33 C39 C42 112.0(3) . . ?
C41 C39 C40 109.8(3) . . ?
C42 C39 C40 108.4(3) . . ?
C42 C39 C41 108.0(3) . . ?
C33 C34 H34 119.2 . . ?
C33 C34 C29 121.5(3) . . ?
C29 C34 H34 119.2 . . ?
C20 C19 C25 121.2(3) . . ?
C20 C19 C18 116.7(2) . . ?
C18 C19 C25 122.1(3) . . ?
O2 C30 C29 123.8(3) . . ?
O2 C30 C31 119.2(3) . . ?
O2 C30 K1A 90.33(16) . . ?
C29 C30 C31 117.0(2) . . ?
C29 C30 K1A 81.52(16) . . ?
C31 C30 K1A 97.51(18) . . ?
C20 C15 P1 117.8(2) . . ?
C20 C15 C16 122.1(3) . . ?
C16 C15 P1 119.8(2) . . ?
C16 C17 C21 120.5(2) . . ?
C18 C17 C16 118.5(3) . . ?
C18 C17 C21 121.0(3) . . ?
C2 C3 C7 120.4(3) . . ?
C4 C3 C7 120.6(3) . . ?
C4 C3 C2 119.0(3) . . ?
P1 C29 K1A 96.48(10) . . ?
C34 C29 P1 117.1(2) . . ?
C34 C29 C30 121.8(3) . . ?
C34 C29 K1A 99.57(17) . . ?
C30 C29 P1 121.07(19) . . ?
C30 C29 K1A 73.85(15) . . ?
C19 C20 C15 121.5(3) . . ?
C19 C20 H20 119.2 . . ?
C15 C20 H20 119.2 . . ?
C9 C7 C3 110.8(3) . . ?
C9 C7 C10 108.4(3) . . ?
C10 C7 C3 111.9(3) . . ?
C8 C7 C3 109.8(3) . . ?
C8 C7 C9 109.2(3) . . ?
C8 C7 C10 106.7(3) . . ?
O1 C16 C15 123.2(2) . . ?
O1 C16 C17 120.2(2) . . ?
C15 C16 C17 116.6(2) . . ?
C22 C21 C17 109.5(2) . . ?
C22 C21 C23 110.8(3) . . ?
C22 C21 C24 107.0(3) . . ?
C23 C21 C17 110.1(3) . . ?
C23 C21 C24 107.5(3) . . ?
C24 C21 C17 111.9(2) . . ?
C30 C31 C35 120.8(2) . . ?
C32 C31 C30 118.4(3) . . ?
C32 C31 C35 120.8(3) . . ?
C19 C25 C28 106.6(4) . . ?
C19 C25 C28B 108.0(5) . . ?
C19 C25 C27B 110.3(5) . . ?
C26 C25 C19 109.1(4) . . ?
C26 C25 C28 107.0(4) . . ?
C27 C25 C19 113.0(4) . . ?
C27 C25 C26 111.7(7) . . ?
C27 C25 C28 109.2(7) . . ?
C27B C25 C28B 103.9(7) . . ?
C26B C25 C19 115.2(6) . . ?
C26B C25 C28B 110.8(9) . . ?
C26B C25 C27B 108.1(9) . . ?
C33 C32 H32 117.8 . . ?
C31 C32 C33 124.5(3) . . ?
C31 C32 H32 117.8 . . ?
C31 C35 C36 109.4(3) . . ?
C38 C35 C31 112.7(3) . . ?
C38 C35 C36 107.4(3) . . ?
C38 C35 C37 107.0(3) . . ?
C37 C35 C31 110.0(3) . . ?
C37 C35 C36 110.4(3) . . ?
C19 C18 H18 117.7 . . ?
C17 C18 C19 124.5(3) . . ?
C17 C18 H18 117.7 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40B 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
O3 C2 C3 118.5(3) . . ?
O3 C2 C1 125.2(2) . . ?
O3 C2 K1B 80.31(18) . 2_655 ?
C3 C2 K1B 106.4(2) . 2_655 ?
C1 C2 C3 116.3(2) . . ?
C1 C2 K1B 84.48(19) . 2_655 ?
P1 C1 K1B 94.77(13) . 2_655 ?
C2 C1 P1 122.4(2) . . ?
C2 C1 K1B 68.91(18) . 2_655 ?
C6 C1 P1 115.4(2) . . ?
C6 C1 C2 121.9(2) . . ?
C6 C1 K1B 113.4(2) . 2_655 ?
C35 C36 H36A 112(2) . . ?
C35 C36 H36B 107(3) . . ?
C35 C36 H36C 109(4) . . ?
H36A C36 H36B 104(4) . . ?
H36A C36 H36C 112(4) . . ?
H36B C36 H36C 114(4) . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41B 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22B 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
H14A C14 H14B 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C11 C14 H14A 109.5 . . ?
C11 C14 H14B 109.5 . . ?
C11 C14 H14C 109.5 . . ?
C7 C9 H9A 109.5 . . ?
C7 C9 H9B 109.5 . . ?
C7 C9 H9C 109.5 . . ?
H9A C9 H9B 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C35 C38 H38A 109.5 . . ?
C35 C38 H38B 109.5 . . ?
C35 C38 H38C 109.5 . . ?
H38A C38 H38B 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
H12A C12 H12B 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H13A C13 H13B 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
C11 C13 H13A 109.5 . . ?
C11 C13 H13B 109.5 . . ?
C11 C13 H13C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23B 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C6 C5 C11 122.8(3) . . ?
C6 C5 C4 117.0(3) . . ?
C4 C5 C11 120.1(3) . . ?
C7 C10 H10A 109.5 . . ?
C7 C10 H10B 109.5 . . ?
C7 C10 H10C 109.5 . . ?
H10A C10 H10B 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C14 C11 C13 108.2(3) . . ?
C14 C11 C5 112.2(3) . . ?
C12 C11 C14 108.3(3) . . ?
C12 C11 C13 110.2(4) . . ?
C12 C11 C5 109.3(3) . . ?
C5 C11 C13 108.5(3) . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42B 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C35 C37 H37A 113(3) . . ?
C35 C37 H37B 109(3) . . ?
C35 C37 H37C 119(3) . . ?
H37A C37 H37B 109(4) . . ?
H37A C37 H37C 93(4) . . ?
H37B C37 H37C 112(4) . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24B 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8B 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C1 C6 H6 119.3 . . ?
C5 C6 C1 121.5(3) . . ?
C5 C6 H6 119.3 . . ?
C3 C4 C5 124.3(3) . . ?
C3 C4 H4 117.8 . . ?
C5 C4 H4 117.8 . . ?
Ni1 K1A Ni2 46.500(18) . . ?
Ni1 K1A O3 33.91(4) . 2_655 ?
Ni1 K1A C30 85.06(6) . . ?
Ni1 K1A C29 75.70(5) . . ?
O3 K1A Ni2 69.95(4) 2_655 . ?
O3 K1A C29 109.49(6) 2_655 . ?
O1 K1A Ni1 38.06(4) . . ?
O1 K1A Ni2 78.42(4) . . ?
O1 K1A O3 51.81(5) . 2_655 ?
O1 K1A C30 93.71(7) . . ?
O1 K1A C29 72.24(7) . . ?
C30 K1A Ni2 50.63(5) . . ?
C30 K1A O3 117.13(7) . 2_655 ?
C30 K1A C29 24.62(7) . . ?
C29 K1A Ni2 58.87(5) . . ?
O4A K1A Ni1 141.05(12) . . ?
O4A K1A Ni2 127.97(10) . . ?
O4A K1A O3 109.01(13) . 2_655 ?
O4A K1A O1 143.80(13) . . ?
O4A K1A C30 121.86(14) . . ?
O4A K1A C29 140.03(14) . . ?
O4A Si2A C48 106.3(3) . . ?
O4A Si2A C47 111.6(3) . . ?
O4A Si2A C46 108.5(4) . . ?
C48 Si2A C47 109.3(4) . . ?
C46 Si2A C48 111.9(3) . . ?
C46 Si2A C47 109.2(4) . . ?
O4A Si1A C43 106.5(2) . . ?
O4A Si1A C44 107.3(3) . . ?
O4A Si1A C45 111.8(3) . . ?
C44 Si1A C43 109.1(4) . . ?
C45 Si1A C43 109.9(3) . . ?
C45 Si1A C44 112.0(4) . . ?
Si2A O4A K1A 117.8(2) . . ?
Si1A O4A K1A 106.1(2) . . ?
Si1A O4A Si2A 135.6(3) . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26B 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C25 C27 H27A 109.5 . . ?
C25 C27 H27B 109.5 . . ?
C25 C27 H27C 109.5 . . ?
H27A C27 H27B 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C25 C28 H28A 109.5 . . ?
C25 C28 H28B 109.5 . . ?
C25 C28 H28C 109.5 . . ?
H28A C28 H28B 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
Si1A C43 H43A 109.5 . . ?
Si1A C43 H43B 109.5 . . ?
Si1A C43 H43C 109.5 . . ?
H43A C43 H43B 109.5 . . ?
H43A C43 H43C 109.5 . . ?
H43B C43 H43C 109.5 . . ?
Si1A C44 H44A 109.5 . . ?
Si1A C44 H44B 109.5 . . ?
Si1A C44 H44C 109.5 . . ?
H44A C44 H44B 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
Si2A C48 H48A 119(4) . . ?
Si2A C48 H48B 116(4) . . ?
Si2A C48 H48C 117(4) . . ?
H48A C48 H48B 99(6) . . ?
H48A C48 H48C 107(6) . . ?
H48B C48 H48C 95(6) . . ?
Si1A C45 H45A 109.5 . . ?
Si1A C45 H45B 109.5 . . ?
Si1A C45 H45C 109.5 . . ?
H45A C45 H45B 109.5 . . ?
H45A C45 H45C 109.5 . . ?
H45B C45 H45C 109.5 . . ?
Si2A C47 H47A 109.5 . . ?
Si2A C47 H47B 109.5 . . ?
Si2A C47 H47C 109.5 . . ?
H47A C47 H47B 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
Si2A C46 H46A 109.5 . . ?
Si2A C46 H46B 109.5 . . ?
Si2A C46 H46C 109.5 . . ?
H46A C46 H46B 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
Ni1 K1B P1 51.87(6) . 2_655 ?
Ni1 K1B N1 32.08(5) . 2_655 ?
Ni2 K1B Ni1 47.89(6) . . ?
Ni2 K1B P1 52.54(6) . 2_655 ?
Ni2 K1B N1 32.83(5) . 2_655 ?
Ni2 K1B C1 80.13(10) . 2_655 ?
O2 K1B Ni1 79.70(10) 2_655 . ?
O2 K1B Ni2 36.17(6) 2_655 . ?
O2 K1B P1 53.24(7) 2_655 2_655 ?
O2 K1B N1 51.79(8) 2_655 2_655 ?
O2 K1B C1 77.82(11) 2_655 2_655 ?
O3 K1B Ni1 34.44(6) 2_655 . ?
O3 K1B Ni2 79.28(10) 2_655 . ?
O3 K1B P1 54.33(7) 2_655 2_655 ?
O3 K1B O2 102.71(12) 2_655 2_655 ?
O3 K1B N1 51.49(8) 2_655 2_655 ?
O3 K1B C1 46.07(9) 2_655 2_655 ?
N1 K1B P1 25.31(4) 2_655 2_655 ?
C2 K1B Ni1 55.39(9) 2_655 . ?
C2 K1B Ni2 90.98(12) 2_655 . ?
C2 K1B P1 47.67(8) 2_655 2_655 ?
C2 K1B O2 100.88(13) 2_655 2_655 ?
C2 K1B O3 25.20(7) 2_655 2_655 ?
C2 K1B N1 58.38(9) 2_655 2_655 ?
C2 K1B C1 26.62(8) 2_655 2_655 ?
C1 K1B Ni1 63.51(9) 2_655 . ?
C1 K1B P1 28.13(6) 2_655 2_655 ?
C1 K1B N1 49.30(8) 2_655 2_655 ?
O4B K1B Ni1 130.0(4) . . ?
O4B K1B Ni2 141.7(5) . . ?
O4B Si1B C1AA 108.4(13) . . ?
O4B Si1B C0AA 110(2) . . ?
O4B Si1B C2AA 109.3(12) . . ?
C1AA Si1B C2AA 111.4(12) . . ?
C0AA Si1B C1AA 105(2) . . ?
C0AA Si1B C2AA 112(2) . . ?
O4B Si2B C4AA 108(2) . . ?
O4B Si2B C46A 108.8(19) . . ?
C4AA Si2B C46A 111(2) . . ?
C47A Si2B O4B 111(3) . . ?
C47A Si2B C4AA 104(3) . . ?
C47A Si2B C46A 114(3) . . ?
Si1B O4B K1B 108.4(11) . . ?
Si2B O4B K1B 108.6(10) . . ?
Si2B O4B Si1B 142.8(18) . . ?
C25 C28B H28D 109.5 . . ?
C25 C28B H28E 109.5 . . ?
C25 C28B H28F 109.5 . . ?
H28D C28B H28E 109.5 . . ?
H28D C28B H28F 109.5 . . ?
H28E C28B H28F 109.5 . . ?
C25 C27B H27D 109.5 . . ?
C25 C27B H27E 109.5 . . ?
C25 C27B H27F 109.5 . . ?
H27D C27B H27E 109.5 . . ?
H27D C27B H27F 109.5 . . ?
H27E C27B H27F 109.5 . . ?
C25 C26B H26D 109.5 . . ?
C25 C26B H26E 109.5 . . ?
C25 C26B H26F 109.5 . . ?
H26D C26B H26E 109.5 . . ?
H26D C26B H26F 109.5 . . ?
H26E C26B H26F 109.5 . . ?
Si1B C1AA H1AA 109.5 . . ?
Si1B C1AA H1AB 109.5 . . ?
Si1B C1AA H1AC 109.5 . . ?
H1AA C1AA H1AB 109.5 . . ?
H1AA C1AA H1AC 109.5 . . ?
H1AB C1AA H1AC 109.5 . . ?
Si1B C0AA H0AA 109.5 . . ?
Si1B C0AA H0AB 109.5 . . ?
Si1B C0AA H0AC 109.5 . . ?
H0AA C0AA H0AB 109.5 . . ?
H0AA C0AA H0AC 109.5 . . ?
H0AB C0AA H0AC 109.5 . . ?
Si2B C4AA H4AA 109.5 . . ?
Si2B C4AA H4AB 109.5 . . ?
Si2B C4AA H4AC 109.5 . . ?
H4AA C4AA H4AB 109.5 . . ?
H4AA C4AA H4AC 109.5 . . ?
H4AB C4AA H4AC 109.5 . . ?
Si2B C47A H47D 109.5 . . ?
Si2B C47A H47E 109.5 . . ?
Si2B C47A H47F 109.5 . . ?
H47D C47A H47E 109.5 . . ?
H47D C47A H47F 109.5 . . ?
H47E C47A H47F 109.5 . . ?
Si2B C46A H46D 109.5 . . ?
Si2B C46A H46E 109.5 . . ?
Si2B C46A H46F 109.5 . . ?
H46D C46A H46E 109.5 . . ?
H46D C46A H46F 109.5 . . ?
H46E C46A H46F 109.5 . . ?
Si1B C2AA H2AA 109.5 . . ?
Si1B C2AA H2AB 109.5 . . ?
Si1B C2AA H2AC 109.5 . . ?
H2AA C2AA H2AB 109.5 . . ?
H2AA C2AA H2AC 109.5 . . ?
H2AB C2AA H2AC 109.5 . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ni1 Ni1 N1 Ni2 -87.52(9) 2_655 . . . ?
Ni1 Ni1 N1 P1 139.9(2) 2_655 . . . ?
Ni1 Ni1 N1 K1B -55.17(18) 2_655 . . 2_655 ?
Ni1 Ni2 O2 C30 72.9(3) 2_655 . . . ?
Ni1 Ni2 O2 C30 -6.8(3) . . . . ?
Ni1 Ni2 O2 K1B -122.69(9) . . . 2_655 ?
Ni1 Ni2 O2 K1B -42.93(11) 2_655 . . 2_655 ?
Ni1 Ni2 N1 Ni1 -91.58(9) . . . 2_655 ?
Ni1 Ni2 N1 Ni1 91.58(9) 2_655 . . . ?
Ni1 Ni2 N1 P1 133.03(19) . . . . ?
Ni1 Ni2 N1 P1 -135.39(19) 2_655 . . . ?
Ni1 Ni2 N1 K1B -159.48(11) . . . 2_655 ?
Ni1 Ni2 N1 K1B -67.90(10) 2_655 . . 2_655 ?
Ni1 O3 C2 C3 164.2(2) 2_655 . . . ?
Ni1 O3 C2 C1 -15.4(4) 2_655 . . . ?
Ni1 O3 C2 K1B 60.7(2) 2_655 . . 2_655 ?
Ni1 O1 C16 C15 -38.5(4) . . . . ?
Ni1 O1 C16 C17 143.1(2) . . . . ?
Ni2 Ni1 N1 Ni1 87.52(9) . . . 2_655 ?
Ni2 Ni1 N1 P1 -132.6(2) . . . . ?
Ni2 Ni1 N1 K1B 32.35(17) . . . 2_655 ?
Ni2 O2 C30 C29 -36.3(4) . . . . ?
Ni2 O2 C30 C31 142.5(2) . . . . ?
Ni2 O2 C30 K1A 43.7(2) . . . . ?
P1 C15 C20 C19 -172.4(2) . . . . ?
P1 C15 C16 O1 -4.4(4) . . . . ?
P1 C15 C16 C17 174.1(2) . . . . ?
P1 C1 C6 C5 -170.7(3) . . . . ?
O2 Ni2 O2 C30 -148.5(3) 2_655 . . . ?
O2 Ni2 O2 K1B 95.62(11) 2_655 . . 2_655 ?
O2 Ni2 N1 Ni1 -130.30(9) . . . . ?
O2 Ni2 N1 Ni1 67.0(5) 2_655 . . . ?
O2 Ni2 N1 Ni1 138.12(9) . . . 2_655 ?
O2 Ni2 N1 Ni1 -24.6(6) 2_655 . . 2_655 ?
O2 Ni2 N1 P1 2.73(17) . . . . ?
O2 Ni2 N1 P1 -160.0(4) 2_655 . . . ?
O2 Ni2 N1 K1B 70.22(11) . . . 2_655 ?
O2 Ni2 N1 K1B -92.5(5) 2_655 . . 2_655 ?
O2 C30 C29 P1 -3.2(4) . . . . ?
O2 C30 C29 C34 176.1(3) . . . . ?
O2 C30 C29 K1A 84.7(3) . . . . ?
O2 C30 C31 C32 -177.0(3) . . . . ?
O2 C30 C31 C35 2.5(4) . . . . ?
O3 Ni1 N1 Ni1 85.7(4) 2_655 . . 2_655 ?
O3 Ni1 N1 Ni2 -1.8(5) 2_655 . . . ?
O3 Ni1 N1 P1 -134.4(4) 2_655 . . . ?
O3 Ni1 N1 K1B 30.5(5) 2_655 . . 2_655 ?
O3 C2 C1 P1 -7.9(4) . . . . ?
O3 C2 C1 C6 179.1(3) . . . . ?
O3 C2 C1 K1B 74.0(3) . . . 2_655 ?
O1 Ni1 N1 Ni1 -139.95(9) . . . 2_655 ?
O1 Ni1 N1 Ni2 132.53(9) . . . . ?
O1 Ni1 N1 P1 -0.07(18) . . . . ?
O1 Ni1 N1 K1B 164.9(2) . . . 2_655 ?
N1 Ni1 N1 Ni1 41.53(12) 2_655 . . 2_655 ?
N1 Ni1 N1 Ni2 -45.99(8) 2_655 . . . ?
N1 Ni1 N1 P1 -178.59(14) 2_655 . . . ?
N1 Ni1 N1 K1B -13.6(2) 2_655 . . 2_655 ?
N1 Ni2 O2 C30 14.4(7) 2_655 . . . ?
N1 Ni2 O2 C30 34.6(3) . . . . ?
N1 Ni2 O2 K1B -101.4(5) 2_655 . . 2_655 ?
N1 Ni2 O2 K1B -81.23(11) . . . 2_655 ?
N1 Ni2 N1 Ni1 45.85(7) 2_655 . . . ?
N1 Ni2 N1 Ni1 -45.74(7) 2_655 . . 2_655 ?
N1 Ni2 N1 P1 178.9(2) 2_655 . . . ?
N1 Ni2 N1 K1B -113.64(13) 2_655 . . 2_655 ?
N1 P1 C15 C20 -149.6(2) . . . . ?
N1 P1 C15 C16 36.4(3) . . . . ?
N1 P1 C29 C34 -144.7(2) . . . . ?
N1 P1 C29 C30 34.6(3) . . . . ?
N1 P1 C29 K1A -40.47(12) . . . . ?
N1 P1 C1 C2 26.0(3) . . . . ?
N1 P1 C1 C6 -160.6(2) . . . . ?
N1 P1 C1 K1B -41.94(15) . . . 2_655 ?
C33 C34 C29 P1 -179.5(2) . . . . ?
C33 C34 C29 C30 1.3(4) . . . . ?
C33 C34 C29 K1A 78.1(3) . . . . ?
C39 C33 C34 C29 -179.3(3) . . . . ?
C39 C33 C32 C31 178.4(3) . . . . ?
C34 C33 C39 C40 121.8(3) . . . . ?
C34 C33 C39 C41 -118.1(3) . . . . ?
C34 C33 C39 C42 1.6(4) . . . . ?
C34 C33 C32 C31 -2.1(5) . . . . ?
C30 C31 C32 C33 0.6(5) . . . . ?
C30 C31 C35 C36 -60.7(4) . . . . ?
C30 C31 C35 C38 179.9(3) . . . . ?
C30 C31 C35 C37 60.7(4) . . . . ?
C15 P1 N1 Ni1 96.49(18) . . . 2_655 ?
C15 P1 N1 Ni1 -29.4(2) . . . . ?
C15 P1 N1 Ni2 -145.49(15) . . . . ?
C15 P1 N1 K1B 159.32(12) . . . 2_655 ?
C15 P1 C29 C34 -27.3(2) . . . . ?
C15 P1 C29 C30 151.9(2) . . . . ?
C15 P1 C29 K1A 76.92(12) . . . . ?
C15 P1 C1 C2 -94.1(3) . . . . ?
C15 P1 C1 C6 79.2(3) . . . . ?
C15 P1 C1 K1B -162.13(13) . . . 2_655 ?
C3 C2 C1 P1 172.4(2) . . . . ?
C3 C2 C1 C6 -0.5(4) . . . . ?
C3 C2 C1 K1B -105.6(3) . . . 2_655 ?
C29 P1 N1 Ni1 -147.63(16) . . . 2_655 ?
C29 P1 N1 Ni1 86.51(18) . . . . ?
C29 P1 N1 Ni2 -29.60(19) . . . . ?
C29 P1 N1 K1B -84.80(13) . . . 2_655 ?
C29 P1 C15 C20 93.6(2) . . . . ?
C29 P1 C15 C16 -80.4(2) . . . . ?
C29 P1 C1 C2 146.2(2) . . . . ?
C29 P1 C1 C6 -40.4(3) . . . . ?
C29 P1 C1 K1B 78.26(14) . . . 2_655 ?
C29 C30 C31 C32 1.8(4) . . . . ?
C29 C30 C31 C35 -178.6(3) . . . . ?
C20 C19 C25 C26 129.2(5) . . . . ?
C20 C19 C25 C27 4.4(9) . . . . ?
C20 C19 C25 C28 -115.6(5) . . . . ?
C20 C19 C25 C28B -73.9(9) . . . . ?
C20 C19 C25 C27B 39.0(8) . . . . ?
C20 C19 C25 C26B 161.7(11) . . . . ?
C20 C19 C18 C17 0.0(5) . . . . ?
C20 C15 C16 O1 -178.1(3) . . . . ?
C20 C15 C16 C17 0.3(4) . . . . ?
C7 C3 C2 O3 0.3(4) . . . . ?
C7 C3 C2 C1 -180.0(3) . . . . ?
C7 C3 C2 K1B 88.1(3) . . . 2_655 ?
C7 C3 C4 C5 180.0(3) . . . . ?
C16 C15 C20 C19 1.5(4) . . . . ?
C16 C17 C21 C22 -59.6(4) . . . . ?
C16 C17 C21 C23 62.5(3) . . . . ?
C16 C17 C21 C24 -178.0(3) . . . . ?
C16 C17 C18 C19 1.8(4) . . . . ?
C21 C17 C16 O1 -4.3(4) . . . . ?
C21 C17 C16 C15 177.2(3) . . . . ?
C21 C17 C18 C19 -177.3(3) . . . . ?
C31 C30 C29 P1 178.0(2) . . . . ?
C31 C30 C29 C34 -2.8(4) . . . . ?
C31 C30 C29 K1A -94.1(2) . . . . ?
C25 C19 C20 C15 176.8(3) . . . . ?
C25 C19 C18 C17 -178.4(3) . . . . ?
C32 C33 C39 C40 -58.8(4) . . . . ?
C32 C33 C39 C41 61.4(4) . . . . ?
C32 C33 C39 C42 -178.9(3) . . . . ?
C32 C33 C34 C29 1.2(4) . . . . ?
C32 C31 C35 C36 118.9(3) . . . . ?
C32 C31 C35 C38 -0.5(5) . . . . ?
C32 C31 C35 C37 -119.7(3) . . . . ?
C35 C31 C32 C33 -179.0(3) . . . . ?
C18 C19 C20 C15 -1.6(4) . . . . ?
C18 C19 C25 C26 -52.4(5) . . . . ?
C18 C19 C25 C27 -177.3(9) . . . . ?
C18 C19 C25 C28 62.8(6) . . . . ?
C18 C19 C25 C28B 104.5(8) . . . . ?
C18 C19 C25 C27B -142.7(7) . . . . ?
C18 C19 C25 C26B -20.0(12) . . . . ?
C18 C17 C16 O1 176.6(3) . . . . ?
C18 C17 C16 C15 -1.9(4) . . . . ?
C18 C17 C21 C22 119.5(3) . . . . ?
C18 C17 C21 C23 -118.5(3) . . . . ?
C18 C17 C21 C24 1.0(4) . . . . ?
C2 C3 C7 C9 -57.4(4) . . . . ?
C2 C3 C7 C10 -178.5(3) . . . . ?
C2 C3 C7 C8 63.2(4) . . . . ?
C2 C3 C4 C5 1.5(5) . . . . ?
C2 C1 C6 C5 2.6(5) . . . . ?
C1 P1 N1 Ni1 -150.65(16) . . . . ?
C1 P1 N1 Ni1 -24.8(2) . . . 2_655 ?
C1 P1 N1 Ni2 93.24(17) . . . . ?
C1 P1 N1 K1B 38.04(14) . . . 2_655 ?
C1 P1 C15 C20 -29.5(3) . . . . ?
C1 P1 C15 C16 156.5(2) . . . . ?
C1 P1 C29 C34 94.6(2) . . . . ?
C1 P1 C29 C30 -86.1(2) . . . . ?
C1 P1 C29 K1A -161.11(10) . . . . ?
C11 C5 C6 C1 175.8(3) . . . . ?
C11 C5 C4 C3 -177.8(3) . . . . ?
C6 C5 C11 C14 0.2(5) . . . . ?
C6 C5 C11 C12 120.4(4) . . . . ?
C6 C5 C11 C13 -119.4(4) . . . . ?
C6 C5 C4 C3 0.6(5) . . . . ?
C4 C3 C7 C9 124.0(3) . . . . ?
C4 C3 C7 C10 2.9(5) . . . . ?
C4 C3 C7 C8 -115.3(3) . . . . ?
C4 C3 C2 O3 178.9(3) . . . . ?
C4 C3 C2 C1 -1.4(4) . . . . ?
C4 C3 C2 K1B -93.4(3) . . . 2_655 ?
C4 C5 C11 C14 178.5(3) . . . . ?
C4 C5 C11 C12 -61.3(5) . . . . ?
C4 C5 C11 C13 59.0(5) . . . . ?
C4 C5 C6 C1 -2.6(5) . . . . ?
K1A Ni1 N1 Ni1 154.87(7) . . . 2_655 ?
K1A Ni1 N1 Ni2 67.36(7) . . . . ?
K1A Ni1 N1 P1 -65.24(16) . . . . ?
K1A Ni2 O2 C30 134.3(2) 2_655 . . . ?
K1A Ni2 O2 C30 -42.5(2) . . . . ?
