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Determination of the concentration and stable isotopic composition of oxygen in organic matter containing carbon, hydrogen, oxygen, nitrogen, and sulfur

DeNiro, Michael J. and Epstein, Samuel (1989) Determination of the concentration and stable isotopic composition of oxygen in organic matter containing carbon, hydrogen, oxygen, nitrogen, and sulfur. Analytical Chemistry, 61 (17). pp. 1887-1889. ISSN 0003-2700. http://resolver.caltech.edu/CaltechAUTHORS:20130715-134543975

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Abstract

A method for the quantitative production of carbon dioxide from oxygen in organic matter consisting of carbon, hydrogen, oxygen, nitrogen, and sulfur has been developed. Manometric and mass spectrometric analysis of the CO_2 permit direct determination of the concentration and isotopic composition of oxygen in CHONS compounds with accuracy comparable to that previously achievable for CHO and CHON compounds. Samples containing as little as 187 µmol of oxygen with S/O ratios as high as 0.16 have been analyzed by using this method.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1021/ac00192a021 DOIUNSPECIFIED
http://pubs.acs.org/doi/abs/10.1021/ac00192a021PublisherUNSPECIFIED
Additional Information:© 1989 American Chemical Society. Received for review February 21, 1989. Accepted May 24, 1989. This work was supported by National Science Foundation Grants EAR 85-04096, BNS 84-18280, and DMB 84-05003. This is contribution number 4706 from the Division of Geological and Planetary Sciences at Caltech.
Funders:
Funding AgencyGrant Number
NSFEAR 85-04096
NSFBNS 84-18280
NSFDMB 84-05003
Other Numbering System:
Other Numbering System NameOther Numbering System ID
Caltech Division of Geological and Planetary Sciences 4706
Record Number:CaltechAUTHORS:20130715-134543975
Persistent URL:http://resolver.caltech.edu/CaltechAUTHORS:20130715-134543975
Official Citation:Determination of the concentration and stable isotopic composition of oxygen in organic matter containing carbon, hydrogen, oxygen, nitrogen, and sulfur Michael J. DeNiro and Samuel Epstein Analytical Chemistry 1989 61 (17), 1887-1889
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:39369
Collection:CaltechAUTHORS
Deposited By: Tony Diaz
Deposited On:19 Aug 2013 19:24
Last Modified:19 Aug 2013 19:24

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