"Table S2. 40Ar/39Ar step-heating results for the groundmass concentrate, biotite and hornblende samples." ID Temp 40Ar/39Ar 37Ar/39Ar 36Ar/39Ar 39ArK K/Ca Cl/K 40Ar* 39Ar Age ±2s (°C) (x 10-3) (x 10-15 mol) (x 10-3) (%) (%) (Ma) (Ma) "19-133-1, groundmass, 48.78 mg, J=0.0006998±0.11%, D=1.0069±0.001, NM-137, Lab#=52210-01" A 625 2719.94 1.90 8985.98 0.88 0.27 11.76 2.38 2.95 80.07 54.23 B 700 1115.08 1.65 3601.32 2.15 0.31 5.63 4.58 10.20 63.39 13.71 C 750 207.85 1.51 611.45 1.50 0.34 2.08 13.13 15.24 34.18 4.76 D 800 135.75 1.41 368.24 2.19 0.36 1.45 19.93 22.63 33.87 2.54 E 875 88.11 1.30 206.59 3.32 0.39 0.73 30.84 33.79 34.02 0.85 F 975 54.42 0.98 94.41 3.52 0.52 0.77 48.88 45.65 33.30 0.43 G 1075 38.54 0.64 42.79 5.13 0.80 0.74 67.33 62.91 32.48 0.26 H 1250 30.78 4.37 17.43 9.80 0.12 0.57 84.45 95.91 32.65 0.17 I 1650 41.33 20.77 63.14 1.22 0.02 0.97 59.02 100.00 31.11 0.60 total gas age n=9 29.71 0.36 36.58 3.28 plateau n=6 steps C-H 25.46 0.38 85.71 32.70 0.30 "19-135-1, groundmass, 46.98 mg, J=0.0006995±0.11%, D=1.0069±0.001, NM-137, Lab#=52211-01" A 625 16843.42 2.35 55692.38 0.13 0.22 57.35 2.29 0.42 432.55 1459.77 B 700 465.33 1.58 1467.20 0.79 0.32 5.41 6.86 3.01 39.87 30.81 C 750 215.18 1.18 648.33 0.81 0.43 2.93 11.01 5.68 29.69 12.37 D 800 163.05 1.13 467.56 1.25 0.45 1.27 15.32 9.77 31.28 5.93 E 875 133.10 1.35 358.88 2.63 0.38 1.77 20.40 18.40 33.99 1.70 F 975 56.42 0.92 101.80 2.42 0.55 0.74 46.82 26.36 33.06 0.62 G 1075 52.82 0.58 89.14 4.40 0.87 0.52 50.22 40.81 33.19 0.39 H 1250 33.48 1.88 25.23 16.12 0.27 0.47 78.20 93.75 32.79 0.16 I 1650 49.50 20.67 89.23 1.90 0.02 0.95 50.19 100.00 31.66 0.58 total gas age n=9 30.45 0.39 34.63 7.90 plateau n=7 steps B-H 28.42 0.41 93.33 32.86 0.21 "19-137-1 gm B:1:137, groundmass, 47.52 mg, J=0.0006997±0.11%, D=1.0069±0.001, NM-137, Lab#=52208-01" A 625 736.48 0.48 2446.12 1.26 1.07 4.35 1.86 2.10 17.21 9.95 B 700 139.95 0.28 451.65 2.58 1.81 0.98 4.65 6.41 8.21 1.84 C 750 95.08 0.85 300.17 2.85 0.60 1.20 6.79 11.17 8.14 1.20 D 800 69.12 1.35 209.43 4.08 0.38 1.04 10.63 17.98 9.27 0.72 E 875 42.99 0.57 121.42 5.47 0.90 0.56 16.64 27.11 9.01 0.46 F 975 26.60 0.22 66.27 6.20 2.27 0.74 26.45 37.46 8.86 0.30 G 1075 19.40 0.24 42.69 8.64 2.15 