K1A Ni2 N1 Ni1 30.73(7) 2_655 . . 2_655 ?
K1A Ni2 N1 Ni1 -146.63(8) . . . 2_655 ?
K1A Ni2 N1 Ni1 -55.05(6) . . . . ?
K1A Ni2 N1 Ni1 122.31(6) 2_655 . . . ?
K1A Ni2 N1 P1 77.98(14) . . . . ?
K1A Ni2 N1 P1 -104.66(14) 2_655 . . . ?
K1A O3 C2 C3 91.0(3) 2_655 . . . ?
K1A O3 C2 C1 -88.6(3) 2_655 . . . ?
K1A O1 C16 C15 63.8(3) . . . . ?
K1A O1 C16 C17 -114.6(3) . . . . ?
K1A C30 C29 P1 -87.86(18) . . . . ?
K1A C30 C29 C34 91.4(2) . . . . ?
K1A C30 C31 C32 -82.4(3) . . . . ?
K1A C30 C31 C35 97.2(3) . . . . ?
C43 Si1A O4A K1A 34.9(3) . . . . ?
C43 Si1A O4A Si2A -154.3(5) . . . . ?
C44 Si1A O4A K1A -81.8(4) . . . . ?
C44 Si1A O4A Si2A 89.1(6) . . . . ?
C48 Si2A O4A K1A 3.0(4) . . . . ?
C48 Si2A O4A Si1A -167.1(5) . . . . ?
C45 Si1A O4A K1A 155.0(2) . . . . ?
C45 Si1A O4A Si2A -34.1(6) . . . . ?
C47 Si2A O4A K1A -116.0(4) . . . . ?
C47 Si2A O4A Si1A 73.9(6) . . . . ?
C46 Si2A O4A K1A 123.5(4) . . . . ?
C46 Si2A O4A Si1A -46.5(6) . . . . ?
K1B Ni1 N1 Ni1 114.91(10) . . . 2_655 ?
K1B Ni1 N1 Ni2 27.39(11) . . . . ?
K1B Ni1 N1 P1 -105.21(17) . . . . ?
K1B Ni1 N1 K1B 59.7(2) . . . 2_655 ?
K1B Ni2 O2 C30 -77.0(3) . . . . ?
K1B Ni2 O2 C30 115.9(3) 2_655 . . . ?
K1B Ni2 O2 K1B 167.10(12) . . . 2_655 ?
K1B Ni2 N1 Ni1 -30.76(12) . . . . ?
K1B Ni2 N1 Ni1 -122.34(10) . . . 2_655 ?
K1B Ni2 N1 Ni1 159.48(11) 2_655 . . . ?
K1B Ni2 N1 Ni1 67.90(10) 2_655 . . 2_655 ?
K1B Ni2 N1 P1 102.27(17) . . . . ?
K1B Ni2 N1 P1 -67.49(17) 2_655 . . . ?
K1B Ni2 N1 K1B 169.76(9) . . . 2_655 ?
K1B P1 N1 Ni1 -62.83(16) 2_655 . . 2_655 ?
K1B P1 N1 Ni1 171.3(2) 2_655 . . . ?
K1B P1 N1 Ni2 55.20(14) 2_655 . . . ?
K1B P1 C15 C20 -78.7(4) 2_655 . . . ?
K1B P1 C15 C16 107.3(4) 2_655 . . . ?
K1B P1 C29 C34 150.0(2) 2_655 . . . ?
K1B P1 C29 C30 -30.7(2) 2_655 . . . ?
K1B P1 C1 C2 68.0(2) 2_655 . . . ?
K1B P1 C1 C6 -118.7(3) 2_655 . . . ?
K1B O2 C30 C29 53.7(3) 2_655 . . . ?
K1B O2 C30 C31 -127.5(2) 2_655 . . . ?
K1B O3 C2 C3 103.5(3) 2_655 . . . ?
K1B O3 C2 C1 -76.1(3) 2_655 . . . ?
K1B C2 C1 P1 -82.0(2) 2_655 . . . ?
K1B C2 C1 C6 105.1(3) 2_655 . . . ?
K1B C1 C6 C5 81.5(3) 2_655 . . . ?
C1AA Si1B O4B K1B 126.6(13) . . . . ?
C1AA Si1B O4B Si2B -60(3) . . . . ?
C0AA Si1B O4B K1B -119(2) . . . . ?
C0AA Si1B O4B Si2B 55(4) . . . . ?
C4AA Si2B O4B K1B 2(2) . . . . ?
C4AA Si2B O4B Si1B -172(3) . . . . ?
C47A Si2B O4B K1B -111(3) . . . . ?
C47A Si2B O4B Si1B 75(4) . . . . ?
C46A Si2B O4B K1B 123.1(19) . . . . ?
C46A Si2B O4B Si1B -51(4) . . . . ?
C2AA Si1B O4B K1B 5.0(16) . . . . ?
C2AA Si1B O4B Si2B 179(3) . . . . ?
_shelx_res_file
;
TITL v18433 in C2/c
v18433.res
created by SHELXL-2018/3 at 20:00:50 on 30-Jun-2020
CELL 0.71073 28.0668 20.5739 18.0517 90 97.2147 90
ZERR 4 0.0061 0.0035 0.0038 0 0.007 0
LATT 7
SYMM -X,+Y,0.5-Z
SFAC C H K N Ni O P Si
UNIT 374.57 595.7 8 8 12 32 8 16
L.S. 40
PLAN 10
SIZE 0.12 0.16 0.24
TEMP -173.15
FREE K1A C43
FREE K1A Si1A
FREE K1A Si2A
FREE K1A H43a
FREE K1B Si2B
FREE K1B Si1B
FREE K1B C4AA
FREE K1B H4Ac
FREE K1B C2AA
FREE K1B H2Aa
FREE K1B H2Ab
FREE K1B H2Ac
CONF
MORE -1
BOND $H
fmap -2
acta
OMIT -2 4 2
OMIT 2 2 0
OMIT -3 1 1
OMIT 0 0 2
OMIT 2 2 1
REM
REM
REM
WGHT 0.082400 29.148800
FVAR 0.03751 0.79657 0.61014
NI1 5 0.547662 0.186928 0.257857 11.00000 0.01939 0.03284 =
0.01350 0.00143 0.00231 -0.00038
NI2 5 0.500000 0.294141 0.250000 10.50000 0.02183 0.03217 =
0.01404 0.00000 -0.00017 0.00000
P1 7 0.503057 0.221757 0.400039 11.00000 0.02199 0.03563 =
0.01311 0.00039 0.00218 -0.00008
O2 6 0.505593 0.358158 0.325903 11.00000 0.04040 0.03547 =
0.01724 -0.00280 -0.00551 0.00942
O3 6 0.406961 0.169997 0.307921 11.00000 0.02572 0.04099 =
0.01761 -0.00360 0.00588 -0.00367
O1 6 0.590585 0.160022 0.342257 11.00000 0.02134 0.04736 =
0.01665 0.00823 0.00144 0.00002
N1 4 0.500860 0.220644 0.310633 11.00000 0.02034 0.03403 =
0.01328 -0.00104 0.00198 0.00042
C33 1 0.589291 0.341524 0.534911 11.00000 0.03063 0.03856 =
0.01902 -0.00300 -0.00280 0.00728
C39 1 0.621726 0.337579 0.609388 11.00000 0.03681 0.03767 =
0.02063 -0.00352 -0.00828 0.00503
C34 1 0.563916 0.288860 0.503553 11.00000 0.02708 0.03688 =
0.01651 0.00051 0.00019 0.00290
AFIX 43
H34 2 0.566227 0.248416 0.529147 11.00000 -1.20000
AFIX 0
C19 1 0.553538 0.080712 0.542566 11.00000 0.03460 0.03966 =
0.01714 0.00433 0.00357 -0.00199
C30 1 0.530473 0.352471 0.392813 11.00000 0.02529 0.03728 =
0.01805 -0.00358 -0.00215 0.00758
C15 1 0.537352 0.154582 0.438003 11.00000 0.02404 0.03583 =
0.01616 0.00347 0.00084 -0.00176
C17 1 0.606598 0.083428 0.442769 11.00000 0.02359 0.03591 =
0.01889 0.00327 -0.00050 -0.00238
C3 1 0.360005 0.183303 0.407122 11.00000 0.02455 0.04326 =
0.02657 -0.00413 0.00817 -0.00113
C29 1 0.534604 0.293643 0.434355 11.00000 0.02380 0.03484 =
0.01597 -0.00215 0.00045 0.00244
C20 1 0.525610 0.127567 0.505001 11.00000 0.02997 0.03736 =
0.01884 0.00154 0.00541 -0.00159
AFIX 43
H20 2 0.497628 0.142222 0.524590 11.00000 -1.20000
AFIX 0
C7 1 0.315814 0.152988 0.360117 11.00000 0.02611 0.04990 =
0.03413 -0.00634 0.00871 -0.00525
C16 1 0.577983 0.133851 0.404790 11.00000 0.02301 0.03561 =
0.01686 0.00439 0.00032 -0.00506
C21 1 0.650077 0.055453 0.409391 11.00000 0.02873 0.04531 =
0.02337 0.00736 0.00252 0.00489
C31 1 0.555880 0.408085 0.426098 11.00000 0.03489 0.03261 =
0.02246 -0.00380 -0.00238 0.00693
C25 1 0.541878 0.053915 0.617953 11.00000 0.04435 0.05240 =
0.02246 0.01262 0.00670 -0.00105
C32 1 0.583792 0.400418 0.495220 11.00000 0.03758 0.03349 =
0.02616 -0.00581 -0.00628 0.00667
AFIX 43
H32 2 0.600185 0.437521 0.516912 11.00000 -1.20000
AFIX 0
C35 1 0.552661 0.474177 0.386318 11.00000 0.05349 0.03125 =
0.03359 -0.00247 -0.01496 0.00596
C18 1 0.593670 0.059773 0.510001 11.00000 0.03180 0.03427 =
0.02087 0.00439 -0.00102 0.00024
AFIX 43
H18 2 0.613443 0.027242 0.535419 11.00000 -1.20000
AFIX 0
C40 1 0.673212 0.357417 0.597616 11.00000 0.03742 0.04982 =
0.03513 -0.00550 -0.00842 0.00585
AFIX 137
H40A 2 0.685193 0.327914 0.561549 11.00000 -1.50000
H40B 2 0.694118 0.354926 0.645280 11.00000 -1.50000
H40C 2 0.673052 0.402022 0.578538 11.00000 -1.50000
AFIX 0
C2 1 0.404809 0.189936 0.376452 11.00000 0.02360 0.04094 =
0.01855 -0.00073 0.00552 0.00093
C1 1 0.443555 0.218479 0.424136 11.00000 0.02366 0.03926 =
0.01692 -0.00164 0.00481 0.00016
C36 1 0.572215 0.467738 0.310410 11.00000 0.05996 0.03545 =
0.03627 0.00673 -0.00752 -0.00259
H36A 2 0.610834 0.455017 0.317496 11.00000 -1.50000
H36B 2 0.571403 0.515317 0.286452 11.00000 -1.50000
H36C 2 0.556117 0.440875 0.285068 11.00000 -1.50000
C41 1 0.602568 0.383781 0.665768 11.00000 0.04662 0.04841 =
0.02266 -0.00322 -0.00571 0.00808
AFIX 137
H41A 2 0.601723 0.428257 0.646212 11.00000 -1.50000
H41B 2 0.623697 0.382070 0.713268 11.00000 -1.50000
H41C 2 0.570080 0.370452 0.673746 11.00000 -1.50000
AFIX 0
C22 1 0.633403 0.026509 0.332616 11.00000 0.04744 0.05933 =
0.02552 -0.00036 0.00838 0.01051
AFIX 137
H22A 2 0.610620 -0.008819 0.337707 11.00000 -1.50000
H22B 2 0.661182 0.009470 0.310944 11.00000 -1.50000
H22C 2 0.617707 0.060299 0.299921 11.00000 -1.50000
AFIX 0
C14 1 0.436082 0.277567 0.649950 11.00000 0.05022 0.06038 =
0.02167 -0.01143 0.00901 0.00137
AFIX 137
H14A 2 0.445489 0.316464 0.624012 11.00000 -1.50000
H14B 2 0.461772 0.245113 0.652002 11.00000 -1.50000
H14C 2 0.430517 0.289149 0.700818 11.00000 -1.50000
AFIX 0
C9 1 0.302894 0.190687 0.287144 11.00000 0.02744 0.06356 =
0.03688 -0.00580 -0.00011 -0.00658
AFIX 137
H9A 2 0.298161 0.236655 0.298431 11.00000 -1.50000
H9B 2 0.273247 0.172976 0.260174 11.00000 -1.50000
H9C 2 0.329010 0.186539 0.256159 11.00000 -1.50000
AFIX 0
C38 1 0.582117 0.526757 0.430819 11.00000 0.07481 0.03313 =
0.04865 -0.00224 -0.02097 0.00369
AFIX 137
H38A 2 0.569796 0.533273 0.478721 11.00000 -1.50000
H38B 2 0.579632 0.567514 0.402499 11.00000 -1.50000
H38C 2 0.615827 0.513224 0.439794 11.00000 -1.50000
AFIX 0
C12 1 0.350529 0.299794 0.607648 11.00000 0.04595 0.10813 =
0.05027 -0.03871 0.00697 0.01717
AFIX 137
H12A 2 0.346699 0.311514 0.659187 11.00000 -1.50000
H12B 2 0.320303 0.281833 0.582919 11.00000 -1.50000
H12C 2 0.359089 0.338592 0.580726 11.00000 -1.50000
AFIX 0
C13 1 0.376704 0.187299 0.649083 11.00000 0.08046 0.08401 =
0.02983 -0.00920 0.02615 -0.02219
AFIX 137
H13A 2 0.402276 0.154958 0.648362 11.00000 -1.50000
H13B 2 0.346487 0.169518 0.624098 11.00000 -1.50000
H13C 2 0.372948 0.198096 0.700907 11.00000 -1.50000
AFIX 0
C23 1 0.687755 0.108810 0.403897 11.00000 0.02488 0.06688 =
0.04022 0.01592 0.00110 0.00165
AFIX 137
H23A 2 0.673248 0.144605 0.373096 11.00000 -1.50000
H23B 2 0.714789 0.090850 0.381081 11.00000 -1.50000
H23C 2 0.699265 0.125015 0.454007 11.00000 -1.50000
AFIX 0
C5 1 0.395962 0.231242 0.526828 11.00000 0.03495 0.04848 =
0.02193 -0.00611 0.01029 0.00189
C10 1 0.271729 0.152176 0.402554 11.00000 0.02863 0.08324 =
0.04729 -0.01695 0.01345 -0.01365
AFIX 137
H10A 2 0.279033 0.126928 0.448615 11.00000 -1.50000
H10B 2 0.244577 0.132279 0.371194 11.00000 -1.50000
H10C 2 0.263429 0.196803 0.414946 11.00000 -1.50000
AFIX 0
C11 1 0.389973 0.249426 0.607823 11.00000 0.04325 0.06186 =
0.02618 -0.01098 0.01422 -0.00256
C42 1 0.623271 0.268861 0.642281 11.00000 0.05865 0.04403 =
0.02843 0.00078 -0.01724 0.00560
AFIX 137
H42A 2 0.591154 0.256653 0.653314 11.00000 -1.50000
H42B 2 0.645790 0.267812 0.688383 11.00000 -1.50000
H42C 2 0.633857 0.238160 0.606187 11.00000 -1.50000
AFIX 0
C37 1 0.500443 0.497785 0.374882 11.00000 0.05827 0.04070 =
0.04521 -0.00990 -0.01728 0.01962
H37A 2 0.478527 0.465823 0.351915 11.00000 -1.50000
H37B 2 0.498069 0.538658 0.342111 11.00000 -1.50000
H37C 2 0.482428 0.502373 0.419158 11.00000 -1.50000
C24 1 0.674519 0.000432 0.457710 11.00000 0.04658 0.05633 =
0.03380 0.01006 0.00675 0.01885
AFIX 137
H24A 2 0.686582 0.017433 0.507242 11.00000 -1.50000
H24B 2 0.701350 -0.016966 0.433946 11.00000 -1.50000
H24C 2 0.651210 -0.034250 0.462751 11.00000 -1.50000
AFIX 0
C8 1 0.326313 0.082513 0.341960 11.00000 0.05030 0.04915 =
0.03949 -0.00427 0.01771 -0.01485
AFIX 137
H8A 2 0.354018 0.080769 0.313946 11.00000 -1.50000
H8B 2 0.298246 0.063619 0.311798 11.00000 -1.50000
H8C 2 0.333431 0.057816 0.388454 11.00000 -1.50000
AFIX 0
C6 1 0.438251 0.239621 0.497242 11.00000 0.02788 0.04359 =
0.01971 -0.00310 0.00463 0.00152
AFIX 43
H6 2 0.464547 0.260067 0.526485 11.00000 -1.20000
AFIX 0
C4 1 0.357593 0.203286 0.480276 11.00000 0.02881 0.04890 =
0.03219 -0.00651 0.01428 -0.00208
AFIX 43
H4 2 0.328026 0.197618 0.499955 11.00000 -1.20000
AFIX 0
PART 1
K1A 3 0.619876 0.287487 0.318481 21.00000 0.02971 0.04488 =
0.05118 0.00484 0.00132 -0.01112
SI2A 8 0.687437 0.394796 0.190526 21.00000 0.03696 0.04622 =
0.05095 0.01861 0.00575 0.00229
SI1A 8 0.733788 0.370700 0.351548 21.00000 0.02754 0.03540 =
0.05374 0.00605 -0.00437 -0.00153
O4A 6 0.694605 0.362527 0.276100 21.00000 0.03137 0.03948 =
0.03565 0.01150 0.00086 -0.00793
C26 1 0.541106 -0.020577 0.614671 31.00000 0.05436 0.04652 =
0.03289 0.01014 0.00464 -0.01053
AFIX 137
H26A 2 0.515442 -0.034900 0.576287 31.00000 -1.50000
H26B 2 0.535307 -0.037967 0.663282 31.00000 -1.50000
H26C 2 0.572076 -0.036460 0.602346 31.00000 -1.50000
AFIX 0
C27 1 0.497743 0.079805 0.639550 31.00000 0.12356 0.09417 =
0.04490 0.03643 0.04243 0.06239
AFIX 137
H27A 2 0.502078 0.125952 0.652077 31.00000 -1.50000
H27B 2 0.489344 0.056047 0.683144 31.00000 -1.50000
H27C 2 0.471901 0.074963 0.598064 31.00000 -1.50000
AFIX 0
C28 1 0.584374 0.073542 0.677154 31.00000 0.11069 0.04821 =
0.01898 0.00716 -0.00118 -0.00988
AFIX 137
H28A 2 0.614325 0.055716 0.662996 31.00000 -1.50000
H28B 2 0.578988 0.056271 0.726009 31.00000 -1.50000
H28C 2 0.586651 0.121034 0.679847 31.00000 -1.50000
AFIX 0
C43 1 0.732616 0.292923 0.404549 21.00000 0.05272 0.04390 =
0.05292 0.00942 -0.01349 -0.00354
AFIX 137
H43A 2 0.701899 0.289011 0.424675 21.00000 -1.50000
H43B 2 0.758951 0.292649 0.445707 21.00000 -1.50000
H43C 2 0.736384 0.256279 0.371090 21.00000 -1.50000
AFIX 0
C44 1 0.712106 0.437747 0.407917 21.00000 0.04650 0.04164 =
0.06129 -0.01011 -0.00837 0.01401
AFIX 137
H44A 2 0.714993 0.479212 0.382136 21.00000 -1.50000
H44B 2 0.731512 0.439170 0.456968 21.00000 -1.50000
H44C 2 0.678396 0.430161 0.414328 21.00000 -1.50000
AFIX 0
C48 1 0.625597 0.372449 0.147987 21.00000 0.04472 0.07373 =
0.04099 0.00722 -0.00252 0.00045
H48A 2 0.618547 0.327790 0.134233 21.00000 -1.50000
H48B 2 0.614627 0.393193 0.101178 21.00000 -1.50000
H48C 2 0.599652 0.387765 0.172301 21.00000 -1.50000
C45 1 0.795002 0.386136 0.328189 21.00000 0.02970 0.05990 =
0.08014 0.00823 -0.00387 -0.00351
AFIX 137
H45A 2 0.804538 0.350735 0.296840 21.00000 -1.50000
H45B 2 0.817493 0.388503 0.374251 21.00000 -1.50000
H45C 2 0.795448 0.427359 0.301085 21.00000 -1.50000
AFIX 0
C47 1 0.732046 0.361416 0.131679 0.73750 0.05467 0.07433 =
0.06348 0.02639 0.02466 0.00158
AFIX 137
H47A 2 0.764645 0.371135 0.155254 21.00000 -1.50000
H47B 2 0.726921 0.381396 0.082035 21.00000 -1.50000
H47C 2 0.727936 0.314235 0.126931 21.00000 -1.50000
AFIX 0
C46 1 0.695296 0.483979 0.199060 0.71765 0.05978 0.04640 =
0.08190 0.03026 -0.00679 -0.00298
AFIX 137
H46A 2 0.671908 0.501654 0.229706 21.00000 -1.50000
H46B 2 0.690256 0.503767 0.149310 21.00000 -1.50000
H46C 2 0.727883 0.493704 0.222681 21.00000 -1.50000
AFIX 0
PART 0
PART 2
K1B 3 0.599188 0.317232 0.201613 -21.00000 0.03352 0.05069 =
0.05668 -0.00184 0.00300 -0.00872
SI1B 8 0.701415 0.356496 0.342912 -21.00000 0.03215 0.04712 =
0.05052 -0.00322 -0.00426 -0.00349
SI2B 8 0.707770 0.410053 0.182835 -21.00000 0.06450 0.07693 =
0.07657 0.03754 0.02168 -0.00652
O4B 6 0.688762 0.371448 0.251428 -21.00000 0.06721 0.05691 =
0.01676 0.01191 -0.00284 -0.01862
C28B 1 0.555885 0.107028 0.679028 -31.00000 0.06803 0.10354 =
0.01630 0.00123 0.00715 -0.04794
AFIX 137
H28D 2 0.590850 0.112449 0.686396 -31.00000 -1.50000
H28E 2 0.544902 0.093485 0.726097 -31.00000 -1.50000
H28F 2 0.540663 0.148368 0.662788 -31.00000 -1.50000
AFIX 0
C27B 1 0.486718 0.046444 0.616870 -31.00000 0.02931 0.08217 =
0.02979 0.01734 0.01726 -0.00510
AFIX 137
H27D 2 0.471545 0.089395 0.612122 -31.00000 -1.50000
H27E 2 0.479901 0.025956 0.663407 -31.00000 -1.50000
H27F 2 0.473911 0.019269 0.574397 -31.00000 -1.50000
AFIX 0
C26B 1 0.564283 -0.008185 0.640363 -31.00000 0.08434 0.08913 =
0.05040 0.03487 0.03666 0.01447
AFIX 137
H26D 2 0.558939 -0.038929 0.598681 -31.00000 -1.50000
H26E 2 0.550105 -0.025483 0.683205 -31.00000 -1.50000
H26F 2 0.598858 -0.001865 0.654261 -31.00000 -1.50000
AFIX 0
C1AA 1 0.761177 0.316994 0.359517 -21.00000 0.05889 0.08433 =
0.06714 0.00040 -0.01573 0.02058
AFIX 137
H1AA 2 0.761380 0.278293 0.327909 -21.00000 -1.50000
H1AB 2 0.767890 0.304310 0.412121 -21.00000 -1.50000
H1AC 2 0.785848 0.347499 0.347297 -21.00000 -1.50000
AFIX 0
C0AA 1 0.707754 0.431362 0.393774 -21.00000 0.12895 0.22726 =
0.11713 0.08505 -0.01406 -0.09974
AFIX 137
H0AA 2 0.738950 0.450915 0.388237 -21.00000 -1.50000
H0AB 2 0.705766 0.422911 0.446725 -21.00000 -1.50000
H0AC 2 0.682016 0.461237 0.374197 -21.00000 -1.50000
AFIX 0
C4AA 1 0.662183 0.404644 0.104295 -21.00000 0.16042
AFIX 137
H4AA 2 0.677133 0.405507 0.058077 -21.00000 -1.50000
H4AB 2 0.640126 0.441516 0.104856 -21.00000 -1.50000
H4AC 2 0.644332 0.363948 0.106953 -21.00000 -1.50000
AFIX 0
C47A 1 0.752541 0.374634 0.156069 -21.00000 0.14062
AFIX 137
H47D 2 0.779429 0.375440 0.196336 -21.00000 -1.50000
H47E 2 0.761841 0.397027 0.112168 -21.00000 -1.50000
H47F 2 0.744123 0.329463 0.143100 -21.00000 -1.50000
AFIX 0
C46A 1 0.719979 0.497147 0.211653 -21.00000 0.15635 0.02008 =
0.14204 0.02257 -0.03500 -0.01012
AFIX 137
H46D 2 0.693889 0.513187 0.238078 -21.00000 -1.50000
H46E 2 0.721976 0.523823 0.167172 -21.00000 -1.50000
H46F 2 0.750420 0.499705 0.244689 -21.00000 -1.50000
AFIX 0
C2AA 1 0.652219 0.301918 0.374715 -21.00000 0.06768 0.09242 =
0.04874 0.00629 0.01698 0.01589
AFIX 137
H2AA 2 0.621607 0.325421 0.368988 -21.00000 -1.50000
H2AB 2 0.660916 0.290070 0.427256 -21.00000 -1.50000
H2AC 2 0.649057 0.262440 0.344113 -21.00000 -1.50000
AFIX 0
HKLF 4
REM v18433 in C2/c
REM wR2 = 0.1755, GooF = S = 1.101, Restrained GooF = 1.101 for all data
REM R1 = 0.0562 for 10488 Fo > 4sig(Fo) and 0.0850 for all 14000 data
REM 696 parameters refined using 0 restraints
END
WGHT 0.0823 29.1784
REM Highest difference peak 1.015, deepest hole -0.550, 1-sigma level 0.098
Q1 1 0.5370 0.1512 0.2426 11.00000 0.05 0.95
Q2 1 0.5947 0.2926 0.2642 11.00000 0.05 0.89
Q3 1 0.5000 -0.0793 0.7500 10.50000 0.05 0.86
Q4 1 0.5460 0.1430 0.2576 11.00000 0.05 0.82
Q5 1 0.5289 0.1009 0.6248 11.00000 0.05 0.72
Q6 1 0.3117 0.1515 0.3031 11.00000 0.05 0.72
Q7 1 0.5210 0.1923 0.4205 11.00000 0.05 0.70
Q8 1 0.5771 0.2094 0.2625 11.00000 0.05 0.65
Q9 1 0.3579 0.2274 0.6352 11.00000 0.05 0.63
Q10 1 0.5166 0.2614 0.4152 11.00000 0.05 0.61
;
_shelx_res_checksum 4122
#######################################################################
#
# This file contains crystal structure data downloaded from the
# Cambridge Structural Database (CSD) hosted by the Cambridge
# Crystallographic Data Centre (CCDC).
#
# Full information about CCDC data access policies and citation
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1
#
# Audit and citation data items may have been added by the CCDC.
# Please retain this information to preserve the provenance of
# this file and to allow appropriate attribution of the data.
#
#######################################################################
data_d19106
_database_code_depnum_ccdc_archive 'CCDC 1985598'
loop_
_audit_author_name
_audit_author_address
'Manar Shoshani'
;California Institute of Technology
United States of America
;
_audit_update_record
;
2020-07-16 deposited with the CCDC. 2020-07-20 downloaded from the CCDC.
;
_audit_creation_method SHELXL-2018/3
_vrf_PLAT213_d19106
;
PROBLEM: Atom C2 has ADP max/min Ratio ..... 5.3 prolat
RESPONSE: Disordered t-butyl group bears a disordered
C centre, the elongated elipsoid accurately describes
the electron density present
;
_vrf_PLAT214_d19106
;
PROBLEM: Atom C18 (Anion/Solvent) ADP max/min Ratio 5.6 prolat
RESPONSE: ...
;
_vrf_PLAT220_d19106
;
PROBLEM: NonSolvent Resd 1 C Ueq(max) / Ueq(min) Range 8.5 Ratio
RESPONSE: ...
;
# end Validation Reply Form
_shelx_SHELXL_version_number 2018/3
_chemical_name_systematic ?
_chemical_name_common ?
_chemical_melting_point ?
_chemical_formula_moiety ?
