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A simple gas introduction system for cryogenic powder X-ray diffraction

Hodyss, Robert and Vu, Tuan H. and Choukroun, Mathieu and Cable, Morgan L. (2021) A simple gas introduction system for cryogenic powder X-ray diffraction. Journal of Applied Crystallography, 54 (4). pp. 1268-1270. ISSN 1600-5767. doi:10.1107/s1600576721006671. https://resolver.caltech.edu/CaltechAUTHORS:20210901-155450271

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Abstract

A simple system is described for the introduction of gases into standard X-ray diffraction capillaries mounted in situ in the X-ray beam of laboratory X-ray diffraction instruments. This system retains many of the advantages of the standard Norby cell, but does not require custom machining and has less stringent space restrictions. The system has been used to study the crystallization and interaction of volatile organics at cryogenic temperatures, but gas–solid interactions could also be studied at elevated temperatures using this approach.


Item Type:Article
Related URLs:
URLURL TypeDescription
https://doi.org/10.1107/s1600576721006671DOIArticle
ORCID:
AuthorORCID
Hodyss, Robert0000-0002-6523-3660
Vu, Tuan H.0000-0001-6839-9765
Choukroun, Mathieu0000-0001-7447-9139
Cable, Morgan L.0000-0002-3680-302X
Additional Information:© 2021 International Union of Crystallography.
Funders:
Funding AgencyGrant Number
NASA80NM0018D0004
Subject Keywords:cryogenic conditions; powder X-ray diffraction; Norby cell; gas introduction
Issue or Number:4
DOI:10.1107/s1600576721006671
Record Number:CaltechAUTHORS:20210901-155450271
Persistent URL:https://resolver.caltech.edu/CaltechAUTHORS:20210901-155450271
Official Citation:A simple gas introduction system for cryogenic powder X-ray diffraction. Hodyss, R., Vu, T. H., Choukroun, M. & Cable, M. L. (2021). J. Appl. Cryst. 54, 1268-1270; DOI: 10.1107/s1600576721006671
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:110691
Collection:CaltechAUTHORS
Deposited By: Tony Diaz
Deposited On:01 Sep 2021 17:37
Last Modified:01 Sep 2021 17:37

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