0.56 35.10 51.88 8.58 0.17 H 1250 17.05 2.76 34.97 27.74 0.18 0.69 40.73 98.21 8.77 0.12 I 1650 54.38 9.19 160.66 1.07 0.06 0.39 14.09 100.00 9.73 0.90 total gas age n=9 59.88 0.87 8.95 0.56 plateau n=8 steps A-H 58.81 0.88 98.21 8.74 0.15 "19-141-2B gm B:2:137, groundmass, 49.83 mg, J=0.0006999±0.11%, D=1.0069±0.001, NM-137, Lab#=52209-01" A 625 182.59 0.09 580.70 3.89 5.53 1.28 6.02 5.38 13.83 2.09 B 700 22.25 0.09 45.53 13.14 5.79 0.54 39.57 23.51 11.08 0.18 C 750 14.52 0.14 24.86 5.29 3.75 0.57 49.48 30.83 9.05 0.19 D 800 12.05 0.20 21.44 3.54 2.60 0.28 47.57 35.71 7.23 0.23 E 875 11.08 0.29 18.02 5.26 1.74 0.47 52.16 42.98 7.29 0.16 F 975 11.77 0.26 20.37 7.97 1.96 0.36 49.07 53.98 7.28 0.14 G 1075 17.48 0.17 36.39 10.80 3.09 0.70 38.56 68.90 8.49 0.15 H 1250 18.14 0.27 34.08 20.08 1.86 0.62 44.61 96.63 10.19 0.13 I 1650 47.59 1.11 88.39 2.44 0.46 0.76 45.31 100.00 27.05 0.49 total gas age n=9 72.41 3.08 10.10 0.27 plateau n=3 steps D-F 16.77 2.02 23.16 7.27 0.10 "20-49.2, groundmass, 42.43 mg (mixture), J=0.0007078±0.11%, D=1.0069±0.001, NM-137, Lab#=52291-01" A 625 361.71 0.36 1220.18 0.13 1.42 1.39 0.32 0.20 1.50 11.70 B 700 3.04 0.23 9.75 5.20 2.23 0.63 5.83 7.94 0.23 0.09 C 750 2.23 0.20 6.87 4.70 2.50 0.54 9.88 14.95 0.28 0.07 D 800 1.64 0.18 4.92 8.60 2.91 0.48 12.09 27.76 0.25 0.05 E 875 1.49 0.16 4.18 16.86 3.24 0.53 17.79 52.87 0.34 0.03 F 975 2.79 0.16 8.63 13.61 3.10 0.54 9.16 73.14 0.33 0.05 G 1075 10.49 0.24 35.41 7.39 2.09 0.50 0.47 84.14 0.06 0.13 H 1250 15.11 1.71 47.76 6.77 0.30 0.95 7.51 94.23 1.45 0.22 I 1650 20.36 2.73 67.89 3.87 0.19 1.11 2.57 100.00 0.67 0.27 total gas age n=9 67.15 2.44 0.42 0.11 plateau n=5 steps B-F 48.97 2.96 72.94 0.31 0.04 "Table S2. continued 40Ar/39Ar step-heating results for groundmass concentrate, biotite and hornblende samples." ID Temp 40Ar/39Ar 37Ar/39Ar 36Ar/39Ar 39ArK K/Ca Cl/K 40Ar* 39Ar Age ±2s (°C) (x 10-3) (x 10-15 mol) (x 10-3) (%) (%) (Ma) (Ma) "3-89, groundmass, 33.31 mg, J=0.0007034±0.11%, D=1.0069±0.001, NM-137, Lab#=52224-01" A 625 3542.74 0.25 11976.34 0.02 2.04 3.76 0.11 0.04 4.75 419.45 B 700 5.79 0.22 18.85 1.87 2.30 0.85 4.16 3.81 0.31 0.16 C 750 2.17 0.18 6.65 1.97 2.88 0.61 10.27 7.78 0.28 0.13 D 800 1.41 0.16 4.40 4.40 