_chemical_formula_sum 'C112.83 H176.50 Fe N2 Ni3 O7.47 P2 Si2.94'
_chemical_formula_weight 2057.28
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 21/c'
_space_group_name_Hall '-P 2ybc'
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
_cell_length_a 25.101(9)
_cell_length_b 30.772(12)
_cell_length_c 18.538(7)
_cell_angle_alpha 90
_cell_angle_beta 100.85(3)
_cell_angle_gamma 90
_cell_volume 14063(9)
_cell_formula_units_Z 4
_cell_measurement_temperature 100(2)
_cell_measurement_reflns_used 9930
_cell_measurement_theta_min 2.26
_cell_measurement_theta_max 27.11
_exptl_crystal_description Block
_exptl_crystal_colour Brown
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_density_diffrn 0.972
_exptl_crystal_F_000 4434
_exptl_transmission_factor_min ?
_exptl_transmission_factor_max ?
_exptl_crystal_size_max 0.2
_exptl_crystal_size_mid 0.15
_exptl_crystal_size_min 0.15
_exptl_absorpt_coefficient_mu 0.587
_shelx_estimated_absorpt_T_min ?
_shelx_estimated_absorpt_T_max ?
_exptl_absorpt_correction_type ?
_exptl_absorpt_correction_T_min ?
_exptl_absorpt_correction_T_max ?
_exptl_absorpt_process_details ?
_exptl_absorpt_special_details ?
_diffrn_ambient_temperature 100(2)
_diffrn_radiation_wavelength 0.71073
_diffrn_radiation_type MoK\a
_diffrn_source ?
_diffrn_measurement_device_type 'Bruker APEX-II CCD'
_diffrn_measurement_method ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number 164629
_diffrn_reflns_av_unetI/netI 0.0987
_diffrn_reflns_av_R_equivalents 0.0887
_diffrn_reflns_limit_h_min -24
_diffrn_reflns_limit_h_max 31
_diffrn_reflns_limit_k_min -36
_diffrn_reflns_limit_k_max 39
_diffrn_reflns_limit_l_min -19
_diffrn_reflns_limit_l_max 21
_diffrn_reflns_theta_min 1.560
_diffrn_reflns_theta_max 27.573
_diffrn_reflns_theta_full 25.242
_diffrn_measured_fraction_theta_max 0.824
_diffrn_measured_fraction_theta_full 0.973
_diffrn_reflns_Laue_measured_fraction_max 0.824
_diffrn_reflns_Laue_measured_fraction_full 0.973
_diffrn_reflns_point_group_measured_fraction_max 0.824
_diffrn_reflns_point_group_measured_fraction_full 0.973
_reflns_number_total 26796
_reflns_number_gt 19089
_reflns_threshold_expression 'I > 2\s(I)'
_reflns_Friedel_coverage 0.000
_reflns_Friedel_fraction_max .
_reflns_Friedel_fraction_full .
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
Structure factors included contributions from the .fab file.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_computing_data_collection 'APEX2 v2014.11-0 (Bruker-AXS, 2014)'
_computing_cell_refinement 'SAINT V8.38A (?, 2016)'
_computing_data_reduction 'SAINT V8.38A (?, 2016)'
_computing_structure_solution 'XS (Sheldrick, 2008)'
_computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)'
_refine_special_details ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type full
_refine_ls_weighting_scheme calc
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0153P)^2^+301.7568P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary ?
_atom_sites_solution_secondary ?
_atom_sites_solution_hydrogens geom
_refine_ls_hydrogen_treatment constr
_refine_ls_extinction_method none
_refine_ls_extinction_coef .
_refine_ls_number_reflns 26796
_refine_ls_number_parameters 1313
_refine_ls_number_restraints 75
_refine_ls_R_factor_all 0.1714
_refine_ls_R_factor_gt 0.1338
_refine_ls_wR_factor_ref 0.2968
_refine_ls_wR_factor_gt 0.2779
_refine_ls_goodness_of_fit_ref 1.015
_refine_ls_restrained_S_all 1.014
_refine_ls_shift/su_max 0.004
_refine_ls_shift/su_mean 0.000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni3 Ni 0.20602(4) 0.62388(3) 0.52206(5) 0.0177(2) Uani 1 1 d . . . . .
Ni2 Ni 0.25323(4) 0.54751(3) 0.51946(6) 0.0212(2) Uani 1 1 d . . . . .
Ni1 Ni 0.30637(4) 0.62247(3) 0.54135(5) 0.0179(2) Uani 1 1 d . . . . .
Fe04 Fe 0.000000 0.500000 0.500000 0.0351(5) Uani 1 2 d S . P . .
Fe05 Fe 0.500000 0.500000 0.500000 0.0414(5) Uani 1 2 d S . P . .
P2 P 0.24911(8) 0.60415(6) 0.37945(11) 0.0174(4) Uani 1 1 d . . . . .
P1 P 0.26006(9) 0.58779(7) 0.67421(12) 0.0211(5) Uani 1 1 d . . . . .
Si2 Si 0.09869(19) 0.41068(17) 0.0563(3) 0.0594(15) Uani 0.751(8) 1 d . . P . .
Si1 Si 0.0303(2) 0.38170(16) 0.1702(3) 0.0607(16) Uani 0.751(8) 1 d . . P . .
O1 O 0.3572(2) 0.63584(18) 0.6266(3) 0.0223(13) Uani 1 1 d . . . . .
O3 O 0.1635(2) 0.64117(16) 0.5903(3) 0.0212(12) Uani 1 1 d . . . . .
O4 O 0.3481(2) 0.64905(18) 0.4811(3) 0.0221(12) Uani 1 1 d . . . . .
O5 O 0.2468(3) 0.50907(18) 0.4388(3) 0.0280(14) Uani 1 1 d . . . . .
O6 O 0.1586(2) 0.64970(18) 0.4448(3) 0.0221(12) Uani 1 1 d . . . . .
O2 O 0.2571(3) 0.50151(18) 0.5876(3) 0.0305(14) Uani 1 1 d . . . . .
N2 N 0.2537(3) 0.5993(2) 0.4678(4) 0.0188(14) Uani 1 1 d . . . . .
Si4 Si -0.1188(2) 0.75026(18) 0.4610(4) 0.080(2) Uani 0.718(8) 1 d . . P . .
N1 N 0.2579(3) 0.5925(2) 0.5872(4) 0.0219(15) Uani 1 1 d . . . . .
C43 C 0.2888(3) 0.6492(2) 0.3616(4) 0.0163(16) Uani 1 1 d . . . . .
C46 C 0.3516(3) 0.7133(3) 0.3174(4) 0.0200(17) Uani 1 1 d . . . . .
H46 H 0.373946 0.734824 0.301669 0.024 Uiso 1 1 calc R U . . .
C45 C 0.3652(3) 0.6989(3) 0.3889(4) 0.0197(17) Uani 1 1 d . . . . .
C2 C 0.3675(3) 0.6164(3) 0.6899(4) 0.0224(18) Uani 1 1 d . . . . .
C44 C 0.3336(3) 0.6649(2) 0.4131(4) 0.0153(16) Uani 1 1 d . . . . .
C59 C 0.0946(3) 0.6509(2) 0.3322(4) 0.0205(17) Uani 1 1 d . . . . .
Si3 Si -0.1586(3) 0.7633(2) 0.6040(4) 0.103(3) Uani 0.718(8) 1 d . . P . .
C47 C 0.3068(3) 0.6982(3) 0.2661(4) 0.0213(17) Uani 1 1 d . . . . .
C60 C 0.0811(4) 0.6375(3) 0.2608(5) 0.029(2) Uani 1 1 d . . . . .
H60 H 0.046984 0.646693 0.233698 0.035 Uiso 1 1 calc R U . . .
C72 C 0.2615(3) 0.5142(2) 0.3759(5) 0.0222(18) Uani 1 1 d . . . . .
C32 C 0.1662(3) 0.6906(3) 0.7679(5) 0.0219(18) Uani 1 1 d . . . . .
H32 H 0.144804 0.710208 0.789989 0.026 Uiso 1 1 calc R U . . .
C48 C 0.2748(3) 0.6671(3) 0.2894(5) 0.0222(18) Uani 1 1 d . . . . .
H48 H 0.242930 0.657469 0.257267 0.027 Uiso 1 1 calc R U . . .
C29 C 0.2252(3) 0.6319(2) 0.7070(4) 0.0163(16) Uani 1 1 d . . . . .
C58 C 0.1444(4) 0.6380(3) 0.3748(4) 0.0241(19) Uani 1 1 d . . . . .
C62 C 0.1625(3) 0.5996(3) 0.2640(4) 0.0230(18) Uani 1 1 d . . . . .
H62 H 0.185750 0.581901 0.241525 0.028 Uiso 1 1 calc R U . . .
C71 C 0.2719(3) 0.5549(2) 0.3450(4) 0.0191(17) Uani 1 1 d . . . . .
C30 C 0.1800(3) 0.6506(2) 0.6611(4) 0.0207(17) Uani 1 1 d . . . . .
C15 C 0.2312(3) 0.5366(3) 0.6918(5) 0.0234(18) Uani 1 1 d . . . . .
C53 C 0.2951(3) 0.7161(3) 0.1882(4) 0.0214(18) Uani 1 1 d . . . . .
C63 C 0.0565(3) 0.6804(3) 0.3656(4) 0.0213(17) Uani 1 1 d . . . . .
C34 C 0.2402(3) 0.6423(3) 0.7811(4) 0.0203(17) Uani 1 1 d . . . . .
H34 H 0.270785 0.628325 0.809708 0.024 Uiso 1 1 calc R U . . .
C31 C 0.1502(3) 0.6823(3) 0.6948(4) 0.0229(18) Uani 1 1 d . . . . .
C76 C 0.2932(3) 0.5575(3) 0.2790(5) 0.0251(19) Uani 1 1 d . . . . .
H76 H 0.301583 0.585125 0.261188 0.030 Uiso 1 1 calc R U . . .
C57 C 0.1796(3) 0.6129(2) 0.3380(4) 0.0174(16) Uani 1 1 d . . . . .
C33 C 0.2123(3) 0.6722(3) 0.8136(4) 0.0214(18) Uani 1 1 d . . . . .
C54 C 0.2881(4) 0.7659(3) 0.1886(5) 0.028(2) Uani 1 1 d . . . . .
H54A H 0.254948 0.773149 0.206688 0.042 Uiso 1 1 calc R U . . .
H54B H 0.285446 0.777109 0.138540 0.042 Uiso 1 1 calc R U . . .
H54C H 0.319424 0.779014 0.220688 0.042 Uiso 1 1 calc R U . . .
C61 C 0.1131(4) 0.6116(3) 0.2244(4) 0.027(2) Uani 1 1 d . . . . .
C6 C 0.3451(4) 0.5656(4) 0.7833(5) 0.042(3) Uani 1 1 d . . . . .
H6 H 0.319784 0.546383 0.798600 0.051 Uiso 1 1 calc R U . . .
C64 C 0.0850(3) 0.7235(3) 0.3888(5) 0.0260(19) Uani 1 1 d . . . . .
H64A H 0.117475 0.718071 0.426194 0.039 Uiso 1 1 calc R U . . .
H64B H 0.060313 0.742666 0.408968 0.039 Uiso 1 1 calc R U . . .
H64C H 0.095508 0.737360 0.345939 0.039 Uiso 1 1 calc R U . . .
C3 C 0.4195(3) 0.6216(3) 0.7374(5) 0.031(2) Uani 1 1 d . . . . .
C49 C 0.4139(3) 0.7193(3) 0.4414(4) 0.028(2) Uani 1 1 d . . . . .
C42 C 0.2365(4) 0.7336(3) 0.9032(5) 0.032(2) Uani 1 1 d . . . . .
H42A H 0.267470 0.741353 0.880606 0.048 Uiso 1 1 calc R U . . .
H42B H 0.244272 0.741500 0.955318 0.048 Uiso 1 1 calc R U . . .
H42C H 0.204192 0.749348 0.878456 0.048 Uiso 1 1 calc R U . . .
C19 C 0.1918(4) 0.4955(3) 0.7801(5) 0.035(2) Uani 1 1 d . . . . .
C16 C 0.2392(4) 0.4995(3) 0.6497(5) 0.032(2) Uani 1 1 d . . . . .
C39 C 0.2261(4) 0.6841(3) 0.8955(4) 0.027(2) Uani 1 1 d . . . . .
C35 C 0.1008(3) 0.7046(3) 0.6492(5) 0.0253(19) Uani 1 1 d . . . . .
C75 C 0.3017(4) 0.5207(3) 0.2409(5) 0.032(2) Uani 1 1 d . . . . .
C20 C 0.2068(4) 0.5346(3) 0.7539(5) 0.030(2) Uani 1 1 d . . . . .
H20 H 0.200506 0.560751 0.778285 0.037 Uiso 1 1 calc R U . . .
C65 C 0.0389(4) 0.6583(3) 0.4323(5) 0.031(2) Uani 1 1 d . . . . .
H65A H 0.017508 0.632343 0.415930 0.047 Uiso 1 1 calc R U . . .
H65B H 0.016978 0.678642 0.455105 0.047 Uiso 1 1 calc R U . . .
H65C H 0.071202 0.650051 0.468214 0.047 Uiso 1 1 calc R U . . .
C81 C 0.3242(4) 0.5238(3) 0.1684(5) 0.032(2) Uani 1 1 d . . . . .
C37 C 0.1158(3) 0.7286(3) 0.5832(4) 0.0249(19) Uani 1 1 d . . . . .
H37A H 0.149497 0.744884 0.599102 0.037 Uiso 1 1 calc R U . . .
H37B H 0.086553 0.748784 0.562959 0.037 Uiso 1 1 calc R U . . .
H37C H 0.120773 0.707503 0.545488 0.037 Uiso 1 1 calc R U . . .
C7 C 0.4603(3) 0.6539(3) 0.7173(5) 0.033(2) Uani 1 1 d . . . . .
C55 C 0.3421(4) 0.7045(3) 0.1497(5) 0.031(2) Uani 1 1 d . . . . .
H55A H 0.375882 0.716676 0.177411 0.047 Uiso 1 1 calc R U . . .
H55B H 0.335069 0.716622 0.099879 0.047 Uiso 1 1 calc R U . . .
H55C H 0.345333 0.672848 0.147060 0.047 Uiso 1 1 calc R U . . .
C40 C 0.2753(4) 0.6603(3) 0.9349(5) 0.041(3) Uani 1 1 d . . . . .
H40A H 0.267948 0.629034 0.933608 0.061 Uiso 1 1 calc R U . . .
H40B H 0.283925 0.670167 0.986042 0.061 Uiso 1 1 calc R U . . .
H40C H 0.306020 0.666312 0.910755 0.061 Uiso 1 1 calc R U . . .
C73 C 0.2685(4) 0.4764(3) 0.3318(5) 0.030(2) Uani 1 1 d . . . . .
C74 C 0.2884(4) 0.4815(3) 0.2685(5) 0.030(2) Uani 1 1 d . . . . .
H74 H 0.293419 0.456083 0.241499 0.036 Uiso 1 1 calc R U . . .
C36 C 0.0556(3) 0.6716(3) 0.6243(5) 0.032(2) Uani 1 1 d . . . . .
H36A H 0.068772 0.648907 0.594925 0.047 Uiso 1 1 calc R U . . .
H36B H 0.024402 0.686290 0.594586 0.047 Uiso 1 1 calc R U . . .
H36C H 0.044774 0.658427 0.667447 0.047 Uiso 1 1 calc R U . . .
C25 C 0.1658(5) 0.4914(3) 0.8468(6) 0.050(3) Uani 1 1 d . . . . .
C56 C 0.2427(4) 0.6964(3) 0.1434(5) 0.032(2) Uani 1 1 d . . . . .
H56A H 0.247570 0.665041 0.137929 0.048 Uiso 1 1 calc R U . . .
H56B H 0.234774 0.709992 0.094729 0.048 Uiso 1 1 calc R U . . .
H56C H 0.212550 0.701615 0.168972 0.048 Uiso 1 1 calc R U . . .
C98 C 0.0698(4) 0.5376(3) 0.4911(7) 0.043(3) Uani 1 1 d . . . . .
C41 C 0.1771(4) 0.6722(3) 0.9318(5) 0.034(2) Uani 1 1 d . . . . .
H41A H 0.144623 0.687318 0.906196 0.050 Uiso 1 1 calc R U . . .
H41B H 0.184758 0.681113 0.983488 0.050 Uiso 1 1 calc R U . . .
H41C H 0.171033 0.640767 0.928670 0.050 Uiso 1 1 calc R U . . .
C4 C 0.4303(4) 0.5999(4) 0.8022(5) 0.048(3) Uani 1 1 d . . . . .
H4 H 0.464202 0.605365 0.833420 0.057 Uiso 1 1 calc R U . . .
C52 C 0.4394(4) 0.7571(3) 0.4067(5) 0.038(2) Uani 1 1 d . . . . .
H52A H 0.456253 0.746175 0.366681 0.057 Uiso 1 1 calc R U . . .
H52B H 0.466982 0.771039 0.443881 0.057 Uiso 1 1 calc R U . . .
H52C H 0.411221 0.778312 0.387148 0.057 Uiso 1 1 calc R U . . .
C77 C 0.2519(4) 0.4309(3) 0.3565(5) 0.037(2) Uani 1 1 d . . . . .
C95 C -0.0084(4) 0.5647(3) 0.5216(6) 0.037(2) Uani 1 1 d . . . . .
C9 C 0.4364(4) 0.6992(3) 0.7048(6) 0.043(3) Uani 1 1 d . . . . .
H9A H 0.405997 0.698691 0.662987 0.065 Uiso 1 1 calc R U . . .
H9B H 0.464234 0.719341 0.694557 0.065 Uiso 1 1 calc R U . . .
H9C H 0.423384 0.708754 0.748895 0.065 Uiso 1 1 calc R U . . .
C50 C 0.4586(4) 0.6847(3) 0.4641(5) 0.036(2) Uani 1 1 d . . . . .
H50A H 0.444145 0.660709 0.489283 0.053 Uiso 1 1 calc R U . . .
H50B H 0.489478 0.697867 0.497139 0.053 Uiso 1 1 calc R U . . .
H50C H 0.470577 0.673667 0.420165 0.053 Uiso 1 1 calc R U . . .
C66 C 0.0034(4) 0.6908(3) 0.3113(5) 0.035(2) Uani 1 1 d . . . . .
H66A H 0.011968 0.704814 0.267440 0.052 Uiso 1 1 calc R U . . .
H66B H -0.018945 0.710449 0.334891 0.052 Uiso 1 1 calc R U . . .
H66C H -0.016645 0.663844 0.297291 0.052 Uiso 1 1 calc R U . . .
C97 C 0.0295(4) 0.5412(3) 0.4254(6) 0.043(3) Uani 1 1 d . . . . .
C38 C 0.0753(4) 0.7389(3) 0.6922(5) 0.036(2) Uani 1 1 d . . . . .
H38A H 0.055856 0.724347 0.726619 0.055 Uiso 1 1 calc R U . . .
H38B H 0.049844 0.756701 0.657976 0.055 Uiso 1 1 calc R U . . .
H38C H 0.103841 0.757407 0.719642 0.055 Uiso 1 1 calc R U . . .
C27 C 0.1107(6) 0.4696(4) 0.8250(7) 0.061(4) Uani 1 1 d . . . . .
H27A H 0.088897 0.485603 0.784125 0.091 Uiso 1 1 calc R U . . .
H27B H 0.092136 0.469654 0.867003 0.091 Uiso 1 1 calc R U . . .
H27C H 0.115679 0.439620 0.809864 0.091 Uiso 1 1 calc R U . . .
C67 C 0.0941(4) 0.5986(3) 0.1443(5) 0.040(2) Uani 1 1 d . . . . .
C17 C 0.2298(5) 0.4586(3) 0.6801(6) 0.042(3) Uani 1 1 d . . . . .
C87 C 0.5264(4) 0.5471(3) 0.5781(6) 0.040(2) Uani 1 1 d . . . . .
C99 C 0.0463(4) 0.5526(3) 0.5513(6) 0.041(2) Uani 1 1 d . . . . .
C89 C 0.4586(4) 0.5592(3) 0.4765(6) 0.041(3) Uani 1 1 d . . . . .
C85 C 0.4362(4) 0.5348(4) 0.5308(6) 0.046(3) Uani 1 1 d . . . . .
C18 C 0.2056(5) 0.4584(3) 0.7427(6) 0.042(3) Uani 1 1 d . . . . .
H18 H 0.197811 0.430901 0.761450 0.050 Uiso 1 1 calc R U . . .
C96 C -0.0191(5) 0.5586(3) 0.4440(6) 0.045(3) Uani 1 1 d . . . . .
C86 C 0.4783(4) 0.5284(4) 0.5926(6) 0.046(3) Uani 1 1 d . . . . .
C8 C 0.4780(4) 0.6376(3) 0.6472(5) 0.037(2) Uani 1 1 d . . . . .
H8A H 0.489840 0.607286 0.653886 0.056 Uiso 1 1 calc R U . . .
H8B H 0.507981 0.655510 0.636999 0.056 Uiso 1 1 calc R U . . .
H8C H 0.447333 0.639565 0.605819 0.056 Uiso 1 1 calc R U . . .
C70 C 0.1364(4) 0.5733(4) 0.1133(6) 0.048(3) Uani 1 1 d . . . . .
H70A H 0.168790 0.591352 0.115008 0.073 Uiso 1 1 calc R U . . .
H70B H 0.121729 0.565247 0.062293 0.073 Uiso 1 1 calc R U . . .
H70C H 0.146097 0.546949 0.142527 0.073 Uiso 1 1 calc R U . . .
C26 C 0.2022(6) 0.4646(4) 0.9060(6) 0.066(4) Uani 1 1 d . . . . .
H26A H 0.204117 0.434580 0.888831 0.099 Uiso 1 1 calc R U . . .
H26B H 0.187162 0.464754 0.951105 0.099 Uiso 1 1 calc R U . . .
H26C H 0.238721 0.477169 0.916011 0.099 Uiso 1 1 calc R U . . .
C79 C 0.2894(4) 0.4181(3) 0.4297(6) 0.040(3) Uani 1 1 d . . . . .
H79A H 0.326888 0.415645 0.421993 0.061 Uiso 1 1 calc R U . . .
H79B H 0.277687 0.390171 0.446647 0.061 Uiso 1 1 calc R U . . .
H79C H 0.287467 0.440475 0.466765 0.061 Uiso 1 1 calc R U . . .
C69 C 0.0804(5) 0.6396(4) 0.0966(5) 0.058(3) Uani 1 1 d . . . . .
H69A H 0.054075 0.657290 0.116510 0.086 Uiso 1 1 calc R U . . .
H69B H 0.064816 0.631004 0.046144 0.086 Uiso 1 1 calc R U . . .
H69C H 0.113497 0.656486 0.096922 0.086 Uiso 1 1 calc R U . . .
C51 C 0.3942(4) 0.7374(3) 0.5094(5) 0.037(2) Uani 1 1 d . . . . .
H51A H 0.364877 0.758357 0.493692 0.055 Uiso 1 1 calc R U . . .
H51B H 0.424337 0.751833 0.541754 0.055 Uiso 1 1 calc R U . . .
H51C H 0.380690 0.713467 0.535902 0.055 Uiso 1 1 calc R U . . .
O8 O -0.1520(4) 0.7681(3) 0.5219(7) 0.057(3) Uani 0.718(8) 1 d . . P . .
C88 C 0.5148(4) 0.5667(4) 0.5049(6) 0.044(3) Uani 1 1 d . . . . .
C104 C 0.0749(4) 0.5545(3) 0.6284(6) 0.048(3) Uani 1 1 d . . . . .
H10S H 0.048740 0.559859 0.660473 0.072 Uiso 1 1 calc R U . . .
H10T H 0.101636 0.578100 0.634113 0.072 Uiso 1 1 calc R U . . .
H10U H 0.093514 0.526840 0.641830 0.072 Uiso 1 1 calc R U . . .
C94 C 0.4272(4) 0.5729(4) 0.4013(6) 0.052(3) Uani 1 1 d . . . . .
H94A H 0.452461 0.576808 0.367464 0.078 Uiso 1 1 calc R U . . .
H94B H 0.408247 0.600315 0.405921 0.078 Uiso 1 1 calc R U . . .
H94C H 0.400687 0.550351 0.382255 0.078 Uiso 1 1 calc R U . . .
C5 C 0.3959(5) 0.5704(4) 0.8268(6) 0.054(3) Uani 1 1 d . . . . .
C92 C 0.5814(4) 0.5502(4) 0.6285(6) 0.051(3) Uani 1 1 d . . . . .
H92A H 0.581275 0.532587 0.672525 0.077 Uiso 1 1 calc R U . . .
H92B H 0.589032 0.580540 0.642720 0.077 Uiso 1 1 calc R U . . .
H92C H 0.609429 0.539351 0.602731 0.077 Uiso 1 1 calc R U . . .
C10 C 0.5120(4) 0.6584(4) 0.7764(6) 0.055(3) Uani 1 1 d . . . . .
H10A H 0.502220 0.667615 0.822794 0.083 Uiso 1 1 calc R U . . .
H10B H 0.536105 0.680022 0.760737 0.083 Uiso 1 1 calc R U . . .
H10C H 0.530660 0.630262 0.783379 0.083 Uiso 1 1 calc R U . . .
C28 C 0.1570(7) 0.5356(4) 0.8804(7) 0.074(5) Uani 1 1 d . . . . .
H28A H 0.191428 0.551492 0.890640 0.111 Uiso 1 1 calc R U . . .
H28B H 0.143563 0.531362 0.926232 0.111 Uiso 1 1 calc R U . . .
H28C H 0.130361 0.552303 0.845824 0.111 Uiso 1 1 calc R U . . .
C78 C 0.1920(4) 0.4322(4) 0.3643(6) 0.046(3) Uani 1 1 d . . . . .
H78A H 0.186172 0.456781 0.395630 0.069 Uiso 1 1 calc R U . . .
H78B H 0.182621 0.405081 0.386647 0.069 Uiso 1 1 calc R U . . .
H78C H 0.168987 0.435663 0.315745 0.069 Uiso 1 1 calc R U . . .
C100 C -0.0488(4) 0.5845(4) 0.5652(7) 0.050(3) Uani 1 1 d . . . . .
H10V H -0.085893 0.579336 0.538900 0.075 Uiso 1 1 calc R U . . .
H10W H -0.042318 0.615790 0.570815 0.075 Uiso 1 1 calc R U . . .
H10X H -0.043843 0.570863 0.613863 0.075 Uiso 1 1 calc R U . . .
C91 C 0.4712(5) 0.5069(4) 0.6642(7) 0.060(3) Uani 1 1 d . . . . .
H91A H 0.444181 0.483703 0.653622 0.090 Uiso 1 1 calc R U . . .
H91B H 0.459061 0.528599 0.696234 0.090 Uiso 1 1 calc R U . . .
H91C H 0.505968 0.494623 0.688679 0.090 Uiso 1 1 calc R U . . .
C93 C 0.5529(5) 0.5928(4) 0.4695(7) 0.058(3) Uani 1 1 d . . . . .
H93A H 0.588586 0.578837 0.478121 0.088 Uiso 1 1 calc R U . . .
H93B H 0.556175 0.622147 0.490506 0.088 Uiso 1 1 calc R U . . .
H93C H 0.538895 0.594663 0.416512 0.088 Uiso 1 1 calc R U . . .
C68 C 0.0436(4) 0.5692(4) 0.1389(6) 0.055(3) Uani 1 1 d . . . . .
H68A H 0.053405 0.542587 0.167222 0.083 Uiso 1 1 calc R U . . .
H68B H 0.029892 0.561799 0.087355 0.083 Uiso 1 1 calc R U . . .
H68C H 0.015403 0.584745 0.158695 0.083 Uiso 1 1 calc R U . . .
C21 C 0.2462(6) 0.4164(3) 0.6461(7) 0.060(4) Uani 1 1 d . . . . .
C103 C 0.1256(5) 0.5218(3) 0.4956(8) 0.064(4) Uani 1 1 d . . . . .
H10Y H 0.143919 0.520659 0.547113 0.096 Uiso 1 1 calc R U . . .
H H 0.145299 0.541501 0.468396 0.096 Uiso 1 1 calc R U . . .
HA H 0.124811 0.492597 0.474149 0.096 Uiso 1 1 calc R U . . .
C23 C 0.2120(5) 0.4094(4) 0.5696(6) 0.054(3) Uani 1 1 d . . . . .
H23A H 0.174018 0.404810 0.573667 0.081 Uiso 1 1 calc R U . . .
H23B H 0.225339 0.383912 0.546858 0.081 Uiso 1 1 calc R U . . .
H23C H 0.214620 0.435119 0.539230 0.081 Uiso 1 1 calc R U . . .
C80 C 0.2585(6) 0.3957(3) 0.3005(6) 0.057(3) Uani 1 1 d . . . . .
H80A H 0.238730 0.404229 0.251876 0.085 Uiso 1 1 calc R U . . .
H80B H 0.243981 0.368136 0.314972 0.085 Uiso 1 1 calc R U . . .
H80C H 0.297073 0.392142 0.298845 0.085 Uiso 1 1 calc R U . . .
C12 C 0.4611(6) 0.5163(6) 0.8913(9) 0.109(7) Uani 1 1 d . . . . .
H12A H 0.451780 0.498136 0.847263 0.164 Uiso 1 1 calc R U . . .
H12B H 0.471085 0.497670 0.934599 0.164 Uiso 1 1 calc R U . . .
H12C H 0.491840 0.535088 0.886665 0.164 Uiso 1 1 calc R U . . .
C90 C 0.3774(4) 0.5217(4) 0.5240(7) 0.059(3) Uani 1 1 d . . . . .
H90A H 0.361479 0.516940 0.472157 0.089 Uiso 1 1 calc R U . . .
H90B H 0.357508 0.544784 0.543864 0.089 Uiso 1 1 calc R U . . .
H90C H 0.375166 0.494777 0.551588 0.089 Uiso 1 1 calc R U . . .
C11 C 0.4123(5) 0.5443(6) 0.8995(7) 0.073(4) Uani 1 1 d . . . . .
C102 C 0.0383(5) 0.5311(4) 0.3496(7) 0.056(3) Uani 1 1 d . . . . .
H10Z H 0.064397 0.507201 0.351784 0.085 Uiso 1 1 calc R U . . .
HB H 0.052477 0.556873 0.328681 0.085 Uiso 1 1 calc R U . . .
HC H 0.003781 0.522515 0.318766 0.085 Uiso 1 1 calc R U . . .
C101 C -0.0681(5) 0.5672(4) 0.3902(7) 0.058(3) Uani 1 1 d . . . . .
H10 H -0.064188 0.554932 0.342664 0.087 Uiso 1 1 calc R U . . .
HD H -0.073790 0.598618 0.385278 0.087 Uiso 1 1 calc R U . . .
HE H -0.099228 0.553749 0.406376 0.087 Uiso 1 1 calc R U . . .
C22 C 0.3064(5) 0.4187(4) 0.6450(7) 0.062(4) Uani 1 1 d . . . . .
H22A H 0.314101 0.445053 0.619127 0.094 Uiso 1 1 calc R U . . .
H22B H 0.317139 0.393104 0.619598 0.094 Uiso 1 1 calc R U . . .
H22C H 0.326928 0.419348 0.695475 0.094 Uiso 1 1 calc R U . . .
C13 C 0.4286(6) 0.5779(6) 0.9618(7) 0.098(6) Uani 1 1 d . . . . .
H13A H 0.459934 0.594632 0.952835 0.148 Uiso 1 1 calc R U . . .
H13B H 0.438085 0.562694 1.008889 0.148 Uiso 1 1 calc R U . . .
H13C H 0.398132 0.597600 0.963036 0.148 Uiso 1 1 calc R U . . .
C108 C 0.0991(7) 0.3809(5) -0.0276(9) 0.058(4) Uani 0.751(8) 1 d . . P . .
H10D H 0.120530 0.354277 -0.016444 0.087 Uiso 0.751(8) 1 calc R U P . .
H10E H 0.115189 0.398933 -0.061474 0.087 Uiso 0.751(8) 1 calc R U P . .
H10F H 0.061832 0.373282 -0.050484 0.087 Uiso 0.751(8) 1 calc R U P . .
C24 C 0.2358(7) 0.3766(4) 0.6918(8) 0.083(5) Uani 1 1 d . . . . .
H24A H 0.258861 0.378394 0.740618 0.124 Uiso 1 1 calc R U . . .
H24B H 0.244356 0.350042 0.667170 0.124 Uiso 1 1 calc R U . . .
H24C H 0.197612 0.376124 0.696653 0.124 Uiso 1 1 calc R U . . .
C109 C 0.0702(9) 0.4650(5) 0.0353(10) 0.080(6) Uani 0.751(8) 1 d . . P . .
H10G H 0.044046 0.464194 -0.011184 0.120 Uiso 0.751(8) 1 calc R U P . .
H10H H 0.099419 0.485418 0.031017 0.120 Uiso 0.751(8) 1 calc R U P . .
H10I H 0.051838 0.474534 0.074767 0.120 Uiso 0.751(8) 1 calc R U P . .
C107 C -0.0350(8) 0.3568(7) 0.1406(10) 0.096(8) Uani 0.751(8) 1 d . . P . .
H10J H -0.056803 0.374799 0.102490 0.144 Uiso 0.751(8) 1 calc R U P . .
H10K H -0.053460 0.354167 0.182459 0.144 Uiso 0.751(8) 1 calc R U P . .
H10L H -0.030172 0.327869 0.120663 0.144 Uiso 0.751(8) 1 calc R U P . .
C116 C -0.0476(8) 0.7720(7) 0.4777(15) 0.095(7) Uani 0.718(8) 1 d . . P . .
H11D H -0.048600 0.803772 0.475382 0.142 Uiso 0.718(8) 1 calc R U P . .
H11E H -0.028611 0.760697 0.440063 0.142 Uiso 0.718(8) 1 calc R U P . .
H11F H -0.028572 0.762731 0.526332 0.142 Uiso 0.718(8) 1 calc R U P . .
C110 C 0.1668(8) 0.4212(12) 0.1103(12) 0.154(15) Uani 0.751(8) 1 d . . P . .
H11A H 0.187577 0.394025 0.116608 0.231 Uiso 0.751(8) 1 calc R U P . .
H11B H 0.163668 0.432751 0.158567 0.231 Uiso 0.751(8) 1 calc R U P . .
H11C H 0.185565 0.442390 0.084473 0.231 Uiso 0.751(8) 1 calc R U P . .
C106 C 0.0688(7) 0.3462(8) 0.2465(12) 0.091(7) Uani 0.751(8) 1 d . . P . .
H10M H 0.063246 0.315504 0.232788 0.137 Uiso 0.751(8) 1 calc R U P . .
H10N H 0.055491 0.351632 0.292043 0.137 Uiso 0.751(8) 1 calc R U P . .
H10O H 0.107592 0.353023 0.253878 0.137 Uiso 0.751(8) 1 calc R U P . .
C105 C 0.0246(10) 0.4382(7) 0.2048(12) 0.105(9) Uani 0.751(8) 1 d . . P . .
H10P H 0.060903 0.449677 0.223778 0.158 Uiso 0.751(8) 1 calc R U P . .
H10Q H 0.003424 0.437866 0.244135 0.158 Uiso 0.751(8) 1 calc R U P . .
H10R H 0.006377 0.456647 0.164485 0.158 Uiso 0.751(8) 1 calc R U P . .
C115 C -0.1204(13) 0.6928(7) 0.461(2) 0.191(17) Uani 0.718(8) 1 d . . P . .
H11G H -0.103544 0.681909 0.509275 0.287 Uiso 0.718(8) 1 calc R U P . .
H11H H -0.100455 0.681825 0.423836 0.287 Uiso 0.718(8) 1 calc R U P . .
H11I H -0.158142 0.682861 0.448687 0.287 Uiso 0.718(8) 1 calc R U P . .
C112 C -0.1935(12) 0.7133(9) 0.6186(17) 0.175(15) Uani 0.718(8) 1 d . . P . .
H11J H -0.229736 0.713321 0.587616 0.263 Uiso 0.718(8) 1 calc R U P . .
H11K H -0.196817 0.711258 0.670330 0.263 Uiso 0.718(8) 1 calc R U P . .
H11L H -0.172816 0.688413 0.605769 0.263 Uiso 0.718(8) 1 calc R U P . .
C113 C -0.198(2) 0.8092(12) 0.625(2) 0.26(2) Uani 0.718(8) 1 d . . P . .
H11M H -0.178529 0.836230 0.618919 0.394 Uiso 0.718(8) 1 calc R U P . .
H11N H -0.202852 0.807040 0.676424 0.394 Uiso 0.718(8) 1 calc R U P . .
H11O H -0.233262 0.809295 0.592498 0.394 Uiso 0.718(8) 1 calc R U P . .
C114 C -0.1541(14) 0.7704(13) 0.3701(15) 0.181(15) Uani 0.718(8) 1 d . . P . .
H11P H -0.191413 0.759438 0.359975 0.272 Uiso 0.718(8) 1 calc R U P . .
H11Q H -0.134915 0.760136 0.331878 0.272 Uiso 0.718(8) 1 calc R U P . .
H11R H -0.154546 0.802240 0.370305 0.272 Uiso 0.718(8) 1 calc R U P . .
C111 C -0.1023(18) 0.7715(19) 0.660(2) 0.30(3) Uani 0.718(8) 1 d . . P . .
H11S H -0.075272 0.750346 0.650801 0.452 Uiso 0.718(8) 1 calc R U P . .
H11T H -0.108146 0.768102 0.710776 0.452 Uiso 0.718(8) 1 calc R U P . .
H11U H -0.089363 0.800970 0.653503 0.452 Uiso 0.718(8) 1 calc R U P . .
O7 O 0.0630(7) 0.3831(4) 0.1052(8) 0.105(6) Uani 0.751(8) 1 d . . P . .
C1 C 0.3298(4) 0.5885(3) 0.7167(4) 0.0250(19) Uani 1 1 d . . . . .
C14 C 0.3681(6) 0.5148(7) 0.9162(9) 0.128(9) Uani 1 1 d . . . . .
H14A H 0.334620 0.531509 0.914281 0.192 Uiso 1 1 calc R U . . .
H14B H 0.379275 0.502327 0.965406 0.192 Uiso 1 1 calc R U . . .
H14C H 0.361690 0.491327 0.879858 0.192 Uiso 1 1 calc R U . . .
C84A C 0.3773(6) 0.5001(5) 0.1748(8) 0.054(4) Uani 0.838(15) 1 d . . P A 1
H84A H 0.405582 0.516172 0.207856 0.081 Uiso 0.838(15) 1 calc R U P A 1
H84B H 0.387013 0.497891 0.126172 0.081 Uiso 0.838(15) 1 calc R U P A 1
H84C H 0.373794 0.470937 0.194506 0.081 Uiso 0.838(15) 1 calc R U P A 1
C82A C 0.2820(6) 0.5015(5) 0.1051(6) 0.054(4) Uani 0.838(15) 1 d . . P A 1
H82A H 0.276901 0.471074 0.117880 0.082 Uiso 0.838(15) 1 calc R U P A 1
H82B H 0.295728 0.502785 0.059003 0.082 Uiso 0.838(15) 1 calc R U P A 1
H82C H 0.247197 0.516815 0.099025 0.082 Uiso 0.838(15) 1 calc R U P A 1
C83A C 0.3310(7) 0.5705(5) 0.1436(8) 0.065(5) Uani 0.838(15) 1 d . . P A 1
H83A H 0.297885 0.586979 0.145375 0.098 Uiso 0.838(15) 1 calc R U P A 1
H83B H 0.337774 0.570368 0.093268 0.098 Uiso 0.838(15) 1 calc R U P A 1
H83C H 0.361746 0.584002 0.176343 0.098 Uiso 0.838(15) 1 calc R U P A 1
C83B C 0.3775(18) 0.5481(15) 0.188(3) 0.016(12) Uani 0.162(15) 1 d . U P A 2
H83D H 0.400576 0.534120 0.229725 0.024 Uiso 0.162(15) 1 calc R U P A 2
H83E H 0.370489 0.578266 0.200112 0.024 Uiso 0.162(15) 1 calc R U P A 2
H83F H 0.395849 0.547693 0.145425 0.024 Uiso 0.162(15) 1 calc R U P A 2
C82B C 0.285(3) 0.543(2) 0.114(3) 0.045(18) Uani 0.162(15) 1 d . U P A 2
H82D H 0.297594 0.542877 0.067371 0.067 Uiso 0.162(15) 1 calc R U P A 2
H82E H 0.278956 0.573144 0.128299 0.067 Uiso 0.162(15) 1 calc R U P A 2
H82F H 0.250950 0.526779 0.109247 0.067 Uiso 0.162(15) 1 calc R U P A 2
C84B C 0.338(3) 0.476(2) 0.143(4) 0.042(17) Uani 0.162(15) 1 d . U P A 2
H84D H 0.354767 0.458478 0.186013 0.062 Uiso 0.162(15) 1 calc R U P A 2
H84E H 0.364152 0.477708 0.109175 0.062 Uiso 0.162(15) 1 calc R U P A 2
H84F H 0.305199 0.461259 0.117829 0.062 Uiso 0.162(15) 1 calc R U P A 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ni3 0.0234(5) 0.0141(5) 0.0163(5) 0.0001(4) 0.0058(4) -0.0009(4)
Ni2 0.0322(6) 0.0153(5) 0.0167(5) 0.0014(4) 0.0055(4) 0.0008(4)
Ni1 0.0229(5) 0.0167(5) 0.0146(5) 0.0002(4) 0.0042(4) 0.0006(4)
Fe04 0.0346(11) 0.0224(10) 0.0503(13) 0.0001(9) 0.0131(9) -0.0166(8)
Fe05 0.0351(11) 0.0448(12) 0.0466(13) 0.0009(10) 0.0136(9) 0.0200(10)
P2 0.0236(11) 0.0110(9) 0.0179(11) 0.0009(8) 0.0049(8) 0.0003(8)
P1 0.0344(12) 0.0134(10) 0.0165(11) 0.0024(8) 0.0071(9) 0.0012(9)
Si2 0.051(3) 0.067(3) 0.060(3) 0.002(2) 0.012(2) -0.028(2)
Si1 0.061(3) 0.059(3) 0.071(3) -0.022(2) 0.035(2) -0.030(2)
O1 0.023(3) 0.030(3) 0.011(3) -0.001(2) -0.003(2) 0.005(2)
O3 0.037(3) 0.009(3) 0.019(3) 0.001(2) 0.010(2) -0.001(2)
O4 0.020(3) 0.026(3) 0.021(3) 0.002(2) 0.005(2) 0.005(2)
O5 0.045(4) 0.019(3) 0.023(3) -0.001(3) 0.016(3) -0.001(3)
O6 0.029(3) 0.022(3) 0.018(3) -0.001(2) 0.011(2) 0.004(2)
O2 0.050(4) 0.016(3) 0.029(4) 0.002(3) 0.016(3) 0.004(3)
N2 0.022(4) 0.019(3) 0.016(4) 0.002(3) 0.007(3) 0.003(3)
Si4 0.043(3) 0.059(3) 0.140(6) -0.035(4) 0.024(3) -0.011(2)
N1 0.030(4) 0.008(3) 0.030(4) 0.000(3) 0.012(3) 0.008(3)
C43 0.015(4) 0.018(4) 0.018(4) -0.007(3) 0.007(3) 0.005(3)
C46 0.017(4) 0.017(4) 0.028(5) -0.004(3) 0.008(3) -0.005(3)
C45 0.019(4) 0.023(4) 0.018(4) 0.002(3) 0.003(3) 0.007(3)
C2 0.030(5) 0.017(4) 0.020(4) 0.007(3) 0.004(3) 0.009(3)
C44 0.017(4) 0.011(4) 0.016(4) 0.000(3) -0.001(3) 0.008(3)
C59 0.027(4) 0.013(4) 0.023(5) 0.001(3) 0.007(3) -0.003(3)
Si3 0.132(6) 0.080(5) 0.104(5) 0.002(4) 0.040(5) -0.064(4)
C47 0.025(4) 0.018(4) 0.021(4) 0.000(3) 0.005(3) -0.001(3)
C60 0.030(5) 0.022(5) 0.033(5) 0.003(4) 0.004(4) -0.010(4)
C72 0.030(5) 0.010(4) 0.027(5) -0.004(3) 0.007(4) -0.006(3)
C32 0.011(4) 0.026(4) 0.029(5) -0.005(4) 0.006(3) -0.002(3)
C48 0.025(4) 0.018(4) 0.025(5) -0.003(4) 0.007(4) -0.002(3)
C29 0.032(4) 0.005(3) 0.013(4) -0.001(3) 0.007(3) -0.001(3)
C58 0.040(5) 0.014(4) 0.019(5) 0.001(3) 0.007(4) -0.006(4)
C62 0.031(5) 0.020(4) 0.019(4) -0.003(3) 0.007(4) -0.010(3)
C71 0.035(5) 0.012(4) 0.009(4) -0.001(3) 0.001(3) 0.000(3)
C30 0.029(4) 0.012(4) 0.022(5) 0.002(3) 0.006(4) -0.005(3)
C15 0.032(5) 0.016(4) 0.025(5) 0.010(3) 0.010(4) -0.002(3)
C53 0.029(4) 0.016(4) 0.019(4) 0.003(3) 0.004(3) -0.004(3)
C63 0.020(4) 0.022(4) 0.020(4) -0.003(3) -0.002(3) 0.001(3)
C34 0.024(4) 0.017(4) 0.021(4) 0.005(3) 0.006(3) -0.001(3)
C31 0.028(4) 0.023(4) 0.019(4) -0.004(4) 0.007(3) 0.004(4)
C76 0.028(5) 0.025(5) 0.024(5) 0.003(4) 0.008(4) 0.005(4)
C57 0.024(4) 0.012(4) 0.016(4) 0.000(3) 0.001(3) -0.010(3)
C33 0.021(4) 0.029(5) 0.015(4) -0.002(4) 0.006(3) 0.000(3)
C54 0.028(5) 0.019(4) 0.036(5) 0.010(4) 0.006(4) 0.008(4)
C61 0.039(5) 0.029(5) 0.012(4) -0.003(4) 0.002(4) -0.008(4)
C6 0.049(6) 0.056(7) 0.023(5) 0.013(5) 0.010(5) 0.012(5)
C64 0.025(4) 0.032(5) 0.021(5) 0.003(4) 0.004(4) -0.008(4)
C3 0.025(4) 0.049(6) 0.020(5) -0.003(4) 0.005(4) 0.004(4)
C49 0.018(4) 0.050(6) 0.015(4) -0.006(4) 0.001(3) -0.014(4)
C42 0.031(5) 0.041(6) 0.023(5) -0.014(4) 0.003(4) -0.008(4)
C19 0.059(6) 0.023(5) 0.024(5) 0.010(4) 0.012(4) -0.005(4)
C16 0.053(6) 0.019(4) 0.023(5) 0.005(4) 0.006(4) 0.003(4)
C39 0.036(5) 0.034(5) 0.011(4) -0.004(4) 0.002(4) -0.006(4)
C35 0.011(4) 0.033(5) 0.029(5) -0.005(4) -0.005(3) 0.000(3)
C75 0.053(6) 0.024(5) 0.023(5) -0.005(4) 0.014(4) 0.006(4)
C20 0.048(6) 0.016(4) 0.029(5) -0.003(4) 0.009(4) -0.014(4)
C65 0.041(5) 0.033(5) 0.018(5) -0.004(4) 0.003(4) -0.009(4)
C81 0.048(6) 0.030(5) 0.023(5) -0.010(4) 0.017(4) -0.004(4)
C37 0.014(4) 0.033(5) 0.023(5) -0.007(4) -0.007(3) 0.006(3)
C7 0.015(4) 0.055(6) 0.026(5) -0.006(4) -0.008(4) 0.017(4)
C55 0.043(6) 0.027(5) 0.027(5) 0.005(4) 0.017(4) -0.006(4)
C40 0.058(7) 0.050(6) 0.011(5) -0.008(4) 0.002(4) -0.004(5)
C73 0.041(5) 0.018(4) 0.032(5) -0.001(4) 0.011(4) -0.001(4)
C74 0.046(6) 0.019(4) 0.027(5) -0.011(4) 0.014(4) 0.000(4)
C36 0.021(4) 0.042(6) 0.031(5) -0.003(4) 0.003(4) -0.016(4)
C25 0.085(9) 0.033(6) 0.037(6) 0.005(5) 0.029(6) -0.017(6)
C56 0.040(5) 0.033(5) 0.021(5) 0.014(4) 0.001(4) 0.000(4)
C98 0.041(6) 0.022(5) 0.071(8) -0.006(5) 0.026(6) -0.015(4)
C41 0.041(6) 0.036(5) 0.026(5) -0.005(4) 0.013(4) -0.004(4)
C4 0.022(5) 0.090(9) 0.029(6) 0.015(6) 0.000(4) 0.015(5)
C52 0.032(5) 0.046(6) 0.035(6) -0.002(5) 0.003(4) -0.014(4)
C77 0.065(7) 0.017(5) 0.034(6) -0.002(4) 0.026(5) 0.002(4)
C95 0.039(5) 0.004(4) 0.069(7) 0.001(4) 0.012(5) 0.000(4)
C9 0.027(5) 0.049(6) 0.055(7) -0.024(5) 0.008(5) 0.008(4)
C50 0.023(5) 0.044(6) 0.037(6) 0.006(5) 0.000(4) -0.004(4)
C66 0.029(5) 0.042(6) 0.037(6) -0.002(5) 0.014(4) -0.001(4)
C97 0.053(7) 0.024(5) 0.058(7) -0.007(5) 0.025(6) -0.017(5)
C38 0.041(6) 0.036(5) 0.030(5) -0.018(4) -0.002(4) 0.004(4)
C27 0.099(10) 0.044(7) 0.047(7) 0.012(6) 0.038(7) -0.006(7)
C67 0.035(5) 0.050(6) 0.030(5) -0.014(5) -0.004(4) -0.008(5)
C17 0.065(7) 0.028(5) 0.037(6) 0.007(4) 0.023(5) 0.004(5)
C87 0.030(5) 0.044(6) 0.048(6) 0.007(5) 0.011(5) 0.020(5)
C99 0.039(6) 0.021(5) 0.060(7) 0.001(5) 0.006(5) -0.011(4)
C89 0.036(5) 0.036(6) 0.049(6) 0.003(5) 0.001(5) 0.027(5)
C85 0.024(5) 0.057(7) 0.064(7) 0.003(6) 0.023(5) 0.022(5)
C18 0.073(8) 0.014(5) 0.042(6) 0.016(4) 0.020(5) -0.010(5)
C96 0.066(7) 0.022(5) 0.044(7) -0.001(5) 0.000(6) -0.011(5)
C86 0.041(6) 0.050(7) 0.054(7) -0.007(5) 0.023(5) 0.022(5)
C8 0.032(5) 0.045(6) 0.035(6) -0.018(5) 0.009(4) -0.003(4)
C70 0.048(6) 0.063(8) 0.030(6) -0.011(5) -0.006(5) 0.002(6)
C26 0.094(10) 0.079(9) 0.028(6) 0.004(6) 0.020(6) -0.031(8)
C79 0.058(7) 0.013(4) 0.054(7) 0.006(4) 0.018(5) 0.010(4)
C69 0.085(9) 0.065(8) 0.018(5) 0.009(5) 0.000(5) 0.011(7)
C51 0.050(6) 0.038(6) 0.022(5) -0.007(4) 0.005(4) -0.018(5)
O8 0.038(6) 0.044(6) 0.093(7) 0.010(5) 0.021(5) -0.005(5)
C88 0.025(5) 0.050(6) 0.051(7) -0.013(5) -0.004(5) 0.016(5)
C104 0.039(6) 0.026(5) 0.073(8) -0.013(5) -0.005(5) -0.009(4)
C94 0.043(6) 0.042(6) 0.064(8) -0.007(6) -0.010(5) 0.027(5)
C5 0.046(7) 0.082(9) 0.035(6) 0.020(6) 0.009(5) 0.011(6)
C92 0.048(7) 0.056(7) 0.054(7) 0.008(6) 0.024(5) 0.026(6)
C10 0.017(5) 0.092(10) 0.052(7) -0.006(7) -0.006(5) 0.001(5)
C28 0.130(13) 0.051(8) 0.057(8) -0.010(6) 0.058(8) -0.037(8)
C78 0.057(7) 0.040(6) 0.043(6) -0.006(5) 0.014(5) -0.014(5)
C100 0.037(6) 0.044(6) 0.075(8) -0.002(6) 0.023(6) -0.005(5)
C91 0.076(9) 0.057(8) 0.056(8) -0.001(6) 0.037(7) 0.019(7)
C93 0.052(7) 0.043(7) 0.082(9) 0.018(6) 0.018(7) 0.013(6)
C68 0.045(7) 0.070(8) 0.046(7) -0.020(6) -0.004(5) -0.023(6)
C21 0.117(11) 0.015(5) 0.065(8) 0.010(5) 0.056(8) -0.002(6)
C103 0.055(7) 0.026(6) 0.121(12) -0.007(6) 0.041(8) -0.010(5)
C23 0.083(9) 0.038(6) 0.046(7) -0.021(5) 0.025(6) -0.013(6)
C80 0.111(11) 0.011(5) 0.054(7) -0.010(5) 0.033(7) -0.017(6)
C12 0.083(11) 0.161(18) 0.088(12) 0.085(12) 0.025(9) 0.055(11)
C90 0.040(6) 0.068(8) 0.077(9) -0.007(7) 0.028(6) 0.019(6)
C11 0.042(7) 0.125(13) 0.047(8) 0.039(8) -0.003(6) 0.014(8)
C102 0.071(8) 0.042(6) 0.066(8) 0.007(6) 0.038(7) -0.014(6)
C101 0.069(8) 0.042(7) 0.062(8) -0.006(6) 0.014(7) -0.025(6)
C22 0.092(10) 0.040(7) 0.058(8) 0.003(6) 0.021(7) 0.035(7)
C13 0.070(10) 0.19(2) 0.031(7) 0.028(10) 0.002(7) 0.005(11)
C108 0.070(11) 0.031(8) 0.079(12) 0.014(8) 0.030(9) 0.011(7)
C24 0.162(15) 0.021(6) 0.083(10) 0.024(6) 0.069(10) 0.017(8)
C109 0.123(18) 0.039(10) 0.067(12) -0.010(9) -0.010(11) -0.023(10)
C107 0.108(16) 0.133(19) 0.046(11) -0.005(11) 0.012(10) -0.094(15)
C116 0.058(11) 0.071(13) 0.17(2) -0.007(15) 0.049(12) 0.011(10)
C110 0.059(14) 0.31(4) 0.072(15) 0.01(2) -0.032(12) -0.08(2)
C106 0.047(11) 0.14(2) 0.094(16) -0.013(14) 0.021(10) -0.019(12)
C105 0.123(19) 0.107(18) 0.104(17) -0.068(15) 0.066(15) -0.041(15)
C115 0.15(3) 0.031(12) 0.42(5) -0.067(17) 0.13(3) -0.032(13)
C112 0.15(3) 0.16(2) 0.19(3) 0.12(2) -0.04(2) -0.12(2)
C113 0.47(6) 0.15(2) 0.27(5) -0.03(3) 0.31(4) -0.05(4)
C114 0.19(3) 0.26(4) 0.073(13) -0.02(2) -0.024(17) -0.06(3)
C111 0.24(3) 0.49(7) 0.14(2) 0.05(4) -0.05(3) -0.27(4)
O7 0.179(16) 0.058(8) 0.113(12) -0.014(8) 0.115(12) -0.044(9)
C1 0.034(5) 0.025(5) 0.017(4) -0.002(4) 0.005(4) -0.002(4)
C14 0.073(10) 0.22(2) 0.089(12) 0.128(14) 0.008(9) 0.023(12)
C84A 0.063(9) 0.057(9) 0.057(9) 0.006(7) 0.050(8) 0.013(7)
C82A 0.061(9) 0.084(12) 0.020(7) -0.004(7) 0.010(6) 0.007(8)
C83A 0.117(14) 0.055(9) 0.042(9) -0.001(7) 0.063(9) -0.010(9)
C83B 0.02(2) 0.01(2) 0.02(2) 0.010(18) 0.002(18) 0.004(18)
C82B 0.05(3) 0.05(3) 0.03(3) -0.03(3) 0.00(3) -0.01(3)
C84B 0.03(3) 0.04(3) 0.06(3) -0.02(3) 0.02(3) 0.01(2)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ni3 O6 1.859(6) . ?
Ni3 N2 1.864(6) . ?
Ni3 N1 1.869(7) . ?
Ni3 O3 1.878(5) . ?
Ni3 Ni1 2.4768(16) . ?
Ni3 Ni2 2.6363(17) . ?
Ni2 N1 1.857(7) . ?