3.20 0.51 8.70 16.63 0.16 0.06 E 875 1.07 0.15 3.01 9.06 3.46 0.38 17.72 34.85 0.24 0.03 F 975 1.21 0.16 3.47 14.96 3.12 0.46 16.60 64.93 0.26 0.02 G 1075 5.40 0.28 17.81 9.05 1.82 0.47 3.03 83.13 0.21 0.09 H 1250 13.34 1.03 44.72 6.31 0.50 0.56 1.56 95.82 0.27 0.21 I 1650 14.30 3.68 47.98 2.08 0.14 1.01 2.97 100.00 0.54 0.28 total gas age n=9 49.73 2.46 0.25 0.27 plateau n=7 steps B-H 47.63 2.56 95.77 0.24 0.03 "19-141-2A bi, A1:137, 8.54 mg biotite, J=0.0006943±0.11%, D=1.0069±0.001, NM-137, Lab#=52192-01" A 650 586.19 0.18 1969.12 0.22 2.82 3.33 0.74 0.91 5.41 11.73 B 750 130.66 0.34 424.01 0.56 1.51 1.91 4.13 3.20 6.74 2.06 C 850 26.21 0.05 70.74 1.49 10.89 0.67 20.25 9.28 6.64 0.48 D 920 12.52 0.03 24.21 1.94 19.70 0.51 42.88 17.22 6.71 0.20 E 1000 12.68 0.03 24.07 2.50 16.33 0.59 43.92 27.45 6.96 0.19 F 1075 13.02 0.05 25.86 2.85 11.02 0.68 41.35 39.11 6.73 0.17 G 1110 13.54 0.05 27.76 1.63 10.92 0.54 39.44 45.77 6.68 0.24 H 1180 10.93 0.07 18.84 2.27 6.88 0.14 49.12 55.05 6.71 0.19 I 1210 7.51 0.09 6.78 1.97 5.72 0.64 73.44 63.09 6.90 0.10 J 1250 6.51 0.08 3.33 4.33 6.41 0.47 84.98 80.79 6.92 0.06 K 1300 6.02 0.02 1.72 4.41 31.02 0.68 91.56 98.84 6.90 0.05 L 1650 15.70 0.13 32.99 0.28 3.83 0.20 37.97 100.00 7.45 0.66 total gas age n=12 24.46 13.85 6.81 0.31 plateau n=11 steps B-L 24.24 13.95 99.09 6.88 0.06 "19-141-2b bi, A3:137, 10.46 mg biotite, J=0.0006941±0.11%, D=1.0069±0.001, NM-137, Lab#=52194-02" A 650 2170.82 0.27 7395.49 0.03 1.88 -7.44 -0.67 0.11 -18.29 123.60 B 750 272.49 0.04 909.51 0.80 13.88 0.76 1.37 2.75 4.67 3.54 C 850 46.53 0.02 137.92 1.58 27.33 0.66 12.42 7.95 7.22 0.67 D 920 11.42 0.01 19.91 3.07 50.25 0.61 48.48 18.04 6.92 0.16 E 1000 10.47 0.01 16.54 3.02 42.63 0.55 53.34 27.99 6.98 0.14 F 1075 10.00 0.01 15.79 2.92 43.96 0.67 53.38 37.58 6.67 0.15 G 1110 8.94 0.03 11.44 2.03 18.24 0.65 62.22 44.25 6.95 0.14 H 1180 8.02 0.02 8.46 2.90 25.04 0.84 68.85 53.78 6.90 0.10 I 1210 7.09 0.02 5.39 2.13 33.93 0.85 77.56 60.78 6.88 0.12 J 1250 6.28 0.01 2.45 4.41 64.56 0.57 88.46 75.28 6.94 0.06 K 1300 5.92 0.00 1.45 7.17 104.07 0.63 92.80 98.87 6.87 0.04 L 1650 11.21 0.19 18.20 0.34 2.69 0.15 52.17 100.00 7.31 0.57 total gas age n=12 30.40 55.24 6.82 0.36 plateau n=12 steps A-L 