Ni2 N2 1.862(6) . ?
Ni2 O2 1.888(6) . ?
Ni2 O5 1.890(6) . ?
Ni2 Ni1 2.6570(17) . ?
Ni1 N2 1.853(7) . ?
Ni1 N1 1.856(7) . ?
Ni1 O4 1.858(6) . ?
Ni1 O1 1.880(5) . ?
Fe04 C95 2.048(8) . ?
Fe04 C95 2.048(8) 3_566 ?
Fe04 C96 2.091(10) . ?
Fe04 C96 2.091(10) 3_566 ?
Fe04 C97 2.109(10) . ?
Fe04 C97 2.109(10) 3_566 ?
Fe04 C99 2.111(9) 3_566 ?
Fe04 C99 2.111(9) . ?
Fe04 C98 2.131(9) . ?
Fe04 C98 2.131(9) 3_566 ?
Fe05 C87 2.069(11) 3_666 ?
Fe05 C87 2.069(11) . ?
Fe05 C88 2.086(11) . ?
Fe05 C88 2.086(11) 3_666 ?
Fe05 C86 2.089(10) . ?
Fe05 C86 2.089(10) 3_666 ?
Fe05 C85 2.093(9) . ?
Fe05 C85 2.093(9) 3_666 ?
Fe05 C89 2.103(9) . ?
Fe05 C89 2.103(9) 3_666 ?
P2 N2 1.626(7) . ?
P2 C43 1.772(8) . ?
P2 C71 1.781(8) . ?
P2 C57 1.789(8) . ?
P1 N1 1.611(7) . ?
P1 C1 1.779(9) . ?
P1 C29 1.781(7) . ?
P1 C15 1.789(8) . ?
Si2 O7 1.628(11) . ?
Si2 C108 1.808(17) . ?
Si2 C109 1.832(18) . ?
Si2 C110 1.841(18) . ?
Si1 O7 1.582(12) . ?
Si1 C107 1.797(17) . ?
Si1 C105 1.87(2) . ?
Si1 C106 1.90(2) . ?
O1 C2 1.300(9) . ?
O3 C30 1.333(10) . ?
O4 C44 1.336(9) . ?
O5 C72 1.297(10) . ?
O6 C58 1.331(10) . ?
O2 C16 1.314(11) . ?
Si4 O8 1.620(13) . ?
Si4 C115 1.77(2) . ?
Si4 C114 1.86(3) . ?
Si4 C116 1.88(2) . ?
C43 C44 1.418(11) . ?
C43 C48 1.430(11) . ?
C46 C45 1.379(11) . ?
C46 C47 1.407(11) . ?
C46 H46 0.9500 . ?
C45 C44 1.435(11) . ?
C45 C49 1.545(11) . ?
C2 C1 1.433(12) . ?
C2 C3 1.441(12) . ?
C59 C60 1.366(12) . ?
C59 C58 1.406(12) . ?
C59 C63 1.531(11) . ?
Si3 O8 1.568(14) . ?
Si3 C111 1.61(3) . ?
Si3 C113 1.81(4) . ?
Si3 C112 1.82(2) . ?
C47 C48 1.370(11) . ?
C47 C53 1.522(11) . ?
C60 C61 1.394(13) . ?
C60 H60 0.9500 . ?
C72 C71 1.421(11) . ?
C72 C73 1.451(11) . ?
C32 C31 1.364(12) . ?
C32 C33 1.417(11) . ?
C32 H32 0.9500 . ?
C48 H48 0.9500 . ?
C29 C34 1.392(11) . ?
C29 C30 1.408(11) . ?
C58 C57 1.437(11) . ?
C62 C61 1.367(12) . ?
C62 C57 1.419(11) . ?
C62 H62 0.9500 . ?
C71 C76 1.426(11) . ?
C30 C31 1.441(11) . ?
C15 C20 1.402(12) . ?
C15 C16 1.419(12) . ?
C53 C55 1.531(12) . ?
C53 C56 1.541(12) . ?
C53 C54 1.542(11) . ?
C63 C64 1.529(11) . ?
C63 C65 1.546(12) . ?
C63 C66 1.547(12) . ?
C34 C33 1.363(11) . ?
C34 H34 0.9500 . ?
C31 C35 1.525(11) . ?
C76 C75 1.374(12) . ?
C76 H76 0.9500 . ?
C33 C39 1.537(11) . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C61 C67 1.524(12) . ?
C6 C5 1.384(15) . ?
C6 C1 1.410(12) . ?
C6 H6 0.9500 . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C3 C4 1.358(13) . ?
C3 C7 1.523(14) . ?
C49 C52 1.526(13) . ?
C49 C51 1.542(12) . ?
C49 C50 1.547(13) . ?
C42 C39 1.549(12) . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C19 C20 1.378(12) . ?
C19 C18 1.411(14) . ?
C19 C25 1.509(13) . ?
C16 C17 1.416(13) . ?
C39 C40 1.500(13) . ?
C39 C41 1.552(12) . ?
C35 C36 1.528(11) . ?
C35 C38 1.533(12) . ?
C35 C37 1.535(12) . ?
C75 C74 1.373(12) . ?
C75 C81 1.554(12) . ?
C20 H20 0.9500 . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C81 C82B 1.40(7) . ?
C81 C84A 1.504(16) . ?
C81 C83B 1.52(5) . ?
C81 C83A 1.528(16) . ?
C81 C82A 1.582(16) . ?
C81 C84B 1.62(6) . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C7 C9 1.517(14) . ?
C7 C8 1.535(12) . ?
C7 C10 1.539(12) . ?
C55 H55A 0.9800 . ?
C55 H55B 0.9800 . ?
C55 H55C 0.9800 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C73 C74 1.369(12) . ?
C73 C77 1.555(12) . ?
C74 H74 0.9500 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C25 C27 1.520(17) . ?
C25 C26 1.531(17) . ?
C25 C28 1.530(16) . ?
C56 H56A 0.9800 . ?
C56 H56B 0.9800 . ?
C56 H56C 0.9800 . ?
C98 C97 1.433(16) . ?
C98 C99 1.435(15) . ?
C98 C103 1.471(15) . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C4 C5 1.386(16) . ?
C4 H4 0.9500 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C77 C80 1.531(13) . ?
C77 C78 1.539(14) . ?
C77 C79 1.549(14) . ?
C95 C96 1.425(15) . ?
C95 C99 1.428(14) . ?
C95 C100 1.536(14) . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 H50C 0.9800 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C97 C96 1.433(15) . ?
C97 C102 1.496(15) . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
C67 C70 1.514(14) . ?
C67 C69 1.543(15) . ?
C67 C68 1.544(14) . ?
C17 C18 1.407(14) . ?
C17 C21 1.534(14) . ?
C87 C86 1.408(15) . ?
C87 C88 1.464(15) . ?
C87 C92 1.517(15) . ?
C99 C104 1.475(15) . ?
C89 C88 1.428(14) . ?
C89 C85 1.451(15) . ?
C89 C94 1.526(14) . ?
C85 C86 1.417(15) . ?
C85 C90 1.513(15) . ?
C18 H18 0.9500 . ?
C96 C101 1.453(16) . ?
C86 C91 1.522(16) . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C70 H70A 0.9800 . ?
C70 H70B 0.9800 . ?
C70 H70C 0.9800 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C79 H79A 0.9800 . ?
C79 H79B 0.9800 . ?
C79 H79C 0.9800 . ?
C69 H69A 0.9800 . ?
C69 H69B 0.9800 . ?
C69 H69C 0.9800 . ?
C51 H51A 0.9800 . ?
C51 H51B 0.9800 . ?
C51 H51C 0.9800 . ?
C88 C93 1.492(16) . ?
C104 H10S 0.9800 . ?
C104 H10T 0.9800 . ?
C104 H10U 0.9800 . ?
C94 H94A 0.9800 . ?
C94 H94B 0.9800 . ?
C94 H94C 0.9800 . ?
C5 C11 1.555(15) . ?
C92 H92A 0.9800 . ?
C92 H92B 0.9800 . ?
C92 H92C 0.9800 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C78 H78A 0.9800 . ?
C78 H78B 0.9800 . ?
C78 H78C 0.9800 . ?
C100 H10V 0.9800 . ?
C100 H10W 0.9800 . ?
C100 H10X 0.9800 . ?
C91 H91A 0.9800 . ?
C91 H91B 0.9800 . ?
C91 H91C 0.9800 . ?
C93 H93A 0.9800 . ?
C93 H93B 0.9800 . ?
C93 H93C 0.9800 . ?
C68 H68A 0.9800 . ?
C68 H68B 0.9800 . ?
C68 H68C 0.9800 . ?
C21 C22 1.518(18) . ?
C21 C23 1.528(17) . ?
C21 C24 1.537(14) . ?
C103 H10Y 0.9800 . ?
C103 H 0.9800 . ?
C103 HA 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C80 H80A 0.9800 . ?
C80 H80B 0.9800 . ?
C80 H80C 0.9800 . ?
C12 C11 1.531(19) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C90 H90A 0.9800 . ?
C90 H90B 0.9800 . ?
C90 H90C 0.9800 . ?
C11 C14 1.51(2) . ?
C11 C13 1.55(2) . ?
C102 H10Z 0.9800 . ?
C102 HB 0.9800 . ?
C102 HC 0.9800 . ?
C101 H10 0.9800 . ?
C101 HD 0.9800 . ?
C101 HE 0.9800 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 H13C 0.9800 . ?
C108 H10D 0.9800 . ?
C108 H10E 0.9800 . ?
C108 H10F 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C109 H10G 0.9800 . ?
C109 H10H 0.9800 . ?
C109 H10I 0.9800 . ?
C107 H10J 0.9800 . ?
C107 H10K 0.9800 . ?
C107 H10L 0.9800 . ?
C116 H11D 0.9800 . ?
C116 H11E 0.9800 . ?
C116 H11F 0.9800 . ?
C110 H11A 0.9800 . ?
C110 H11B 0.9800 . ?
C110 H11C 0.9800 . ?
C106 H10M 0.9800 . ?
C106 H10N 0.9800 . ?
C106 H10O 0.9800 . ?
C105 H10P 0.9800 . ?
C105 H10Q 0.9800 . ?
C105 H10R 0.9800 . ?
C115 H11G 0.9800 . ?
C115 H11H 0.9800 . ?
C115 H11I 0.9800 . ?
C112 H11J 0.9800 . ?
C112 H11K 0.9800 . ?
C112 H11L 0.9800 . ?
C113 H11M 0.9800 . ?
C113 H11N 0.9800 . ?
C113 H11O 0.9800 . ?
C114 H11P 0.9800 . ?
C114 H11Q 0.9800 . ?
C114 H11R 0.9800 . ?
C111 H11S 0.9800 . ?
C111 H11T 0.9800 . ?
C111 H11U 0.9800 . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C84A H84A 0.9800 . ?
C84A H84B 0.9800 . ?
C84A H84C 0.9800 . ?
C82A H82A 0.9800 . ?
C82A H82B 0.9800 . ?
C82A H82C 0.9800 . ?
C83A H83A 0.9800 . ?
C83A H83B 0.9800 . ?
C83A H83C 0.9800 . ?
C83B H83D 0.9800 . ?
C83B H83E 0.9800 . ?
C83B H83F 0.9800 . ?
C82B H82D 0.9800 . ?
C82B H82E 0.9800 . ?
C82B H82F 0.9800 . ?
C84B H84D 0.9800 . ?
C84B H84E 0.9800 . ?
C84B H84F 0.9800 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O6 Ni3 N2 98.1(3) . . ?
O6 Ni3 N1 170.2(3) . . ?
N2 Ni3 N1 72.5(3) . . ?
O6 Ni3 O3 92.0(2) . . ?
N2 Ni3 O3 169.4(3) . . ?
N1 Ni3 O3 97.3(3) . . ?
O6 Ni3 Ni1 127.24(17) . . ?
N2 Ni3 Ni1 48.0(2) . . ?
N1 Ni3 Ni1 48.1(2) . . ?
O3 Ni3 Ni1 126.79(18) . . ?
O6 Ni3 Ni2 126.29(17) . . ?
N2 Ni3 Ni2 44.9(2) . . ?
N1 Ni3 Ni2 44.8(2) . . ?
O3 Ni3 Ni2 125.39(16) . . ?
Ni1 Ni3 Ni2 62.53(4) . . ?
N1 Ni2 N2 72.8(3) . . ?
N1 Ni2 O2 96.7(3) . . ?
N2 Ni2 O2 169.2(3) . . ?
N1 Ni2 O5 170.6(3) . . ?
N2 Ni2 O5 97.8(3) . . ?
O2 Ni2 O5 92.7(3) . . ?
N1 Ni2 Ni3 45.1(2) . . ?
N2 Ni2 Ni3 44.98(19) . . ?
O2 Ni2 Ni3 128.52(18) . . ?
O5 Ni2 Ni3 126.93(19) . . ?
N1 Ni2 Ni1 44.3(2) . . ?
N2 Ni2 Ni1 44.2(2) . . ?
O2 Ni2 Ni1 126.0(2) . . ?
O5 Ni2 Ni1 129.03(18) . . ?
Ni3 Ni2 Ni1 55.79(4) . . ?
N2 Ni1 N1 73.0(3) . . ?
N2 Ni1 O4 97.5(3) . . ?
N1 Ni1 O4 170.5(3) . . ?
N2 Ni1 O1 168.4(3) . . ?
N1 Ni1 O1 97.1(3) . . ?
O4 Ni1 O1 92.2(2) . . ?
N2 Ni1 Ni3 48.4(2) . . ?
N1 Ni1 Ni3 48.5(2) . . ?
O4 Ni1 Ni3 125.31(17) . . ?
O1 Ni1 Ni3 128.94(18) . . ?
N2 Ni1 Ni2 44.5(2) . . ?
N1 Ni1 Ni2 44.3(2) . . ?
O4 Ni1 Ni2 127.85(18) . . ?
O1 Ni1 Ni2 124.07(18) . . ?
Ni3 Ni1 Ni2 61.68(4) . . ?
C95 Fe04 C95 180.0 . 3_566 ?
C95 Fe04 C96 40.3(4) . . ?
C95 Fe04 C96 139.7(4) 3_566 . ?
C95 Fe04 C96 139.7(4) . 3_566 ?
C95 Fe04 C96 40.3(4) 3_566 3_566 ?
C96 Fe04 C96 180.0(3) . 3_566 ?
C95 Fe04 C97 66.8(4) . . ?
C95 Fe04 C97 113.2(4) 3_566 . ?
C96 Fe04 C97 39.9(4) . . ?
C96 Fe04 C97 140.1(4) 3_566 . ?
C95 Fe04 C97 113.2(4) . 3_566 ?
C95 Fe04 C97 66.8(4) 3_566 3_566 ?
C96 Fe04 C97 140.1(4) . 3_566 ?
C96 Fe04 C97 39.9(4) 3_566 3_566 ?
C97 Fe04 C97 180.0 . 3_566 ?
C95 Fe04 C99 139.9(4) . 3_566 ?
C95 Fe04 C99 40.1(4) 3_566 3_566 ?
C96 Fe04 C99 112.4(4) . 3_566 ?
C96 Fe04 C99 67.6(4) 3_566 3_566 ?
C97 Fe04 C99 113.3(4) . 3_566 ?
C97 Fe04 C99 66.7(4) 3_566 3_566 ?
C95 Fe04 C99 40.1(4) . . ?
C95 Fe04 C99 139.9(4) 3_566 . ?
C96 Fe04 C99 67.6(4) . . ?
C96 Fe04 C99 112.4(4) 3_566 . ?
C97 Fe04 C99 66.7(4) . . ?
C97 Fe04 C99 113.3(4) 3_566 . ?
C99 Fe04 C99 180.0 3_566 . ?
C95 Fe04 C98 66.7(4) . . ?
C95 Fe04 C98 113.3(4) 3_566 . ?
C96 Fe04 C98 67.0(4) . . ?
C96 Fe04 C98 113.0(4) 3_566 . ?
C97 Fe04 C98 39.5(4) . . ?
C97 Fe04 C98 140.5(4) 3_566 . ?
C99 Fe04 C98 140.5(4) 3_566 . ?
C99 Fe04 C98 39.5(4) . . ?
C95 Fe04 C98 113.3(4) . 3_566 ?
C95 Fe04 C98 66.7(4) 3_566 3_566 ?
C96 Fe04 C98 113.0(4) . 3_566 ?
C96 Fe04 C98 67.0(4) 3_566 3_566 ?
C97 Fe04 C98 140.5(4) . 3_566 ?
C97 Fe04 C98 39.5(4) 3_566 3_566 ?
C99 Fe04 C98 39.5(4) 3_566 3_566 ?
C99 Fe04 C98 140.5(4) . 3_566 ?
C98 Fe04 C98 180.0 . 3_566 ?
C87 Fe05 C87 180.0 3_666 . ?
C87 Fe05 C88 138.7(4) 3_666 . ?
C87 Fe05 C88 41.3(4) . . ?
C87 Fe05 C88 41.3(4) 3_666 3_666 ?
C87 Fe05 C88 138.7(4) . 3_666 ?
C88 Fe05 C88 180.0 . 3_666 ?
C87 Fe05 C86 140.4(4) 3_666 . ?
C87 Fe05 C86 39.6(4) . . ?
C88 Fe05 C86 67.9(4) . . ?
C88 Fe05 C86 112.1(4) 3_666 . ?
C87 Fe05 C86 39.6(4) 3_666 3_666 ?
C87 Fe05 C86 140.4(4) . 3_666 ?
C88 Fe05 C86 112.1(4) . 3_666 ?
C88 Fe05 C86 67.9(4) 3_666 3_666 ?
C86 Fe05 C86 180.0(5) . 3_666 ?
C87 Fe05 C85 112.9(4) 3_666 . ?
C87 Fe05 C85 67.1(4) . . ?
C88 Fe05 C85 67.9(4) . . ?
C88 Fe05 C85 112.1(4) 3_666 . ?
C86 Fe05 C85 39.6(4) . . ?
C86 Fe05 C85 140.4(4) 3_666 . ?
C87 Fe05 C85 67.1(4) 3_666 3_666 ?
C87 Fe05 C85 112.9(4) . 3_666 ?
C88 Fe05 C85 112.1(4) . 3_666 ?
C88 Fe05 C85 67.9(4) 3_666 3_666 ?
C86 Fe05 C85 140.4(4) . 3_666 ?
C86 Fe05 C85 39.6(4) 3_666 3_666 ?
C85 Fe05 C85 180.0 . 3_666 ?
C87 Fe05 C89 112.5(4) 3_666 . ?
C87 Fe05 C89 67.5(4) . . ?
C88 Fe05 C89 39.9(4) . . ?
C88 Fe05 C89 140.1(4) 3_666 . ?
C86 Fe05 C89 67.1(4) . . ?
C86 Fe05 C89 112.9(4) 3_666 . ?
C85 Fe05 C89 40.5(4) . . ?
C85 Fe05 C89 139.5(4) 3_666 . ?
C87 Fe05 C89 67.5(4) 3_666 3_666 ?
C87 Fe05 C89 112.5(4) . 3_666 ?
C88 Fe05 C89 140.1(4) . 3_666 ?
C88 Fe05 C89 39.9(4) 3_666 3_666 ?
C86 Fe05 C89 112.9(4) . 3_666 ?
C86 Fe05 C89 67.1(4) 3_666 3_666 ?
C85 Fe05 C89 139.5(4) . 3_666 ?
C85 Fe05 C89 40.5(4) 3_666 3_666 ?
C89 Fe05 C89 180.0 . 3_666 ?
N2 P2 C43 108.8(4) . . ?
N2 P2 C71 108.4(3) . . ?
C43 P2 C71 111.6(4) . . ?
N2 P2 C57 109.0(4) . . ?
C43 P2 C57 109.8(3) . . ?
C71 P2 C57 109.1(4) . . ?
N1 P1 C1 106.7(4) . . ?
N1 P1 C29 110.3(3) . . ?
C1 P1 C29 110.1(4) . . ?
N1 P1 C15 108.8(4) . . ?
C1 P1 C15 109.2(4) . . ?
C29 P1 C15 111.5(4) . . ?
O7 Si2 C108 107.9(7) . . ?
O7 Si2 C109 111.1(9) . . ?
C108 Si2 C109 110.2(8) . . ?
O7 Si2 C110 109.9(11) . . ?
C108 Si2 C110 113.7(11) . . ?
C109 Si2 C110 104.0(13) . . ?
O7 Si1 C107 110.7(9) . . ?
O7 Si1 C105 108.7(8) . . ?
C107 Si1 C105 112.2(11) . . ?
O7 Si1 C106 108.5(9) . . ?
C107 Si1 C106 106.8(10) . . ?
C105 Si1 C106 110.0(11) . . ?
C2 O1 Ni1 130.3(5) . . ?
C30 O3 Ni3 127.9(5) . . ?
C44 O4 Ni1 130.1(5) . . ?
C72 O5 Ni2 129.7(5) . . ?
C58 O6 Ni3 130.6(5) . . ?
C16 O2 Ni2 129.7(5) . . ?
P2 N2 Ni1 127.8(4) . . ?
P2 N2 Ni2 126.2(4) . . ?
Ni1 N2 Ni2 91.3(3) . . ?
P2 N2 Ni3 125.1(4) . . ?
Ni1 N2 Ni3 83.6(3) . . ?
Ni2 N2 Ni3 90.1(3) . . ?
O8 Si4 C115 109.1(13) . . ?
O8 Si4 C114 107.4(13) . . ?
C115 Si4 C114 108.9(19) . . ?
O8 Si4 C116 111.3(9) . . ?
C115 Si4 C116 112.1(12) . . ?
C114 Si4 C116 107.9(14) . . ?
P1 N1 Ni1 126.9(4) . . ?
P1 N1 Ni2 126.6(4) . . ?
Ni1 N1 Ni2 91.4(3) . . ?
P1 N1 Ni3 125.6(4) . . ?
Ni1 N1 Ni3 83.3(3) . . ?
Ni2 N1 Ni3 90.1(3) . . ?
C44 C43 C48 121.5(7) . . ?
C44 C43 P2 122.9(6) . . ?
C48 C43 P2 115.4(6) . . ?
C45 C46 C47 124.6(7) . . ?
C45 C46 H46 117.7 . . ?
C47 C46 H46 117.7 . . ?
C46 C45 C44 118.9(7) . . ?
C46 C45 C49 119.9(7) . . ?
C44 C45 C49 121.2(7) . . ?
O1 C2 C1 123.9(8) . . ?
O1 C2 C3 120.2(8) . . ?
C1 C2 C3 115.9(7) . . ?
O4 C44 C43 123.4(7) . . ?
O4 C44 C45 119.5(7) . . ?
C43 C44 C45 117.0(7) . . ?
C60 C59 C58 119.4(8) . . ?
C60 C59 C63 120.7(8) . . ?
C58 C59 C63 119.9(7) . . ?
O8 Si3 C111 112.1(16) . . ?
O8 Si3 C113 107.5(14) . . ?
C111 Si3 C113 101(3) . . ?
O8 Si3 C112 111.5(13) . . ?
C111 Si3 C112 115.1(19) . . ?
C113 Si3 C112 109.3(18) . . ?
C48 C47 C46 117.2(8) . . ?
C48 C47 C53 122.1(7) . . ?
C46 C47 C53 120.6(7) . . ?
C59 C60 C61 125.5(9) . . ?
C59 C60 H60 117.2 . . ?
C61 C60 H60 117.2 . . ?
O5 C72 C71 125.1(7) . . ?
O5 C72 C73 119.6(7) . . ?
C71 C72 C73 115.4(7) . . ?
C31 C32 C33 125.0(8) . . ?
C31 C32 H32 117.5 . . ?
C33 C32 H32 117.5 . . ?
C47 C48 C43 120.7(8) . . ?
C47 C48 H48 119.7 . . ?
C43 C48 H48 119.7 . . ?
C34 C29 C30 122.6(7) . . ?
C34 C29 P1 117.0(6) . . ?
C30 C29 P1 119.8(6) . . ?
O6 C58 C59 121.1(8) . . ?
O6 C58 C57 122.3(8) . . ?
C59 C58 C57 116.6(7) . . ?
C61 C62 C57 121.4(8) . . ?
C61 C62 H62 119.3 . . ?
C57 C62 H62 119.3 . . ?
C72 C71 C76 121.5(7) . . ?
C72 C71 P2 120.6(6) . . ?
C76 C71 P2 117.2(6) . . ?
O3 C30 C29 124.9(7) . . ?
O3 C30 C31 118.9(7) . . ?
C29 C30 C31 116.2(7) . . ?
C20 C15 C16 123.0(7) . . ?
C20 C15 P1 116.3(6) . . ?
C16 C15 P1 120.2(6) . . ?
C47 C53 C55 109.3(7) . . ?
C47 C53 C56 111.2(7) . . ?
C55 C53 C56 108.1(7) . . ?
C47 C53 C54 110.9(7) . . ?
C55 C53 C54 109.4(7) . . ?
C56 C53 C54 107.9(7) . . ?
C64 C63 C59 109.5(7) . . ?
C64 C63 C65 110.2(7) . . ?
C59 C63 C65 110.9(7) . . ?
C64 C63 C66 107.6(7) . . ?
C59 C63 C66 112.8(7) . . ?
C65 C63 C66 105.7(7) . . ?
C33 C34 C29 121.8(8) . . ?
C33 C34 H34 119.1 . . ?
C29 C34 H34 119.1 . . ?
C32 C31 C30 118.5(8) . . ?
C32 C31 C35 121.6(7) . . ?
C30 C31 C35 119.9(7) . . ?
C75 C76 C71 121.0(8) . . ?
C75 C76 H76 119.5 . . ?
C71 C76 H76 119.5 . . ?
C62 C57 C58 120.8(7) . . ?
C62 C57 P2 117.8(6) . . ?
C58 C57 P2 120.9(6) . . ?
C34 C33 C32 115.8(7) . . ?
C34 C33 C39 124.0(8) . . ?
C32 C33 C39 120.1(7) . . ?
C53 C54 H54A 109.5 . . ?
C53 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C53 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C62 C61 C60 116.2(8) . . ?
C62 C61 C67 122.5(8) . . ?
C60 C61 C67 121.3(8) . . ?
C5 C6 C1 121.7(10) . . ?
C5 C6 H6 119.1 . . ?
C1 C6 H6 119.1 . . ?
C63 C64 H64A 109.5 . . ?
C63 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C63 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C4 C3 C2 119.5(9) . . ?
C4 C3 C7 120.5(8) . . ?
C2 C3 C7 119.9(8) . . ?
C52 C49 C51 107.2(8) . . ?
C52 C49 C50 107.4(7) . . ?
C51 C49 C50 110.8(8) . . ?
C52 C49 C45 112.9(7) . . ?
C51 C49 C45 108.9(7) . . ?
C50 C49 C45 109.7(7) . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C20 C19 C18 115.1(8) . . ?
C20 C19 C25 123.5(9) . . ?
C18 C19 C25 121.3(8) . . ?
O2 C16 C17 120.1(8) . . ?
O2 C16 C15 123.4(8) . . ?
C17 C16 C15 116.4(8) . . ?
C40 C39 C33 112.1(7) . . ?
C40 C39 C42 109.0(8) . . ?
C33 C39 C42 109.1(7) . . ?
C40 C39 C41 108.7(8) . . ?
C33 C39 C41 108.9(7) . . ?
C42 C39 C41 108.9(7) . . ?
C31 C35 C36 110.4(7) . . ?
C31 C35 C38 113.4(7) . . ?
C36 C35 C38 104.7(7) . . ?
C31 C35 C37 111.3(7) . . ?
C36 C35 C37 111.0(7) . . ?
C38 C35 C37 105.8(7) . . ?
C74 C75 C76 117.4(8) . . ?
C74 C75 C81 121.9(8) . . ?
C76 C75 C81 120.7(8) . . ?
C19 C20 C15 121.2(8) . . ?
C19 C20 H20 119.4 . . ?
C15 C20 H20 119.4 . . ?
C63 C65 H65A 109.5 . . ?
C63 C65 H65B 109.5 . . ?
H65A C65 H65B 109.5 . . ?
C63 C65 H65C 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C82B C81 C83B 115(3) . . ?
C84A C81 C83A 109.3(10) . . ?
C82B C81 C75 109(3) . . ?
C84A C81 C75 111.3(9) . . ?
C83B C81 C75 106.0(19) . . ?
C83A C81 C75 113.5(8) . . ?
C84A C81 C82A 107.9(10) . . ?
C83A C81 C82A 106.3(11) . . ?
C75 C81 C82A 108.3(8) . . ?
C82B C81 C84B 110(4) . . ?
C83B C81 C84B 107(3) . . ?
C75 C81 C84B 109(3) . . ?
C35 C37 H37A 109.5 . . ?
C35 C37 H37B 109.5 . . ?
H37A C37 H37B 109.5 . . ?
C35 C37 H37C 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
C9 C7 C3 111.8(7) . . ?
C9 C7 C8 109.9(8) . . ?
C3 C7 C8 107.9(8) . . ?
C9 C7 C10 106.5(9) . . ?
C3 C7 C10 113.5(8) . . ?
C8 C7 C10 107.1(8) . . ?
C53 C55 H55A 109.5 . . ?
C53 C55 H55B 109.5 . . ?
H55A C55 H55B 109.5 . . ?
C53 C55 H55C 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C74 C73 C72 119.6(8) . . ?
C74 C73 C77 121.2(8) . . ?
C72 C73 C77 119.2(7) . . ?
C73 C74 C75 125.0(8) . . ?
C73 C74 H74 117.5 . . ?
C75 C74 H74 117.5 . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C19 C25 C27 109.3(9) . . ?
C19 C25 C26 109.9(10) . . ?
C27 C25 C26 110.1(9) . . ?
C19 C25 C28 112.1(8) . . ?
C27 C25 C28 107.9(11) . . ?
C26 C25 C28 107.5(10) . . ?
C53 C56 H56A 109.5 . . ?
C53 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C53 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C97 C98 C99 108.0(9) . . ?
C97 C98 C103 125.9(11) . . ?
C99 C98 C103 126.1(11) . . ?
C97 C98 Fe04 69.4(5) . . ?
C99 C98 Fe04 69.5(5) . . ?
C103 C98 Fe04 127.2(7) . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C3 C4 C5 125.6(10) . . ?
C3 C4 H4 117.2 . . ?
C5 C4 H4 117.2 . . ?
C49 C52 H52A 109.5 . . ?
C49 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C49 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C80 C77 C78 108.4(9) . . ?
C80 C77 C79 106.8(8) . . ?
C78 C77 C79 111.6(8) . . ?
C80 C77 C73 111.6(7) . . ?
C78 C77 C73 109.0(8) . . ?
C79 C77 C73 109.5(8) . . ?
C96 C95 C99 109.9(9) . . ?
C96 C95 C100 124.4(10) . . ?
C99 C95 C100 125.5(10) . . ?
C96 C95 Fe04 71.5(5) . . ?
C99 C95 Fe04 72.3(5) . . ?
C100 C95 Fe04 126.2(7) . . ?
C7 C9 H9A 109.5 . . ?
C7 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C7 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C49 C50 H50A 109.5 . . ?
C49 C50 H50B 109.5 . . ?
H50A C50 H50B 109.5 . . ?
C49 C50 H50C 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C63 C66 H66A 109.5 . . ?
C63 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C63 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C98 C97 C96 108.8(9) . . ?
C98 C97 C102 125.2(10) . . ?
C96 C97 C102 125.9(11) . . ?
C98 C97 Fe04 71.1(6) . . ?
C96 C97 Fe04 69.4(6) . . ?
C102 C97 Fe04 128.6(7) . . ?
C35 C38 H38A 109.5 . . ?
C35 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C35 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C25 C27 H27A 109.5 . . ?
C25 C27 H27B 109.5 . . ?
H27A C27 H27B 109.5 . . ?
C25 C27 H27C 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C70 C67 C61 113.1(8) . . ?
C70 C67 C69 107.4(9) . . ?
C61 C67 C69 109.7(8) . . ?
C70 C67 C68 107.5(9) . . ?
C61 C67 C68 108.7(8) . . ?
C69 C67 C68 110.4(9) . . ?
C18 C17 C16 117.5(9) . . ?
C18 C17 C21 121.8(8) . . ?
C16 C17 C21 120.7(8) . . ?
C86 C87 C88 108.5(9) . . ?
C86 C87 C92 128.5(10) . . ?
C88 C87 C92 123.0(9) . . ?
C86 C87 Fe05 71.0(6) . . ?
C88 C87 Fe05 70.0(6) . . ?
C92 C87 Fe05 127.4(7) . . ?
C95 C99 C98 106.8(10) . . ?
C95 C99 C104 128.4(10) . . ?
C98 C99 C104 124.7(10) . . ?
C95 C99 Fe04 67.6(5) . . ?
C98 C99 Fe04 71.0(6) . . ?
C104 C99 Fe04 126.4(7) . . ?
C88 C89 C85 108.2(9) . . ?
C88 C89 C94 126.6(10) . . ?
C85 C89 C94 125.1(10) . . ?
C88 C89 Fe05 69.4(6) . . ?
C85 C89 Fe05 69.4(5) . . ?
C94 C89 Fe05 125.3(7) . . ?
C86 C85 C89 107.8(9) . . ?
C86 C85 C90 126.6(10) . . ?
C89 C85 C90 125.4(10) . . ?
C86 C85 Fe05 70.0(5) . . ?
C89 C85 Fe05 70.1(5) . . ?
C90 C85 Fe05 128.7(8) . . ?
C17 C18 C19 125.9(8) . . ?
C17 C18 H18 117.1 . . ?
C19 C18 H18 117.1 . . ?
C95 C96 C97 106.5(10) . . ?
C95 C96 C101 130.1(11) . . ?
C97 C96 C101 123.4(11) . . ?
C95 C96 Fe04 68.3(5) . . ?
C97 C96 Fe04 70.7(6) . . ?
C101 C96 Fe04 125.7(7) . . ?
C87 C86 C85 108.9(10) . . ?
C87 C86 C91 126.0(11) . . ?
C85 C86 C91 125.0(10) . . ?
C87 C86 Fe05 69.5(6) . . ?
C85 C86 Fe05 70.3(6) . . ?
C91 C86 Fe05 128.7(8) . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C67 C70 H70A 109.5 . . ?
C67 C70 H70B 109.5 . . ?
H70A C70 H70B 109.5 . . ?
C67 C70 H70C 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C77 C79 H79A 109.5 . . ?
C77 C79 H79B 109.5 . . ?
H79A C79 H79B 109.5 . . ?
C77 C79 H79C 109.5 . . ?
H79A C79 H79C 109.5 . . ?
H79B C79 H79C 109.5 . . ?
C67 C69 H69A 109.5 . . ?
C67 C69 H69B 109.5 . . ?
H69A C69 H69B 109.5 . . ?
C67 C69 H69C 109.5 . . ?
H69A C69 H69C 109.5 . . ?
H69B C69 H69C 109.5 . . ?
C49 C51 H51A 109.5 . . ?
C49 C51 H51B 109.5 . . ?
H51A C51 H51B 109.5 . . ?
C49 C51 H51C 109.5 . . ?
H51A C51 H51C 109.5 . . ?
H51B C51 H51C 109.5 . . ?
Si3 O8 Si4 143.7(9) . . ?
C89 C88 C87 106.5(10) . . ?
C89 C88 C93 126.5(10) . . ?
C87 C88 C93 126.7(9) . . ?
C89 C88 Fe05 70.7(6) . . ?
C87 C88 Fe05 68.8(6) . . ?
C93 C88 Fe05 129.4(8) . . ?
C99 C104 H10S 109.5 . . ?
C99 C104 H10T 109.5 . . ?
H10S C104 H10T 109.5 . . ?
C99 C104 H10U 109.5 . . ?
H10S C104 H10U 109.5 . . ?
H10T C104 H10U 109.5 . . ?
C89 C94 H94A 109.5 . . ?
C89 C94 H94B 109.5 . . ?
H94A C94 H94B 109.5 . . ?
C89 C94 H94C 109.5 . . ?
H94A C94 H94C 109.5 . . ?
H94B C94 H94C 109.5 . . ?
C6 C5 C4 116.1(10) . . ?
C6 C5 C11 120.9(11) . . ?
C4 C5 C11 122.9(10) . . ?
C87 C92 H92A 109.5 . . ?
C87 C92 H92B 109.5 . . ?
H92A C92 H92B 109.5 . . ?
C87 C92 H92C 109.5 . . ?
H92A C92 H92C 109.5 . . ?
H92B C92 H92C 109.5 . . ?
C7 C10 H10A 109.5 . . ?
C7 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C7 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C25 C28 H28A 109.5 . . ?
C25 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C25 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C77 C78 H78A 109.5 . . ?
C77 C78 H78B 109.5 . . ?
H78A C78 H78B 109.5 . . ?
C77 C78 H78C 109.5 . . ?
H78A C78 H78C 109.5 . . ?
H78B C78 H78C 109.5 . . ?
C95 C100 H10V 109.5 . . ?
C95 C100 H10W 109.5 . . ?
H10V C100 H10W 109.5 . . ?
C95 C100 H10X 109.5 . . ?
H10V C100 H10X 109.5 . . ?
H10W C100 H10X 109.5 . . ?
C86 C91 H91A 109.5 . . ?
C86 C91 H91B 109.5 . . ?
H91A C91 H91B 109.5 . . ?
C86 C91 H91C 109.5 . . ?
H91A C91 H91C 109.5 . . ?
H91B C91 H91C 109.5 . . ?
C88 C93 H93A 109.5 . . ?
C88 C93 H93B 109.5 . . ?
H93A C93 H93B 109.5 . . ?
C88 C93 H93C 109.5 . . ?
H93A C93 H93C 109.5 . . ?
H93B C93 H93C 109.5 . . ?
C67 C68 H68A 109.5 . . ?
C67 C68 H68B 109.5 . . ?
H68A C68 H68B 109.5 . . ?
C67 C68 H68C 109.5 . . ?
H68A C68 H68C 109.5 . . ?
H68B C68 H68C 109.5 . . ?
C22 C21 C23 112.4(10) . . ?
C22 C21 C17 108.1(10) . . ?
C23 C21 C17 110.7(10) . . ?
C22 C21 C24 108.5(12) . . ?
C23 C21 C24 106.0(11) . . ?
C17 C21 C24 111.2(9) . . ?
C98 C103 H10Y 109.5 . . ?
C98 C103 H 109.5 . . ?
H10Y C103 H 109.5 . . ?
C98 C103 HA 109.5 . . ?
H10Y C103 HA 109.5 . . ?
H C103 HA 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C77 C80 H80A 109.5 . . ?
C77 C80 H80B 109.5 . . ?
H80A C80 H80B 109.5 . . ?
C77 C80 H80C 109.5 . . ?
H80A C80 H80C 109.5 . . ?
H80B C80 H80C 109.5 . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C85 C90 H90A 109.5 . . ?
C85 C90 H90B 109.5 . . ?
H90A C90 H90B 109.5 . . ?
C85 C90 H90C 109.5 . . ?
H90A C90 H90C 109.5 . . ?
H90B C90 H90C 109.5 . . ?
C14 C11 C12 108.3(15) . . ?
C14 C11 C13 110.5(13) . . ?
C12 C11 C13 110.3(12) . . ?
C14 C11 C5 113.8(10) . . ?
C12 C11 C5 106.9(11) . . ?
C13 C11 C5 107.0(13) . . ?
C97 C102 H10Z 109.5 . . ?
C97 C102 HB 109.5 . . ?
H10Z C102 HB 109.5 . . ?
C97 C102 HC 109.5 . . ?
H10Z C102 HC 109.5 . . ?
HB C102 HC 109.5 . . ?
C96 C101 H10 109.5 . . ?
C96 C101 HD 109.5 . . ?
H10 C101 HD 109.5 . . ?
C96 C101 HE 109.5 . . ?
H10 C101 HE 109.5 . . ?
HD C101 HE 109.5 . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C11 C13 H13A 109.5 . . ?
C11 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C11 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
Si2 C108 H10D 109.5 . . ?
Si2 C108 H10E 109.5 . . ?
H10D C108 H10E 109.5 . . ?
Si2 C108 H10F 109.5 . . ?
H10D C108 H10F 109.5 . . ?
H10E C108 H10F 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
Si2 C109 H10G 109.5 . . ?
Si2 C109 H10H 109.5 . . ?
H10G C109 H10H 109.5 . . ?
Si2 C109 H10I 109.5 . . ?
H10G C109 H10I 109.5 . . ?
H10H C109 H10I 109.5 . . ?
Si1 C107 H10J 109.5 . . ?
Si1 C107 H10K 109.5 . . ?
H10J C107 H10K 109.5 . . ?
Si1 C107 H10L 109.5 . . ?
H10J C107 H10L 109.5 . . ?
H10K C107 H10L 109.5 . . ?
Si4 C116 H11D 109.5 . . ?
Si4 C116 H11E 109.5 . . ?
H11D C116 H11E 109.5 . . ?
Si4 C116 H11F 109.5 . . ?
H11D C116 H11F 109.5 . . ?
H11E C116 H11F 109.5 . . ?
Si2 C110 H11A 109.5 . . ?
Si2 C110 H11B 109.5 . . ?
H11A C110 H11B 109.5 . . ?
Si2 C110 H11C 109.5 . . ?
H11A C110 H11C 109.5 . . ?
H11B C110 H11C 109.5 . . ?
Si1 C106 H10M 109.5 . . ?
Si1 C106 H10N 109.5 . . ?
H10M C106 H10N 109.5 . . ?
Si1 C106 H10O 109.5 . . ?
H10M C106 H10O 109.5 . . ?
H10N C106 H10O 109.5 . . ?
Si1 C105 H10P 109.5 . . ?
Si1 C105 H10Q 109.5 . . ?
H10P C105 H10Q 109.5 . . ?
Si1 C105 H10R 109.5 . . ?
H10P C105 H10R 109.5 . . ?
H10Q C105 H10R 109.5 . . ?
Si4 C115 H11G 109.5 . . ?
Si4 C115 H11H 109.5 . . ?
H11G C115 H11H 109.5 . . ?
Si4 C115 H11I 109.5 . . ?
H11G C115 H11I 109.5 . . ?
H11H C115 H11I 109.5 . . ?
Si3 C112 H11J 109.5 . . ?
Si3 C112 H11K 109.5 . . ?
H11J C112 H11K 109.5 . . ?
Si3 C112 H11L 109.5 . . ?
H11J C112 H11L 109.5 . . ?
H11K C112 H11L 109.5 . . ?
Si3 C113 H11M 109.5 . . ?
Si3 C113 H11N 109.5 . . ?
H11M C113 H11N 109.5 . . ?
Si3 C113 H11O 109.5 . . ?
H11M C113 H11O 109.5 . . ?
H11N C113 H11O 109.5 . . ?
Si4 C114 H11P 109.5 . . ?
Si4 C114 H11Q 109.5 . . ?
H11P C114 H11Q 109.5 . . ?
Si4 C114 H11R 109.5 . . ?
H11P C114 H11R 109.5 . . ?
H11Q C114 H11R 109.5 . . ?
Si3 C111 H11S 109.5 . . ?
Si3 C111 H11T 109.5 . . ?
H11S C111 H11T 109.5 . . ?
Si3 C111 H11U 109.5 . . ?
H11S C111 H11U 109.5 . . ?
H11T C111 H11U 109.5 . . ?
Si1 O7 Si2 149.1(9) . . ?
C6 C1 C2 120.9(8) . . ?
C6 C1 P1 117.6(7) . . ?
C2 C1 P1 120.8(6) . . ?
C11 C14 H14A 109.5 . . ?
C11 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C11 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C81 C84A H84A 109.5 . . ?
C81 C84A H84B 109.5 . . ?
H84A C84A H84B 109.5 . . ?
C81 C84A H84C 109.5 . . ?
H84A C84A H84C 109.5 . . ?
H84B C84A H84C 109.5 . . ?
C81 C82A H82A 109.5 . . ?
C81 C82A H82B 109.5 . . ?
H82A C82A H82B 109.5 . . ?
C81 C82A H82C 109.5 . . ?
H82A C82A H82C 109.5 . . ?
H82B C82A H82C 109.5 . . ?
C81 C83A H83A 109.5 . . ?
C81 C83A H83B 109.5 . . ?
H83A C83A H83B 109.5 . . ?
C81 C83A H83C 109.5 . . ?
H83A C83A H83C 109.5 . . ?
H83B C83A H83C 109.5 . . ?
C81 C83B H83D 109.5 . . ?
C81 C83B H83E 109.5 . . ?
H83D C83B H83E 109.5 . . ?
C81 C83B H83F 109.5 . . ?
H83D C83B H83F 109.5 . . ?
H83E C83B H83F 109.5 . . ?
C81 C82B H82D 109.5 . . ?
C81 C82B H82E 109.5 . . ?
H82D C82B H82E 109.5 . . ?
C81 C82B H82F 109.5 . . ?
H82D C82B H82F 109.5 . . ?
H82E C82B H82F 109.5 . . ?
C81 C84B H84D 109.5 . . ?
C81 C84B H84E 109.5 . . ?
H84D C84B H84E 109.5 . . ?
C81 C84B H84F 109.5 . . ?
H84D C84B H84F 109.5 . . ?
H84E C84B H84F 109.5 . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N2 Ni1 O1 C2 -6.3(17) . . . . ?
N1 Ni1 O1 C2 24.8(7) . . . . ?
O4 Ni1 O1 C2 -153.6(7) . . . . ?
Ni3 Ni1 O1 C2 65.6(7) . . . . ?
Ni2 Ni1 O1 C2 -13.4(7) . . . . ?
O6 Ni3 O3 C30 -149.6(6) . . . . ?
N2 Ni3 O3 C30 49.0(17) . . . . ?
N1 Ni3 O3 C30 33.7(6) . . . . ?
Ni1 Ni3 O3 C30 -8.2(7) . . . . ?
Ni2 Ni3 O3 C30 71.7(6) . . . . ?
N2 Ni1 O4 C44 28.3(7) . . . . ?
O1 Ni1 O4 C44 -158.0(6) . . . . ?
Ni3 Ni1 O4 C44 -15.0(7) . . . . ?
Ni2 Ni1 O4 C44 64.3(7) . . . . ?
N2 Ni2 O5 C72 26.0(8) . . . . ?
O2 Ni2 O5 C72 -151.6(7) . . . . ?
Ni3 Ni2 O5 C72 63.9(8) . . . . ?
Ni1 Ni2 O5 C72 -8.9(8) . . . . ?
N2 Ni3 O6 C58 30.4(7) . . . . ?
O3 Ni3 O6 C58 -146.2(7) . . . . ?
Ni1 Ni3 O6 C58 72.7(7) . . . . ?
Ni2 Ni3 O6 C58 -8.1(7) . . . . ?
N1 Ni2 O2 C16 32.5(8) . . . . ?
N2 Ni2 O2 C16 46.2(19) . . . . ?
O5 Ni2 O2 C16 -146.7(8) . . . . ?
Ni3 Ni2 O2 C16 -3.0(9) . . . . ?
Ni1 Ni2 O2 C16 68.9(8) . . . . ?
C43 P2 N2 Ni1 -18.9(6) . . . . ?
C71 P2 N2 Ni1 102.6(5) . . . . ?
C57 P2 N2 Ni1 -138.7(4) . . . . ?
C43 P2 N2 Ni2 -146.0(4) . . . . ?
C71 P2 N2 Ni2 -24.4(6) . . . . ?
C57 P2 N2 Ni2 94.3(5) . . . . ?
C43 P2 N2 Ni3 92.9(5) . . . . ?
C71 P2 N2 Ni3 -145.5(4) . . . . ?
C57 P2 N2 Ni3 -26.9(6) . . . . ?
N1 Ni1 N2 P2 179.3(5) . . . . ?
O4 Ni1 N2 P2 -1.3(5) . . . . ?
O1 Ni1 N2 P2 -148.3(11) . . . . ?
Ni3 Ni1 N2 P2 130.2(6) . . . . ?
Ni2 Ni1 N2 P2 -139.9(6) . . . . ?
N1 Ni1 N2 Ni2 -40.8(3) . . . . ?
O4 Ni1 N2 Ni2 138.5(2) . . . . ?
O1 Ni1 N2 Ni2 -8.4(14) . . . . ?
Ni3 Ni1 N2 Ni2 -89.9(3) . . . . ?
N1 Ni1 N2 Ni3 49.1(2) . . . . ?
O4 Ni1 N2 Ni3 -131.5(2) . . . . ?
O1 Ni1 N2 Ni3 81.5(13) . . . . ?
Ni2 Ni1 N2 Ni3 89.9(3) . . . . ?
N1 Ni2 N2 P2 -178.3(5) . . . . ?
O2 Ni2 N2 P2 167.5(12) . . . . ?
O5 Ni2 N2 P2 0.5(5) . . . . ?
Ni3 Ni2 N2 P2 -135.6(6) . . . . ?
Ni1 Ni2 N2 P2 140.9(6) . . . . ?
N1 Ni2 N2 Ni1 40.9(3) . . . . ?
O2 Ni2 N2 Ni1 26.6(16) . . . . ?
O5 Ni2 N2 Ni1 -140.4(3) . . . . ?
Ni3 Ni2 N2 Ni1 83.6(3) . . . . ?
N1 Ni2 N2 Ni3 -42.7(3) . . . . ?
O2 Ni2 N2 Ni3 -56.9(16) . . . . ?
O5 Ni2 N2 Ni3 136.1(3) . . . . ?
Ni1 Ni2 N2 Ni3 -83.6(3) . . . . ?
O6 Ni3 N2 P2 1.6(5) . . . . ?
N1 Ni3 N2 P2 178.7(5) . . . . ?
O3 Ni3 N2 P2 162.8(12) . . . . ?
Ni1 Ni3 N2 P2 -132.4(6) . . . . ?
Ni2 Ni3 N2 P2 136.3(6) . . . . ?
O6 Ni3 N2 Ni1 134.0(2) . . . . ?
N1 Ni3 N2 Ni1 -48.9(3) . . . . ?
O3 Ni3 N2 Ni1 -64.8(15) . . . . ?
Ni2 Ni3 N2 Ni1 -91.3(3) . . . . ?
O6 Ni3 N2 Ni2 -134.7(3) . . . . ?
N1 Ni3 N2 Ni2 42.5(3) . . . . ?
O3 Ni3 N2 Ni2 26.5(16) . . . . ?
Ni1 Ni3 N2 Ni2 91.3(3) . . . . ?
C1 P1 N1 Ni1 -31.6(6) . . . . ?
C29 P1 N1 Ni1 88.1(5) . . . . ?
C15 P1 N1 Ni1 -149.3(4) . . . . ?
C1 P1 N1 Ni2 95.1(5) . . . . ?
C29 P1 N1 Ni2 -145.3(5) . . . . ?
C15 P1 N1 Ni2 -22.7(6) . . . . ?
C1 P1 N1 Ni3 -142.6(5) . . . . ?
C29 P1 N1 Ni3 -23.0(6) . . . . ?
C15 P1 N1 Ni3 99.6(5) . . . . ?
N2 Ni1 N1 P1 -179.1(5) . . . . ?
O1 Ni1 N1 P1 7.1(5) . . . . ?
Ni3 Ni1 N1 P1 -130.2(5) . . . . ?
Ni2 Ni1 N1 P1 139.9(6) . . . . ?
N2 Ni1 N1 Ni2 41.0(3) . . . . ?
O1 Ni1 N1 Ni2 -132.8(3) . . . . ?
Ni3 Ni1 N1 Ni2 89.9(3) . . . . ?
N2 Ni1 N1 Ni3 -49.0(3) . . . . ?
O1 Ni1 N1 Ni3 137.3(2) . . . . ?
Ni2 Ni1 N1 Ni3 -89.9(3) . . . . ?
N2 Ni2 N1 P1 179.1(6) . . . . ?
O2 Ni2 N1 P1 -3.5(5) . . . . ?
Ni3 Ni2 N1 P1 136.6(6) . . . . ?
Ni1 Ni2 N1 P1 -140.1(6) . . . . ?
N2 Ni2 N1 Ni1 -40.8(3) . . . . ?
O2 Ni2 N1 Ni1 136.6(3) . . . . ?
Ni3 Ni2 N1 Ni1 -83.3(3) . . . . ?
N2 Ni2 N1 Ni3 42.6(3) . . . . ?
O2 Ni2 N1 Ni3 -140.1(3) . . . . ?
Ni1 Ni2 N1 Ni3 83.3(3) . . . . ?
N2 Ni3 N1 P1 -179.9(6) . . . . ?
O3 Ni3 N1 P1 -2.8(5) . . . . ?
Ni1 Ni3 N1 P1 131.3(6) . . . . ?
Ni2 Ni3 N1 P1 -137.3(6) . . . . ?
N2 Ni3 N1 Ni1 48.8(3) . . . . ?
O3 Ni3 N1 Ni1 -134.2(2) . . . . ?
Ni2 Ni3 N1 Ni1 91.4(3) . . . . ?
N2 Ni3 N1 Ni2 -42.6(3) . . . . ?
O3 Ni3 N1 Ni2 134.5(3) . . . . ?
Ni1 Ni3 N1 Ni2 -91.4(3) . . . . ?
N2 P2 C43 C44 25.0(7) . . . . ?
C71 P2 C43 C44 -94.7(7) . . . . ?
C57 P2 C43 C44 144.2(6) . . . . ?
N2 P2 C43 C48 -158.9(5) . . . . ?
C71 P2 C43 C48 81.4(6) . . . . ?
C57 P2 C43 C48 -39.7(7) . . . . ?
C47 C46 C45 C44 2.8(12) . . . . ?
C47 C46 C45 C49 -177.2(8) . . . . ?
Ni1 O1 C2 C1 -21.9(11) . . . . ?
Ni1 O1 C2 C3 156.9(6) . . . . ?
Ni1 O4 C44 C43 -27.5(10) . . . . ?
Ni1 O4 C44 C45 154.1(6) . . . . ?
C48 C43 C44 O4 179.9(7) . . . . ?
P2 C43 C44 O4 -4.2(10) . . . . ?
C48 C43 C44 C45 -1.6(10) . . . . ?
P2 C43 C44 C45 174.2(5) . . . . ?
C46 C45 C44 O4 176.6(7) . . . . ?
C49 C45 C44 O4 -3.4(11) . . . . ?
C46 C45 C44 C43 -2.0(10) . . . . ?
C49 C45 C44 C43 178.1(7) . . . . ?
C45 C46 C47 C48 0.1(12) . . . . ?
C45 C46 C47 C53 -179.9(7) . . . . ?
C58 C59 C60 C61 -0.3(13) . . . . ?
C63 C59 C60 C61 178.3(8) . . . . ?
Ni2 O5 C72 C71 -19.3(13) . . . . ?
Ni2 O5 C72 C73 160.5(6) . . . . ?
C46 C47 C48 C43 -3.8(11) . . . . ?
C53 C47 C48 C43 176.2(7) . . . . ?
C44 C43 C48 C47 4.7(11) . . . . ?
P2 C43 C48 C47 -171.5(6) . . . . ?
N1 P1 C29 C34 -155.8(6) . . . . ?
C1 P1 C29 C34 -38.2(7) . . . . ?
C15 P1 C29 C34 83.2(7) . . . . ?
N1 P1 C29 C30 32.5(7) . . . . ?
C1 P1 C29 C30 150.0(6) . . . . ?
C15 P1 C29 C30 -88.5(7) . . . . ?
Ni3 O6 C58 C59 155.2(6) . . . . ?
Ni3 O6 C58 C57 -26.8(11) . . . . ?
C60 C59 C58 O6 -178.9(7) . . . . ?
C63 C59 C58 O6 2.5(11) . . . . ?
C60 C59 C58 C57 3.0(11) . . . . ?
C63 C59 C58 C57 -175.6(7) . . . . ?
O5 C72 C71 C76 173.6(8) . . . . ?
C73 C72 C71 C76 -6.2(12) . . . . ?
O5 C72 C71 P2 -16.2(12) . . . . ?
C73 C72 C71 P2 163.9(6) . . . . ?
N2 P2 C71 C72 35.7(8) . . . . ?
C43 P2 C71 C72 155.5(7) . . . . ?
C57 P2 C71 C72 -82.9(7) . . . . ?
N2 P2 C71 C76 -153.8(6) . . . . ?
C43 P2 C71 C76 -33.9(8) . . . . ?
C57 P2 C71 C76 87.6(7) . . . . ?
Ni3 O3 C30 C29 -30.6(10) . . . . ?
Ni3 O3 C30 C31 149.1(6) . . . . ?
C34 C29 C30 O3 -179.0(7) . . . . ?
P1 C29 C30 O3 -7.7(11) . . . . ?
C34 C29 C30 C31 1.3(11) . . . . ?
P1 C29 C30 C31 172.6(6) . . . . ?
N1 P1 C15 C20 -151.4(7) . . . . ?