30.40 55.24 100.00 6.89 0.05 "20-49-3 bi, A5:137, 8.96 mg biotite, J=0.0006929±0.11%, D=1.0069±0.001, NM-137, Lab#=52196-01" A 650 64.24 0.13 213.35 0.21 4.01 1.82 1.88 0.86 1.51 1.97 B 750 19.79 0.16 64.88 0.30 3.19 0.27 3.20 2.09 0.79 0.76 C 850 13.57 0.12 45.31 0.36 4.33 -0.22 1.36 3.53 0.23 0.69 D 920 9.73 0.07 30.45 0.37 7.32 1.28 7.56 5.05 0.92 0.56 E 1000 5.58 0.04 17.83 0.71 12.40 0.86 5.69 7.94 0.40 0.34 F 1075 4.95 0.04 15.95 1.15 12.04 0.47 4.82 12.58 0.30 0.18 G 1110 4.63 0.04 14.49 1.07 12.28 0.47 7.67 16.89 0.44 0.20 H 1180 5.72 0.08 17.78 4.47 6.18 0.48 8.23 35.00 0.59 0.12 I 1210 3.15 0.10 9.59 5.40 5.19 0.64 10.37 56.85 0.41 0.08 J 1250 1.92 0.19 5.10 8.03 2.68 0.44 22.38 89.37 0.54 0.04 K 1300 1.60 0.22 4.17 2.47 2.31 0.65 24.22 99.39 0.48 0.08 L 1650 14.31 0.19 46.24 0.15 2.64 2.97 4.63 100.00 0.83 1.21 total gas age n=12 24.68 5.07 0.51 0.14 plateau n=5 steps G-K 21.43 4.48 86.81 0.51 0.06 "Table S2. continued 40Ar/39Ar step-heating results for groundmass concentrate, biotite and hornblende samples." ID Temp 40Ar/39Ar 37Ar/39Ar 36Ar/39Ar 39ArK K/Ca Cl/K 40Ar* 39Ar Age ±2s (°C) (x 10-3) (x 10-15 mol) (x 10-3) (%) (%) (Ma) (Ma) "BG-4 84-2A bi,F14:137, 9.88 mg biotite, J=0.0007058±0.11%, D=1.0069±0.001, NM-137, Lab#=52245-01" A 650 885.40 0.91 2994.13 0.15 0.56 5.02 0.08 0.52 0.91 25.61 B 750 92.22 1.79 300.03 0.31 0.29 0.33 4.02 1.61 4.72 2.17 C 850 33.68 0.34 101.46 0.57 1.49 1.08 11.05 3.62 4.74 0.70 D 920 12.16 0.06 23.49 1.49 8.71 0.55 42.94 8.83 6.64 0.27 E 1000 8.15 0.03 8.49 4.16 17.96 0.50 69.23 23.37 7.17 0.08 F 1075 7.63 0.05 6.65 6.13 11.30 0.64 74.31 44.74 7.21 0.07 G 1110 8.77 0.07 10.73 2.50 7.65 0.62 63.94 53.47 7.13 0.13 H 1180 8.50 0.13 10.06 2.59 4.06 0.59 65.14 62.50 7.04 0.12 I 1210 7.41 0.12 6.49 2.15 4.33 0.45 74.25 70.02 7.00 0.08 J 1250 6.88 0.25 4.64 3.21 2.05 0.80 80.35 81.21 7.02 0.08 K 1300 6.35 0.05 2.94 4.75 9.64 0.50 86.41 97.79 6.97 0.05 L 1650 10.23 0.18 16.06 0.63 2.80 0.67 53.75 100.00 6.99 0.27 total gas age n=12 28.66 8.77 6.96 0.26 plateau n=8 steps E-L 26.13 9.08 91.17 7.06 0.08 "BG-4 84-2b bi, A8:137, 4.01 mg biotite, J=0.0006913±0.11%, D=1.0069±0.001, NM-137, Lab#=52199-01" A 650 1447.11 0.72 4879.16 0.03 0.71 4.66 0.37 0.32 6.70 87.41 B 