C1 P1 C15 C20 92.5(8) . . . . ?
C29 P1 C15 C20 -29.5(8) . . . . ?
N1 P1 C15 C16 36.2(8) . . . . ?
C1 P1 C15 C16 -80.0(8) . . . . ?
C29 P1 C15 C16 158.1(7) . . . . ?
C48 C47 C53 C55 -116.6(9) . . . . ?
C46 C47 C53 C55 63.4(10) . . . . ?
C48 C47 C53 C56 2.6(11) . . . . ?
C46 C47 C53 C56 -177.3(7) . . . . ?
C48 C47 C53 C54 122.7(8) . . . . ?
C46 C47 C53 C54 -57.3(10) . . . . ?
C60 C59 C63 C64 -117.9(8) . . . . ?
C58 C59 C63 C64 60.8(9) . . . . ?
C60 C59 C63 C65 120.3(8) . . . . ?
C58 C59 C63 C65 -61.1(9) . . . . ?
C60 C59 C63 C66 2.0(11) . . . . ?
C58 C59 C63 C66 -179.4(7) . . . . ?
C30 C29 C34 C33 -1.1(12) . . . . ?
P1 C29 C34 C33 -172.6(6) . . . . ?
C33 C32 C31 C30 3.9(13) . . . . ?
C33 C32 C31 C35 -178.2(8) . . . . ?
O3 C30 C31 C32 177.7(7) . . . . ?
C29 C30 C31 C32 -2.6(11) . . . . ?
O3 C30 C31 C35 -0.2(11) . . . . ?
C29 C30 C31 C35 179.5(7) . . . . ?
C72 C71 C76 C75 3.4(13) . . . . ?
P2 C71 C76 C75 -167.1(7) . . . . ?
C61 C62 C57 C58 2.8(12) . . . . ?
C61 C62 C57 P2 -168.6(6) . . . . ?
O6 C58 C57 C62 177.7(7) . . . . ?
C59 C58 C57 C62 -4.3(11) . . . . ?
O6 C58 C57 P2 -11.3(10) . . . . ?
C59 C58 C57 P2 166.8(6) . . . . ?
N2 P2 C57 C62 -153.2(6) . . . . ?
C43 P2 C57 C62 87.6(6) . . . . ?
C71 P2 C57 C62 -35.0(7) . . . . ?
N2 P2 C57 C58 35.5(7) . . . . ?
C43 P2 C57 C58 -83.7(7) . . . . ?
C71 P2 C57 C58 153.7(6) . . . . ?
C29 C34 C33 C32 2.1(11) . . . . ?
C29 C34 C33 C39 178.2(7) . . . . ?
C31 C32 C33 C34 -3.6(12) . . . . ?
C31 C32 C33 C39 -179.9(8) . . . . ?
C57 C62 C61 C60 0.0(12) . . . . ?
C57 C62 C61 C67 178.7(8) . . . . ?
C59 C60 C61 C62 -1.3(13) . . . . ?
C59 C60 C61 C67 180.0(8) . . . . ?
O1 C2 C3 C4 -177.7(9) . . . . ?
C1 C2 C3 C4 1.2(13) . . . . ?
O1 C2 C3 C7 7.1(12) . . . . ?
C1 C2 C3 C7 -174.1(8) . . . . ?
C46 C45 C49 C52 4.3(11) . . . . ?
C44 C45 C49 C52 -175.7(7) . . . . ?
C46 C45 C49 C51 123.2(8) . . . . ?
C44 C45 C49 C51 -56.9(10) . . . . ?
C46 C45 C49 C50 -115.4(8) . . . . ?
C44 C45 C49 C50 64.5(9) . . . . ?
Ni2 O2 C16 C17 158.8(8) . . . . ?
Ni2 O2 C16 C15 -24.8(14) . . . . ?
C20 C15 C16 O2 173.2(9) . . . . ?
P1 C15 C16 O2 -14.9(13) . . . . ?
C20 C15 C16 C17 -10.4(14) . . . . ?
P1 C15 C16 C17 161.6(8) . . . . ?
C34 C33 C39 C40 2.3(12) . . . . ?
C32 C33 C39 C40 178.4(8) . . . . ?
C34 C33 C39 C42 123.2(9) . . . . ?
C32 C33 C39 C42 -60.8(10) . . . . ?
C34 C33 C39 C41 -118.0(9) . . . . ?
C32 C33 C39 C41 58.0(10) . . . . ?
C32 C31 C35 C36 -112.5(9) . . . . ?
C30 C31 C35 C36 65.4(10) . . . . ?
C32 C31 C35 C38 4.7(12) . . . . ?
C30 C31 C35 C38 -177.5(8) . . . . ?
C32 C31 C35 C37 123.9(9) . . . . ?
C30 C31 C35 C37 -58.3(10) . . . . ?
C71 C76 C75 C74 0.6(14) . . . . ?
C71 C76 C75 C81 179.2(8) . . . . ?
C18 C19 C20 C15 3.5(15) . . . . ?
C25 C19 C20 C15 179.6(10) . . . . ?
C16 C15 C20 C19 3.7(15) . . . . ?
P1 C15 C20 C19 -168.6(8) . . . . ?
C74 C75 C81 C82B 110(3) . . . . ?
C76 C75 C81 C82B -68(3) . . . . ?
C74 C75 C81 C84A -62.0(13) . . . . ?
C76 C75 C81 C84A 119.5(11) . . . . ?
C74 C75 C81 C83B -125(2) . . . . ?
C76 C75 C81 C83B 57(2) . . . . ?
C74 C75 C81 C83A 174.3(11) . . . . ?
C76 C75 C81 C83A -4.2(15) . . . . ?
C74 C75 C81 C82A 56.5(13) . . . . ?
C76 C75 C81 C82A -122.0(11) . . . . ?
C74 C75 C81 C84B -10(3) . . . . ?
C76 C75 C81 C84B 171(3) . . . . ?
C4 C3 C7 C9 -120.4(10) . . . . ?
C2 C3 C7 C9 54.8(11) . . . . ?
C4 C3 C7 C8 118.6(10) . . . . ?
C2 C3 C7 C8 -66.2(10) . . . . ?
C4 C3 C7 C10 0.1(13) . . . . ?
C2 C3 C7 C10 175.3(8) . . . . ?
O5 C72 C73 C74 -174.6(8) . . . . ?
C71 C72 C73 C74 5.3(13) . . . . ?
O5 C72 C73 C77 7.0(13) . . . . ?
C71 C72 C73 C77 -173.2(8) . . . . ?
C72 C73 C74 C75 -1.6(15) . . . . ?
C77 C73 C74 C75 176.9(10) . . . . ?
C76 C75 C74 C73 -1.5(15) . . . . ?
C81 C75 C74 C73 179.9(9) . . . . ?
C20 C19 C25 C27 120.9(11) . . . . ?
C18 C19 C25 C27 -63.3(14) . . . . ?
C20 C19 C25 C26 -118.1(11) . . . . ?
C18 C19 C25 C26 57.7(14) . . . . ?
C20 C19 C25 C28 1.4(17) . . . . ?
C18 C19 C25 C28 177.2(11) . . . . ?
C2 C3 C4 C5 3.6(17) . . . . ?
C7 C3 C4 C5 178.8(11) . . . . ?
C74 C73 C77 C80 -2.5(14) . . . . ?
C72 C73 C77 C80 176.0(9) . . . . ?
C74 C73 C77 C78 -122.1(10) . . . . ?
C72 C73 C77 C78 56.3(12) . . . . ?
C74 C73 C77 C79 115.6(10) . . . . ?
C72 C73 C77 C79 -66.0(11) . . . . ?
C99 C98 C97 C96 0.4(11) . . . . ?
C103 C98 C97 C96 -179.0(9) . . . . ?
Fe04 C98 C97 C96 59.4(7) . . . . ?
C99 C98 C97 C102 176.6(9) . . . . ?
C103 C98 C97 C102 -2.7(16) . . . . ?
Fe04 C98 C97 C102 -124.4(10) . . . . ?
C99 C98 C97 Fe04 -59.0(6) . . . . ?
C103 C98 C97 Fe04 121.7(10) . . . . ?
C62 C61 C67 C70 -3.0(13) . . . . ?
C60 C61 C67 C70 175.7(9) . . . . ?
C62 C61 C67 C69 -122.9(10) . . . . ?
C60 C61 C67 C69 55.8(12) . . . . ?
C62 C61 C67 C68 116.4(10) . . . . ?
C60 C61 C67 C68 -65.0(12) . . . . ?
O2 C16 C17 C18 -173.8(10) . . . . ?
C15 C16 C17 C18 9.6(15) . . . . ?
O2 C16 C17 C21 6.9(16) . . . . ?
C15 C16 C17 C21 -169.7(11) . . . . ?
C96 C95 C99 C98 -1.5(10) . . . . ?
C100 C95 C99 C98 -177.3(9) . . . . ?
Fe04 C95 C99 C98 60.4(6) . . . . ?
C96 C95 C99 C104 178.5(9) . . . . ?
C100 C95 C99 C104 2.8(15) . . . . ?
Fe04 C95 C99 C104 -119.5(10) . . . . ?
C96 C95 C99 Fe04 -61.9(6) . . . . ?
C100 C95 C99 Fe04 122.3(9) . . . . ?
C97 C98 C99 C95 0.7(10) . . . . ?
C103 C98 C99 C95 180.0(9) . . . . ?
Fe04 C98 C99 C95 -58.3(6) . . . . ?
C97 C98 C99 C104 -179.4(9) . . . . ?
C103 C98 C99 C104 0.0(15) . . . . ?
Fe04 C98 C99 C104 121.7(9) . . . . ?
C97 C98 C99 Fe04 58.9(6) . . . . ?
C103 C98 C99 Fe04 -121.7(10) . . . . ?
C88 C89 C85 C86 1.4(12) . . . . ?
C94 C89 C85 C86 179.6(9) . . . . ?
Fe05 C89 C85 C86 60.2(7) . . . . ?
C88 C89 C85 C90 177.3(10) . . . . ?
C94 C89 C85 C90 -4.5(17) . . . . ?
Fe05 C89 C85 C90 -123.9(11) . . . . ?
C88 C89 C85 Fe05 -58.7(7) . . . . ?
C94 C89 C85 Fe05 119.4(10) . . . . ?
C16 C17 C18 C19 -2.8(18) . . . . ?
C21 C17 C18 C19 176.4(12) . . . . ?
C20 C19 C18 C17 -3.9(17) . . . . ?
C25 C19 C18 C17 179.9(11) . . . . ?
C99 C95 C96 C97 1.7(10) . . . . ?
C100 C95 C96 C97 177.6(8) . . . . ?
Fe04 C95 C96 C97 -60.7(6) . . . . ?
C99 C95 C96 C101 -178.5(10) . . . . ?
C100 C95 C96 C101 -2.7(16) . . . . ?
Fe04 C95 C96 C101 119.0(11) . . . . ?
C99 C95 C96 Fe04 62.5(6) . . . . ?
C100 C95 C96 Fe04 -121.7(9) . . . . ?
C98 C97 C96 C95 -1.3(10) . . . . ?
C102 C97 C96 C95 -177.5(9) . . . . ?
Fe04 C97 C96 C95 59.2(6) . . . . ?
C98 C97 C96 C101 179.0(9) . . . . ?
C102 C97 C96 C101 2.8(16) . . . . ?
Fe04 C97 C96 C101 -120.6(10) . . . . ?
C98 C97 C96 Fe04 -60.4(7) . . . . ?
C102 C97 C96 Fe04 123.4(10) . . . . ?
C88 C87 C86 C85 0.7(12) . . . . ?
C92 C87 C86 C85 177.4(10) . . . . ?
Fe05 C87 C86 C85 -59.4(7) . . . . ?
C88 C87 C86 C91 -176.3(10) . . . . ?
C92 C87 C86 C91 0.4(17) . . . . ?
Fe05 C87 C86 C91 123.5(10) . . . . ?
C88 C87 C86 Fe05 60.2(7) . . . . ?
C92 C87 C86 Fe05 -123.2(11) . . . . ?
C89 C85 C86 C87 -1.3(12) . . . . ?
C90 C85 C86 C87 -177.2(10) . . . . ?
Fe05 C85 C86 C87 58.9(7) . . . . ?
C89 C85 C86 C91 175.7(10) . . . . ?
C90 C85 C86 C91 -0.1(18) . . . . ?
Fe05 C85 C86 C91 -124.0(11) . . . . ?
C89 C85 C86 Fe05 -60.2(7) . . . . ?
C90 C85 C86 Fe05 123.9(11) . . . . ?
C111 Si3 O8 Si4 57(3) . . . . ?
C113 Si3 O8 Si4 166(2) . . . . ?
C112 Si3 O8 Si4 -73.9(18) . . . . ?
C115 Si4 O8 Si3 49.8(19) . . . . ?
C114 Si4 O8 Si3 167.8(16) . . . . ?
C116 Si4 O8 Si3 -74.4(15) . . . . ?
C85 C89 C88 C87 -1.0(11) . . . . ?
C94 C89 C88 C87 -179.1(9) . . . . ?
Fe05 C89 C88 C87 -59.7(7) . . . . ?
C85 C89 C88 C93 -176.0(10) . . . . ?
C94 C89 C88 C93 5.9(17) . . . . ?
Fe05 C89 C88 C93 125.2(11) . . . . ?
C85 C89 C88 Fe05 58.7(7) . . . . ?
C94 C89 C88 Fe05 -119.4(10) . . . . ?
C86 C87 C88 C89 0.2(11) . . . . ?
C92 C87 C88 C89 -176.7(9) . . . . ?
Fe05 C87 C88 C89 61.0(7) . . . . ?
C86 C87 C88 C93 175.2(10) . . . . ?
C92 C87 C88 C93 -1.7(16) . . . . ?
Fe05 C87 C88 C93 -124.0(11) . . . . ?
C86 C87 C88 Fe05 -60.8(7) . . . . ?
C92 C87 C88 Fe05 122.3(10) . . . . ?
C1 C6 C5 C4 1.7(17) . . . . ?
C1 C6 C5 C11 -179.1(11) . . . . ?
C3 C4 C5 C6 -5.0(19) . . . . ?
C3 C4 C5 C11 175.8(12) . . . . ?
C18 C17 C21 C22 -122.4(12) . . . . ?
C16 C17 C21 C22 56.8(15) . . . . ?
C18 C17 C21 C23 114.1(12) . . . . ?
C16 C17 C21 C23 -66.7(14) . . . . ?
C18 C17 C21 C24 -3.5(18) . . . . ?
C16 C17 C21 C24 175.8(12) . . . . ?
C6 C5 C11 C14 0(2) . . . . ?
C4 C5 C11 C14 178.8(15) . . . . ?
C6 C5 C11 C12 119.2(14) . . . . ?
C4 C5 C11 C12 -61.7(19) . . . . ?
C6 C5 C11 C13 -122.7(13) . . . . ?
C4 C5 C11 C13 56.4(16) . . . . ?
C107 Si1 O7 Si2 131(3) . . . . ?
C105 Si1 O7 Si2 7(3) . . . . ?
C106 Si1 O7 Si2 -112(3) . . . . ?
C108 Si2 O7 Si1 -162(2) . . . . ?
C109 Si2 O7 Si1 -41(3) . . . . ?
C110 Si2 O7 Si1 73(3) . . . . ?
C5 C6 C1 C2 2.7(15) . . . . ?
C5 C6 C1 P1 -168.5(9) . . . . ?
O1 C2 C1 C6 174.7(8) . . . . ?
C3 C2 C1 C6 -4.1(12) . . . . ?
O1 C2 C1 P1 -14.4(12) . . . . ?
C3 C2 C1 P1 166.8(6) . . . . ?
N1 P1 C1 C6 -150.7(7) . . . . ?
C29 P1 C1 C6 89.5(8) . . . . ?
C15 P1 C1 C6 -33.2(9) . . . . ?
N1 P1 C1 C2 38.1(8) . . . . ?
C29 P1 C1 C2 -81.7(7) . . . . ?
C15 P1 C1 C2 155.6(7) . . . . ?
_refine_diff_density_max 1.261
_refine_diff_density_min -1.372
_refine_diff_density_rms 0.138
_shelx_res_file
;
TITL d19106_a.res in P2(1)/c
d19106.res
created by SHELXL-2018/3 at 12:08:55 on 02-Jul-2020
REM Old TITL d19106 in P2(1)/c
REM SHELXT solution in P2(1)/c
REM R1 0.358, Rweak 0.096, Alpha 0.127, Orientation as input
REM Formula found by SHELXT: C124 Br4
CELL 0.71073 25.1009 30.7719 18.5385 90 100.85 90
ZERR 4 0.0087 0.0121 0.0073 0 0.025 0
LATT 1
SYMM -X,0.5+Y,0.5-Z
SFAC C H Fe N Ni O P Si
UNIT 451.34 706.01 4 8 12 29.89 8 11.78
RIGU O8 Si4 C116 C115 C114 Si3 C112 C113 C111
ISOR 0.025 0.05 C82B C84B C83B
L.S. 6
PLAN 21
TEMP -173.15
CONF
list 4
MORE -1
BOND $H
ABIN
fmap -2
acta
OMIT 0 1 1
OMIT -1 1 1
OMIT 1 1 1
OMIT 0 4 0
REM
REM
REM
WGHT 0.015300 301.756805
FVAR 0.06638 0.83831 0.71772 0.75084
NI3 5 0.206023 0.623878 0.522061 11.00000 0.02345 0.01406 =
0.01628 0.00012 0.00584 -0.00095
NI2 5 0.253232 0.547511 0.519462 11.00000 0.03215 0.01529 =
0.01665 0.00139 0.00550 0.00076
NI1 5 0.306365 0.622467 0.541354 11.00000 0.02288 0.01665 =
0.01458 0.00019 0.00421 0.00056
FE04 3 0.000000 0.500000 0.500000 10.50000 0.03463 0.02242 =
0.05031 0.00015 0.01306 -0.01664
FE05 3 0.500000 0.500000 0.500000 10.50000 0.03510 0.04481 =
0.04663 0.00085 0.01364 0.01997
P2 7 0.249106 0.604153 0.379454 11.00000 0.02364 0.01100 =
0.01794 0.00088 0.00487 0.00028
P1 7 0.260060 0.587791 0.674211 11.00000 0.03445 0.01341 =
0.01650 0.00237 0.00712 0.00121
SI2 8 0.098692 0.410680 0.056309 41.00000 0.05121 0.06711 =
0.06017 0.00206 0.01155 -0.02812
SI1 8 0.030254 0.381700 0.170226 41.00000 0.06130 0.05877 =
0.07078 -0.02205 0.03489 -0.02994
O1 6 0.357214 0.635842 0.626582 11.00000 0.02315 0.03042 =
0.01064 -0.00052 -0.00347 0.00467
O3 6 0.163512 0.641171 0.590259 11.00000 0.03749 0.00939 =
0.01854 0.00056 0.01004 -0.00113
O4 6 0.348065 0.649052 0.481082 11.00000 0.01974 0.02610 =
0.02070 0.00164 0.00458 0.00531
O5 6 0.246822 0.509068 0.438772 11.00000 0.04512 0.01900 =
0.02340 -0.00126 0.01566 -0.00077
O6 6 0.158586 0.649702 0.444850 11.00000 0.02871 0.02203 =
0.01806 -0.00137 0.01092 0.00352
O2 6 0.257096 0.501512 0.587621 11.00000 0.04956 0.01610 =
0.02920 0.00230 0.01570 0.00375
N2 4 0.253745 0.599341 0.467753 11.00000 0.02242 0.01879 =
0.01641 0.00172 0.00661 0.00278
SI4 8 -0.118834 0.750256 0.461013 31.00000 0.04309 0.05852 =
0.14009 -0.03529 0.02378 -0.01081
N1 4 0.257854 0.592463 0.587169 11.00000 0.03042 0.00774 =
0.02989 -0.00036 0.01164 0.00781
C43 1 0.288760 0.649150 0.361596 11.00000 0.01470 0.01813 =
0.01772 -0.00733 0.00743 0.00515
C46 1 0.351580 0.713253 0.317402 11.00000 0.01652 0.01652 =
0.02828 -0.00371 0.00782 -0.00477
AFIX 43
H46 2 0.373946 0.734824 0.301669 11.00000 -1.20000
AFIX 0
C45 1 0.365248 0.698869 0.388926 11.00000 0.01875 0.02251 =
0.01785 0.00157 0.00327 0.00732
C2 1 0.367450 0.616429 0.689942 11.00000 0.03004 0.01689 =
0.01992 0.00652 0.00414 0.00852
C44 1 0.333641 0.664885 0.413118 11.00000 0.01710 0.01070 =
0.01632 0.00042 -0.00138 0.00801
C59 1 0.094557 0.650863 0.332225 11.00000 0.02689 0.01300 =
0.02275 0.00102 0.00736 -0.00312
SI3 8 -0.158551 0.763338 0.603963 31.00000 0.13242 0.08000 =
0.10361 0.00177 0.03952 -0.06443
C47 1 0.306798 0.698205 0.266064 11.00000 0.02457 0.01822 =
0.02132 0.00017 0.00516 -0.00143
C60 1 0.081075 0.637528 0.260812 11.00000 0.03029 0.02203 =
0.03303 0.00307 0.00361 -0.00990
AFIX 43
H60 2 0.046984 0.646693 0.233698 11.00000 -1.20000
AFIX 0
C72 1 0.261531 0.514206 0.375905 11.00000 0.03008 0.01016 =
0.02696 -0.00449 0.00683 -0.00644
C32 1 0.166206 0.690594 0.767946 11.00000 0.01129 0.02589 =
0.02919 -0.00516 0.00550 -0.00245
AFIX 43
H32 2 0.144804 0.710208 0.789989 11.00000 -1.20000
AFIX 0
C48 1 0.274760 0.667144 0.289391 11.00000 0.02495 0.01758 =
0.02472 -0.00350 0.00665 -0.00151
AFIX 43
H48 2 0.242930 0.657469 0.257267 11.00000 -1.20000
AFIX 0
C29 1 0.225243 0.631857 0.706978 11.00000 0.03194 0.00527 =
0.01282 -0.00136 0.00746 -0.00110
C58 1 0.144447 0.637968 0.374752 11.00000 0.03975 0.01393 =
0.01937 0.00114 0.00729 -0.00642
C62 1 0.162459 0.599558 0.264008 11.00000 0.03076 0.02011 =
0.01877 -0.00311 0.00658 -0.01014
AFIX 43
H62 2 0.185750 0.581901 0.241525 11.00000 -1.20000
AFIX 0
C71 1 0.271943 0.554904 0.345029 11.00000 0.03507 0.01231 =
0.00882 -0.00120 0.00138 -0.00029
C30 1 0.179985 0.650581 0.661120 11.00000 0.02895 0.01151 =
0.02240 0.00198 0.00643 -0.00450
C15 1 0.231161 0.536624 0.691826 11.00000 0.03182 0.01561 =
0.02478 0.01017 0.01039 -0.00192
C53 1 0.295100 0.716102 0.188167 11.00000 0.02950 0.01605 =
0.01868 0.00345 0.00444 -0.00409
C63 1 0.056543 0.680400 0.365643 11.00000 0.01978 0.02161 =
0.02037 -0.00299 -0.00168 0.00116
C34 1 0.240246 0.642341 0.781054 11.00000 0.02432 0.01670 =
0.02078 0.00488 0.00623 -0.00132
AFIX 43
H34 2 0.270785 0.628325 0.809708 11.00000 -1.20000
AFIX 0
C31 1 0.150204 0.682318 0.694770 11.00000 0.02805 0.02290 =
0.01859 -0.00416 0.00655 0.00407
C76 1 0.293182 0.557508 0.279045 11.00000 0.02840 0.02463 =
0.02361 0.00288 0.00831 0.00520
AFIX 43
H76 2 0.301583 0.585125 0.261188 11.00000 -1.20000
AFIX 0
C57 1 0.179612 0.612867 0.338008 11.00000 0.02366 0.01206 =
0.01554 -0.00017 0.00148 -0.00952
C33 1 0.212319 0.672164 0.813589 11.00000 0.02103 0.02922 =
0.01505 -0.00247 0.00620 -0.00042
C54 1 0.288091 0.765879 0.188556 11.00000 0.02831 0.01942 =
0.03614 0.00999 0.00570 0.00829
AFIX 137
H54A 2 0.254948 0.773149 0.206688 11.00000 -1.50000
H54B 2 0.285446 0.777109 0.138540 11.00000 -1.50000
H54C 2 0.319424 0.779014 0.220688 11.00000 -1.50000
AFIX 0
C61 1 0.113106 0.611614 0.224373 11.00000 0.03894 0.02874 =
0.01194 -0.00265 0.00183 -0.00798
C6 1 0.345072 0.565626 0.783254 11.00000 0.04851 0.05648 =
0.02282 0.01321 0.00990 0.01194
AFIX 43
H6 2 0.319784 0.546383 0.798600 11.00000 -1.20000
AFIX 0
C64 1 0.085015 0.723492 0.388761 11.00000 0.02458 0.03209 =
0.02120 0.00279 0.00383 -0.00828
AFIX 137
H64A 2 0.117475 0.718071 0.426194 11.00000 -1.50000
H64B 2 0.060313 0.742666 0.408968 11.00000 -1.50000
H64C 2 0.095508 0.737360 0.345939 11.00000 -1.50000
AFIX 0
C3 1 0.419544 0.621618 0.737367 11.00000 0.02457 0.04857 =
0.02046 -0.00313 0.00476 0.00380
C49 1 0.413913 0.719323 0.441417 11.00000 0.01805 0.05014 =
0.01525 -0.00604 0.00137 -0.01420
C42 1 0.236455 0.733617 0.903173 11.00000 0.03092 0.04087 =
0.02295 -0.01428 0.00279 -0.00834
AFIX 137
H42A 2 0.267470 0.741353 0.880606 11.00000 -1.50000
H42B 2 0.244272 0.741500 0.955318 11.00000 -1.50000
H42C 2 0.204192 0.749348 0.878456 11.00000 -1.50000
AFIX 0
C19 1 0.191756 0.495486 0.780097 11.00000 0.05899 0.02342 =
0.02402 0.01027 0.01158 -0.00456
C16 1 0.239186 0.499488 0.649726 11.00000 0.05323 0.01856 =
0.02272 0.00497 0.00593 0.00289
C39 1 0.226070 0.684062 0.895490 11.00000 0.03638 0.03424 =
0.01077 -0.00441 0.00186 -0.00633
C35 1 0.100845 0.704603 0.649213 11.00000 0.01084 0.03270 =
0.02870 -0.00462 -0.00532 -0.00001
C75 1 0.301683 0.520655 0.240887 11.00000 0.05270 0.02377 =
0.02316 -0.00534 0.01376 0.00571
C20 1 0.206780 0.534629 0.753877 11.00000 0.04802 0.01556 =
0.02854 -0.00291 0.00936 -0.01418
AFIX 43
H20 2 0.200506 0.560751 0.778285 11.00000 -1.20000
AFIX 0
C65 1 0.038948 0.658340 0.432325 11.00000 0.04080 0.03326 =
0.01791 -0.00374 0.00280 -0.00893
AFIX 137
H65A 2 0.017508 0.632343 0.415930 11.00000 -1.50000
H65B 2 0.016978 0.678642 0.455105 11.00000 -1.50000
H65C 2 0.071202 0.650051 0.468214 11.00000 -1.50000
AFIX 0
C81 1 0.324158 0.523784 0.168443 11.00000 0.04779 0.02963 =
0.02263 -0.00992 0.01716 -0.00428
C37 1 0.115765 0.728613 0.583229 11.00000 0.01409 0.03344 =
0.02290 -0.00713 -0.00733 0.00650
AFIX 137
H37A 2 0.149497 0.744884 0.599102 11.00000 -1.50000
H37B 2 0.086553 0.748784 0.562959 11.00000 -1.50000
H37C 2 0.120773 0.707503 0.545488 11.00000 -1.50000
AFIX 0
C7 1 0.460332 0.653937 0.717292 11.00000 0.01478 0.05528 =
0.02557 -0.00643 -0.00822 0.01737
C55 1 0.342071 0.704520 0.149666 11.00000 0.04346 0.02702 =
0.02653 0.00461 0.01672 -0.00614
AFIX 137
H55A 2 0.375882 0.716676 0.177411 11.00000 -1.50000
H55B 2 0.335069 0.716622 0.099879 11.00000 -1.50000
H55C 2 0.345333 0.672848 0.147060 11.00000 -1.50000
AFIX 0
C40 1 0.275256 0.660336 0.934890 11.00000 0.05794 0.05044 =
0.01138 -0.00750 0.00192 -0.00375
AFIX 137
H40A 2 0.267948 0.629034 0.933608 11.00000 -1.50000
H40B 2 0.283925 0.670167 0.986042 11.00000 -1.50000
H40C 2 0.306020 0.666312 0.910755 11.00000 -1.50000
AFIX 0
C73 1 0.268549 0.476415 0.331818 11.00000 0.04085 0.01794 =
0.03230 -0.00073 0.01118 -0.00094
C74 1 0.288423 0.481538 0.268452 11.00000 0.04642 0.01901 =
0.02702 -0.01105 0.01362 0.00041
AFIX 43
H74 2 0.293419 0.456083 0.241499 11.00000 -1.20000
AFIX 0
C36 1 0.055646 0.671597 0.624310 11.00000 0.02129 0.04218 =
0.03080 -0.00263 0.00309 -0.01591
AFIX 137
H36A 2 0.068772 0.648907 0.594925 11.00000 -1.50000
H36B 2 0.024402 0.686290 0.594586 11.00000 -1.50000
H36C 2 0.044774 0.658427 0.667447 11.00000 -1.50000
AFIX 0
C25 1 0.165771 0.491368 0.846848 11.00000 0.08485 0.03345 =
0.03707 0.00533 0.02860 -0.01690
C56 1 0.242733 0.696394 0.143373 11.00000 0.04043 0.03336 =
0.02051 0.01409 0.00128 0.00042
AFIX 137
H56A 2 0.247570 0.665041 0.137929 11.00000 -1.50000
H56B 2 0.234774 0.709992 0.094729 11.00000 -1.50000
H56C 2 0.212550 0.701615 0.168972 11.00000 -1.50000
AFIX 0
C98 1 0.069775 0.537570 0.491085 11.00000 0.04108 0.02219 =
0.07057 -0.00555 0.02579 -0.01532
C41 1 0.177112 0.672225 0.931806 11.00000 0.04135 0.03602 =
0.02595 -0.00515 0.01348 -0.00365
AFIX 137
H41A 2 0.144623 0.687318 0.906196 11.00000 -1.50000
H41B 2 0.184758 0.681113 0.983488 11.00000 -1.50000
H41C 2 0.171033 0.640767 0.928670 11.00000 -1.50000
AFIX 0
C4 1 0.430273 0.599897 0.802233 11.00000 0.02209 0.08993 =
0.02932 0.01457 0.00048 0.01475
AFIX 43
H4 2 0.464202 0.605365 0.833420 11.00000 -1.20000
AFIX 0
C52 1 0.439369 0.757091 0.406674 11.00000 0.03160 0.04646 =
0.03485 -0.00154 0.00316 -0.01381
AFIX 137
H52A 2 0.456253 0.746175 0.366681 11.00000 -1.50000
H52B 2 0.466982 0.771039 0.443881 11.00000 -1.50000
H52C 2 0.411221 0.778312 0.387148 11.00000 -1.50000
AFIX 0
C77 1 0.251941 0.430892 0.356524 11.00000 0.06476 0.01702 =
0.03446 -0.00177 0.02648 0.00233
C95 1 -0.008403 0.564655 0.521624 11.00000 0.03869 0.00368 =
0.06896 0.00138 0.01236 -0.00030
C9 1 0.436365 0.699186 0.704830 11.00000 0.02662 0.04880 =
0.05460 -0.02423 0.00816 0.00781
AFIX 137
H9A 2 0.405997 0.698691 0.662987 11.00000 -1.50000
H9B 2 0.464234 0.719341 0.694557 11.00000 -1.50000
H9C 2 0.423384 0.708754 0.748895 11.00000 -1.50000
AFIX 0
C50 1 0.458623 0.684722 0.464076 11.00000 0.02253 0.04438 =
0.03745 0.00643 -0.00022 -0.00421
AFIX 137
H50A 2 0.444145 0.660709 0.489283 11.00000 -1.50000
H50B 2 0.489478 0.697867 0.497139 11.00000 -1.50000
H50C 2 0.470577 0.673667 0.420165 11.00000 -1.50000
AFIX 0
C66 1 0.003358 0.690833 0.311342 11.00000 0.02940 0.04199 =
0.03652 -0.00157 0.01444 -0.00079
AFIX 137
H66A 2 0.011968 0.704814 0.267440 11.00000 -1.50000
H66B 2 -0.018945 0.710449 0.334891 11.00000 -1.50000
H66C 2 -0.016645 0.663844 0.297291 11.00000 -1.50000
AFIX 0
C97 1 0.029468 0.541151 0.425441 11.00000 0.05276 0.02371 =
0.05827 -0.00743 0.02450 -0.01736
C38 1 0.075291 0.738855 0.692245 11.00000 0.04078 0.03561 =
0.02958 -0.01764 -0.00170 0.00353
AFIX 137
H38A 2 0.055856 0.724347 0.726619 11.00000 -1.50000
H38B 2 0.049844 0.756701 0.657976 11.00000 -1.50000
H38C 2 0.103841 0.757407 0.719642 11.00000 -1.50000
AFIX 0
C27 1 0.110735 0.469632 0.825022 11.00000 0.09912 0.04444 =
0.04749 0.01152 0.03779 -0.00575
AFIX 137
H27A 2 0.088897 0.485603 0.784125 11.00000 -1.50000
H27B 2 0.092136 0.469654 0.867003 11.00000 -1.50000
H27C 2 0.115679 0.439620 0.809864 11.00000 -1.50000
AFIX 0
C67 1 0.094124 0.598554 0.144347 11.00000 0.03491 0.05034 =
0.02966 -0.01415 -0.00359 -0.00823
C17 1 0.229765 0.458607 0.680120 11.00000 0.06521 0.02792 =
0.03684 0.00702 0.02295 0.00441
C87 1 0.526383 0.547150 0.578147 11.00000 0.02988 0.04416 =
0.04848 0.00677 0.01129 0.02020
C99 1 0.046263 0.552592 0.551339 11.00000 0.03879 0.02105 =
0.06028 0.00135 0.00551 -0.01105
C89 1 0.458616 0.559236 0.476531 11.00000 0.03566 0.03575 =
0.04932 0.00287 0.00089 0.02728
C85 1 0.436247 0.534811 0.530819 11.00000 0.02399 0.05653 =
0.06384 0.00327 0.02290 0.02183
C18 1 0.205559 0.458444 0.742695 11.00000 0.07348 0.01395 =
0.04163 0.01609 0.02032 -0.00959
AFIX 43
H18 2 0.197811 0.430901 0.761450 11.00000 -1.20000
AFIX 0
C96 1 -0.019148 0.558595 0.444017 11.00000 0.06556 0.02165 =
0.04430 -0.00123 0.00026 -0.01075
C86 1 0.478282 0.528447 0.592605 11.00000 0.04081 0.04979 =
0.05420 -0.00710 0.02323 0.02184
C8 1 0.477965 0.637598 0.647161 11.00000 0.03248 0.04518 =
0.03529 -0.01829 0.00864 -0.00257
AFIX 137
H8A 2 0.489840 0.607286 0.653886 11.00000 -1.50000
H8B 2 0.507981 0.655510 0.636999 11.00000 -1.50000
H8C 2 0.447333 0.639565 0.605819 11.00000 -1.50000
AFIX 0
C70 1 0.136414 0.573299 0.113307 11.00000 0.04794 0.06262 =
0.02955 -0.01077 -0.00559 0.00186
AFIX 137
H70A 2 0.168790 0.591352 0.115008 11.00000 -1.50000
H70B 2 0.121729 0.565247 0.062293 11.00000 -1.50000
H70C 2 0.146097 0.546949 0.142527 11.00000 -1.50000
AFIX 0
C26 1 0.202222 0.464556 0.906022 11.00000 0.09393 0.07943 =
0.02784 0.00435 0.01975 -0.03144
AFIX 137
H26A 2 0.204117 0.434580 0.888831 11.00000 -1.50000
H26B 2 0.187162 0.464754 0.951105 11.00000 -1.50000
H26C 2 0.238721 0.477169 0.916011 11.00000 -1.50000
AFIX 0
C79 1 0.289440 0.418123 0.429705 11.00000 0.05789 0.01283 =
0.05360 0.00646 0.01838 0.00967
AFIX 137
H79A 2 0.326888 0.415645 0.421993 11.00000 -1.50000
H79B 2 0.277687 0.390171 0.446647 11.00000 -1.50000
H79C 2 0.287467 0.440475 0.466765 11.00000 -1.50000
AFIX 0
C69 1 0.080374 0.639574 0.096629 11.00000 0.08498 0.06540 =
0.01834 0.00862 0.00000 0.01144
AFIX 137
H69A 2 0.054075 0.657290 0.116510 11.00000 -1.50000
H69B 2 0.064816 0.631004 0.046144 11.00000 -1.50000
H69C 2 0.113497 0.656486 0.096922 11.00000 -1.50000
AFIX 0
C51 1 0.394154 0.737391 0.509385 11.00000 0.04999 0.03794 =
0.02185 -0.00678 0.00532 -0.01830
AFIX 137
H51A 2 0.364877 0.758357 0.493692 11.00000 -1.50000
H51B 2 0.424337 0.751833 0.541754 11.00000 -1.50000
H51C 2 0.380690 0.713467 0.535902 11.00000 -1.50000
AFIX 0
O8 6 -0.152018 0.768123 0.521875 31.00000 0.03786 0.04371 =
0.09289 0.01037 0.02060 -0.00476
C88 1 0.514798 0.566739 0.504880 11.00000 0.02547 0.04971 =
0.05143 -0.01293 -0.00360 0.01575
C104 1 0.074945 0.554508 0.628405 11.00000 0.03903 0.02623 =
0.07321 -0.01297 -0.00538 -0.00900
AFIX 137
H10S 2 0.048740 0.559859 0.660473 11.00000 -1.50000
H10T 2 0.101636 0.578100 0.634113 11.00000 -1.50000
H10U 2 0.093514 0.526840 0.641830 11.00000 -1.50000
AFIX 0
C94 1 0.427191 0.572900 0.401313 11.00000 0.04288 0.04190 =
0.06375 -0.00671 -0.01039 0.02652
AFIX 137
H94A 2 0.452461 0.576808 0.367464 11.00000 -1.50000
H94B 2 0.408247 0.600315 0.405921 11.00000 -1.50000
H94C 2 0.400687 0.550351 0.382255 11.00000 -1.50000
AFIX 0
C5 1 0.395941 0.570429 0.826814 11.00000 0.04606 0.08217 =
0.03512 0.01999 0.00901 0.01101
C92 1 0.581398 0.550175 0.628486 11.00000 0.04762 0.05643 =
0.05443 0.00757 0.02354 0.02586
AFIX 137
H92A 2 0.581275 0.532587 0.672525 11.00000 -1.50000
H92B 2 0.589032 0.580540 0.642720 11.00000 -1.50000
H92C 2 0.609429 0.539351 0.602731 11.00000 -1.50000
AFIX 0
C10 1 0.512022 0.658360 0.776418 11.00000 0.01697 0.09205 =
0.05191 -0.00626 -0.00560 0.00067
AFIX 137
H10A 2 0.502220 0.667615 0.822794 11.00000 -1.50000
H10B 2 0.536105 0.680022 0.760737 11.00000 -1.50000
H10C 2 0.530660 0.630262 0.783379 11.00000 -1.50000
AFIX 0
C28 1 0.156992 0.535606 0.880400 11.00000 0.13031 0.05053 =
0.05671 -0.00994 0.05843 -0.03723
AFIX 137
H28A 2 0.191428 0.551492 0.890640 11.00000 -1.50000
H28B 2 0.143563 0.531362 0.926232 11.00000 -1.50000
H28C 2 0.130361 0.552303 0.845824 11.00000 -1.50000
AFIX 0
C78 1 0.191983 0.432225 0.364347 11.00000 0.05654 0.04018 =
0.04305 -0.00584 0.01363 -0.01372
AFIX 137
H78A 2 0.186172 0.456781 0.395630 11.00000 -1.50000
H78B 2 0.182621 0.405081 0.386647 11.00000 -1.50000
H78C 2 0.168987 0.435663 0.315745 11.00000 -1.50000
AFIX 0
C100 1 -0.048769 0.584453 0.565250 11.00000 0.03662 0.04372 =
0.07506 -0.00247 0.02283 -0.00482
AFIX 137
H10V 2 -0.085893 0.579336 0.538900 11.00000 -1.50000
H10W 2 -0.042318 0.615790 0.570815 11.00000 -1.50000
H10X 2 -0.043843 0.570863 0.613863 11.00000 -1.50000
AFIX 0
C91 1 0.471246 0.506926 0.664158 11.00000 0.07600 0.05692 =
0.05646 -0.00077 0.03656 0.01934
AFIX 137
H91A 2 0.444181 0.483703 0.653622 11.00000 -1.50000
H91B 2 0.459061 0.528599 0.696234 11.00000 -1.50000
H91C 2 0.505968 0.494623 0.688679 11.00000 -1.50000
AFIX 0
C93 1 0.552880 0.592835 0.469466 11.00000 0.05241 0.04314 =
0.08162 0.01787 0.01777 0.01319
AFIX 137
H93A 2 0.588586 0.578837 0.478121 11.00000 -1.50000
H93B 2 0.556175 0.622147 0.490506 11.00000 -1.50000
H93C 2 0.538895 0.594663 0.416512 11.00000 -1.50000
AFIX 0
C68 1 0.043591 0.569244 0.138908 11.00000 0.04495 0.07033 =
0.04597 -0.02003 -0.00437 -0.02314
AFIX 137
H68A 2 0.053405 0.542587 0.167222 11.00000 -1.50000
H68B 2 0.029892 0.561799 0.087355 11.00000 -1.50000
H68C 2 0.015403 0.584745 0.158695 11.00000 -1.50000
AFIX 0
C21 1 0.246165 0.416378 0.646092 11.00000 0.11650 0.01458 =
0.06474 0.00992 0.05624 -0.00211
C103 1 0.125611 0.521763 0.495559 11.00000 0.05478 0.02608 =
0.12125 -0.00727 0.04140 -0.00961
AFIX 137
H10Y 2 0.143919 0.520659 0.547113 11.00000 -1.50000
H 2 0.145299 0.541501 0.468396 11.00000 -1.50000
HA 2 0.124811 0.492597 0.474149 11.00000 -1.50000
AFIX 0
C23 1 0.211969 0.409432 0.569603 11.00000 0.08260 0.03817 =
0.04575 -0.02054 0.02451 -0.01284
AFIX 137
H23A 2 0.174018 0.404810 0.573667 11.00000 -1.50000
H23B 2 0.225339 0.383912 0.546858 11.00000 -1.50000
H23C 2 0.214620 0.435119 0.539230 11.00000 -1.50000
AFIX 0
C80 1 0.258523 0.395682 0.300515 11.00000 0.11090 0.01096 =
0.05447 -0.01009 0.03305 -0.01727
AFIX 137
H80A 2 0.238730 0.404229 0.251876 11.00000 -1.50000
H80B 2 0.243981 0.368136 0.314972 11.00000 -1.50000
H80C 2 0.297073 0.392142 0.298845 11.00000 -1.50000
AFIX 0
C12 1 0.461143 0.516287 0.891263 11.00000 0.08292 0.16065 =
0.08786 0.08519 0.02474 0.05506
AFIX 137
H12A 2 0.451780 0.498136 0.847263 11.00000 -1.50000
H12B 2 0.471085 0.497670 0.934599 11.00000 -1.50000
H12C 2 0.491840 0.535088 0.886665 11.00000 -1.50000
AFIX 0
C90 1 0.377417 0.521670 0.524007 11.00000 0.04022 0.06755 =
0.07654 -0.00693 0.02807 0.01886
AFIX 137
H90A 2 0.361479 0.516940 0.472157 11.00000 -1.50000
H90B 2 0.357508 0.544784 0.543864 11.00000 -1.50000
H90C 2 0.375166 0.494777 0.551588 11.00000 -1.50000
AFIX 0
C11 1 0.412292 0.544349 0.899483 11.00000 0.04212 0.12538 =
0.04685 0.03890 -0.00256 0.01423
C102 1 0.038292 0.531066 0.349632 11.00000 0.07122 0.04178 =
0.06628 0.00692 0.03814 -0.01368
AFIX 137
H10Z 2 0.064397 0.507201 0.351784 11.00000 -1.50000
HB 2 0.052477 0.556873 0.328681 11.00000 -1.50000
HC 2 0.003781 0.522515 0.318766 11.00000 -1.50000
AFIX 0
C101 1 -0.068071 0.567172 0.390204 11.00000 0.06935 0.04185 =
0.06246 -0.00617 0.01386 -0.02464
AFIX 137
H10 2 -0.064188 0.554932 0.342664 11.00000 -1.50000
HD 2 -0.073790 0.598618 0.385278 11.00000 -1.50000
HE 2 -0.099228 0.553749 0.406376 11.00000 -1.50000
AFIX 0
C22 1 0.306424 0.418674 0.644974 11.00000 0.09152 0.04022 =
0.05838 0.00316 0.02126 0.03480
AFIX 137
H22A 2 0.314101 0.445053 0.619127 11.00000 -1.50000
H22B 2 0.317139 0.393104 0.619598 11.00000 -1.50000
H22C 2 0.326928 0.419348 0.695475 11.00000 -1.50000
AFIX 0
C13 1 0.428602 0.577885 0.961755 11.00000 0.07024 0.19075 =
0.03112 0.02815 0.00166 0.00467
AFIX 137
H13A 2 0.459934 0.594632 0.952835 11.00000 -1.50000
H13B 2 0.438085 0.562694 1.008889 11.00000 -1.50000
H13C 2 0.398132 0.597600 0.963036 11.00000 -1.50000
AFIX 0
C108 1 0.099109 0.380881 -0.027634 41.00000 0.06976 0.03082 =
0.07947 0.01443 0.03036 0.01082
AFIX 137
H10D 2 0.120530 0.354277 -0.016444 41.00000 -1.50000
H10E 2 0.115189 0.398933 -0.061474 41.00000 -1.50000
H10F 2 0.061832 0.373282 -0.050484 41.00000 -1.50000
AFIX 0
C24 1 0.235810 0.376632 0.691774 11.00000 0.16189 0.02140 =
0.08312 0.02424 0.06885 0.01730
AFIX 137
H24A 2 0.258861 0.378394 0.740618 11.00000 -1.50000
H24B 2 0.244356 0.350042 0.667170 11.00000 -1.50000
H24C 2 0.197612 0.376124 0.696653 11.00000 -1.50000
AFIX 0
C109 1 0.070185 0.465024 0.035283 41.00000 0.12271 0.03889 =
0.06724 -0.00991 -0.00987 -0.02330
AFIX 137
H10G 2 0.044046 0.464194 -0.011184 41.00000 -1.50000
H10H 2 0.099419 0.485418 0.031017 41.00000 -1.50000
H10I 2 0.051838 0.474534 0.074767 41.00000 -1.50000
AFIX 0
C107 1 -0.034958 0.356804 0.140591 41.00000 0.10815 0.13294 =
0.04601 -0.00543 0.01245 -0.09365
AFIX 137
H10J 2 -0.056803 0.374799 0.102490 41.00000 -1.50000
H10K 2 -0.053460 0.354167 0.182459 41.00000 -1.50000
H10L 2 -0.030172 0.327869 0.120663 41.00000 -1.50000
AFIX 0
C116 1 -0.047645 0.771958 0.477691 31.00000 0.05849 0.07128 =
0.16549 -0.00690 0.04895 0.01129
AFIX 133
H11D 2 -0.048600 0.803772 0.475382 31.00000 -1.50000
H11E 2 -0.028611 0.760697 0.440063 31.00000 -1.50000
H11F 2 -0.028572 0.762731 0.526332 31.00000 -1.50000
AFIX 0
C110 1 0.166842 0.421190 0.110301 41.00000 0.05922 0.31450 =
0.07189 0.01062 -0.03182 -0.08403
AFIX 137
H11A 2 0.187577 0.394025 0.116608 41.00000 -1.50000
H11B 2 0.163668 0.432751 0.158567 41.00000 -1.50000
H11C 2 0.185565 0.442390 0.084473 41.00000 -1.50000
AFIX 0
C106 1 0.068818 0.346159 0.246472 41.00000 0.04729 0.13560 =
0.09444 -0.01291 0.02070 -0.01900
AFIX 137
H10M 2 0.063246 0.315504 0.232788 41.00000 -1.50000
H10N 2 0.055491 0.351632 0.292043 41.00000 -1.50000
H10O 2 0.107592 0.353023 0.253878 41.00000 -1.50000
AFIX 0
C105 1 0.024564 0.438180 0.204757 41.00000 0.12266 0.10664 =
0.10424 -0.06751 0.06599 -0.04107
AFIX 137
H10P 2 0.060903 0.449677 0.223778 41.00000 -1.50000
H10Q 2 0.003424 0.437866 0.244135 41.00000 -1.50000
H10R 2 0.006377 0.456647 0.164485 41.00000 -1.50000
AFIX 0
C115 1 -0.120421 0.692812 0.460664 31.00000 0.15194 0.03143 =
0.41887 -0.06668 0.12649 -0.03210
AFIX 133
H11G 2 -0.103544 0.681909 0.509275 31.00000 -1.50000
H11H 2 -0.100455 0.681825 0.423836 31.00000 -1.50000
H11I 2 -0.158142 0.682861 0.448687 31.00000 -1.50000
AFIX 0
C112 1 -0.193506 0.713322 0.618606 31.00000 0.14707 0.15846 =
0.19344 0.12052 -0.03812 -0.11751
AFIX 133
H11J 2 -0.229736 0.713321 0.587616 31.00000 -1.50000
H11K 2 -0.196817 0.711258 0.670330 31.00000 -1.50000
H11L 2 -0.172816 0.688413 0.605769 31.00000 -1.50000
AFIX 0
C113 1 -0.197792 0.809231 0.625407 31.00000 0.46596 0.14642 =
0.26926 -0.03107 0.30909 -0.04845
AFIX 133
H11M 2 -0.178529 0.836230 0.618919 31.00000 -1.50000
H11N 2 -0.202852 0.807040 0.676424 31.00000 -1.50000
H11O 2 -0.233262 0.809295 0.592498 31.00000 -1.50000
AFIX 0
C114 1 -0.154090 0.770395 0.370053 31.00000 0.18994 0.26249 =
0.07293 -0.02265 -0.02379 -0.05897
AFIX 133
H11P 2 -0.191413 0.759438 0.359975 31.00000 -1.50000
H11Q 2 -0.134915 0.760136 0.331878 31.00000 -1.50000
H11R 2 -0.154546 0.802240 0.370305 31.00000 -1.50000
AFIX 0
C111 1 -0.102340 0.771485 0.660262 31.00000 0.24184 0.49150 =
0.13527 0.05080 -0.05482 -0.27149
AFIX 133
H11S 2 -0.075272 0.750346 0.650801 31.00000 -1.50000
H11T 2 -0.108146 0.768102 0.710776 31.00000 -1.50000
H11U 2 -0.089363 0.800970 0.653503 31.00000 -1.50000
AFIX 0
O7 6 0.063006 0.383114 0.105223 41.00000 0.17870 0.05801 =
0.11341 -0.01383 0.11453 -0.04385
C1 1 0.329800 0.588541 0.716711 11.00000 0.03359 0.02506 =
0.01652 -0.00158 0.00518 -0.00213
C14 1 0.368081 0.514777 0.916230 11.00000 0.07261 0.21958 =
0.08876 0.12774 0.00786 0.02274
AFIX 137
H14A 2 0.334620 0.531509 0.914281 11.00000 -1.50000
H14B 2 0.379275 0.502327 0.965406 11.00000 -1.50000
H14C 2 0.361690 0.491327 0.879858 11.00000 -1.50000
AFIX 0
PART 1
C84A 1 0.377260 0.500137 0.174798 21.00000 0.06339 0.05713 =
0.05684 0.00566 0.05026 0.01284
AFIX 137
H84A 2 0.405582 0.516172 0.207856 21.00000 -1.50000
H84B 2 0.387013 0.497891 0.126172 21.00000 -1.50000
H84C 2 0.373794 0.470937 0.194506 21.00000 -1.50000
AFIX 0
C82A 1 0.281982 0.501493 0.105056 21.00000 0.06061 0.08352 =
0.02018 -0.00422 0.01002 0.00721
AFIX 137
H82A 2 0.276901 0.471074 0.117880 21.00000 -1.50000
H82B 2 0.295728 0.502785 0.059003 21.00000 -1.50000
H82C 2 0.247197 0.516815 0.099025 21.00000 -1.50000
AFIX 0
C83A 1 0.331004 0.570469 0.143633 21.00000 0.11720 0.05479 =
0.04249 -0.00070 0.06252 -0.00978
AFIX 137
H83A 2 0.297885 0.586979 0.145375 21.00000 -1.50000
H83B 2 0.337774 0.570368 0.093268 21.00000 -1.50000
H83C 2 0.361746 0.584002 0.176343 21.00000 -1.50000
AFIX 0
PART 0
PART 2
C83B 1 0.377484 0.548118 0.187623 -21.00000 0.02094 0.01067 =
0.01656 0.01022 0.00163 0.00431
AFIX 137
H83D 2 0.400576 0.534120 0.229725 -21.00000 -1.50000
H83E 2 0.370489 0.578266 0.200112 -21.00000 -1.50000
H83F 2 0.395849 0.547693 0.145425 -21.00000 -1.50000
AFIX 0
C82B 1 0.284983 0.543091 0.114288 -21.00000 0.05269 0.04554 =
0.03280 -0.02778 0.00164 -0.00588
AFIX 137
H82D 2 0.297594 0.542877 0.067371 -21.00000 -1.50000
H82E 2 0.278956 0.573144 0.128299 -21.00000 -1.50000
H82F 2 0.250950 0.526779 0.109247 -21.00000 -1.50000
AFIX 0
C84B 1 0.338483 0.475546 0.142838 -21.00000 0.03069 0.04187 =
0.05804 -0.02357 0.02274 0.01000
AFIX 137
H84D 2 0.354767 0.458478 0.186013 -21.00000 -1.50000
H84E 2 0.364152 0.477708 0.109175 -21.00000 -1.50000
H84F 2 0.305199 0.461259 0.117829 -21.00000 -1.50000
AFIX 0
HKLF 4
REM d19106_a.res in P2(1)/c
REM wR2 = 0.2968, GooF = S = 1.015, Restrained GooF = 1.014 for all data
REM R1 = 0.1338 for 19089 Fo > 4sig(Fo) and 0.1714 for all 26796 data
REM 1313 parameters refined using 75 restraints
END
WGHT 0.0000 225.2592
REM Highest difference peak 1.261, deepest hole -1.372, 1-sigma level 0.138
Q1 1 0.2834 0.6219 0.4174 11.00000 0.05 -1.37
Q2 1 0.2386 0.5479 0.4228 11.00000 0.05 -1.35
Q3 1 0.1322 0.3854 0.0816 11.00000 0.05 1.26
Q4 1 0.1805 0.6220 0.4024 11.00000 0.05 -1.11
Q5 1 -0.1586 0.7327 0.4935 11.00000 0.05 0.98
Q6 1 0.4933 0.5001 0.4383 11.00000 0.05 -0.92
Q7 1 -0.1712 0.7459 0.4616 11.00000 0.05 0.87
Q8 1 0.2526 0.6051 0.6357 11.00000 0.05 -0.83
Q9 1 -0.1416 0.8010 0.6055 11.00000 0.05 0.81
Q10 1 0.3320 0.6227 0.5030 11.00000 0.05 0.78
Q11 1 0.3222 0.6689 0.5338 11.00000 0.05 -0.78
Q12 1 0.2207 0.5449 0.4760 11.00000 0.05 0.77
Q13 1 0.2716 0.6211 0.5747 11.00000 0.05 0.76
Q14 1 0.1963 0.5823 0.5323 11.00000 0.05 -0.74
Q15 1 0.2720 0.6132 0.5094 11.00000 0.05 0.73
Q16 1 0.2789 0.6700 0.4039 11.00000 0.05 -0.71
Q17 1 0.2251 0.6624 0.5640 11.00000 0.05 0.71
Q18 1 0.0897 0.4287 0.1075 11.00000 0.05 0.68
Q19 1 0.3674 0.5476 0.5582 11.00000 0.05 -0.67
Q20 1 -0.1319 0.7983 0.4267 11.00000 0.05 0.67
Q21 1 0.0394 0.3322 0.1136 11.00000 0.05 0.66
;
_shelx_res_checksum 64699
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