750 40.34 0.79 123.60 0.21 0.65 0.64 9.62 2.42 4.83 1.82 C 850 41.33 0.45 123.46 0.20 1.14 0.47 11.81 4.43 6.08 1.44 D 920 14.18 0.10 28.65 0.46 5.17 0.63 40.34 9.10 7.12 0.57 E 1000 8.05 0.04 6.98 1.32 11.58 0.69 74.44 22.38 7.46 0.15 F 1075 7.77 0.06 6.50 2.05 8.29 0.56 75.35 42.99 7.28 0.13 G 1110 7.89 0.10 7.16 0.96 5.13 0.86 73.29 52.69 7.20 0.18 H 1180 8.87 0.15 9.93 1.10 3.47 0.30 67.07 63.77 7.41 0.21 I 1210 7.76 0.18 6.04 0.93 2.85 1.16 77.22 73.13 7.46 0.19 J 1250 7.43 0.36 5.49 1.25 1.43 0.32 78.58 85.69 7.27 0.14 K 1300 6.50 0.11 2.50 1.07 4.82 0.84 88.76 96.43 7.18 0.17 L 1650 10.91 0.14 17.73 0.36 3.61 1.10 52.09 100.00 7.08 0.54 total gas age n=12 9.94 5.50 7.22 0.53 plateau n=10 steps C-L 9.70 5.62 97.58 7.31 0.10 "19-57-2 hbl, A6:137, 22.18 mg hbl, J=0.0006923±0.11%, D=1.0069±0.001, NM-137, Lab#=52197-01" A 800 54.10 0.35 124.94 0.28 1.46 1.21 31.81 2.85 21.38 1.50 B 850 4.70 0.22 9.21 0.20 2.36 0.80 42.52 4.89 2.50 0.68 C 950 13.65 0.44 33.47 0.17 1.16 1.92 27.81 6.66 4.74 1.04 D 1020 53.29 1.20 159.83 0.07 0.42 1.08 11.56 7.41 7.69 2.84 E 1080 85.95 2.07 258.66 0.05 0.25 3.68 11.27 7.91 12.07 4.78 F 1120 40.02 2.97 95.94 0.06 0.17 2.58 29.77 8.52 14.86 3.11 G 1160 21.00 4.12 62.76 0.52 0.12 0.92 13.31 13.90 3.50 0.72 H 1200 7.17 4.35 22.57 2.16 0.12 0.67 12.00 36.25 1.08 0.22 I 1300 3.39 5.35 9.14 6.08 0.10 1.06 33.49 99.00 1.43 0.07 J 1400 27.40 87.26 98.99 0.06 0.01 14.24 19.60 99.65 7.26 2.91 K 1650 47.82 10.81 149.30 0.03 0.05 1.37 9.62 100.00 5.79 4.95 total gas age n=11 9.69 0.21 2.34 0.30 plateau n=2 steps H-I 8.24 0.10 85.10 1.40 0.21 "19-141-1 hbl, M3:137, 21.70 mg, J=0.0007079±0.11%, D=1.0069±0.001, NM-137, Lab#=52289-01" A 800 2353.10 5.99 8085.04 0.02 0.09 7.62 -1.51 0.17 -46.21 237.59 B 850 987.60 26.03 3431.33 0.02 0.02 -0.52 -2.45 0.30 -31.93 83.33 C 950 104.14 5.11 326.35 0.02 0.10 5.82 7.80 0.47 10.39 10.52 D 1020 36.47 3.17 123.36 0.03 0.16 -2.96 0.75 0.68 0.35 6.36 E 1080 40.30 2.44 125.25 0.03 0.21 -1.71 8.67 0.96 4.46 5.12 F 1120 33.30 2.71 96.74 0.04 0.19 -0.11 14.82 1.28 6.31 3.94 G 1160 13.82 3.31 31.96 0.28 0.15 1.11 33.62 3.54 5.94 0.75 H 1200 8.88 3.48 13.13 0.93 0.15 0.53 59.57 11.05 6.77 0.25 I 1300 6.27 3.70 4.49 10.71 0.14 0.64 83.73 97.70 6.71 0.05 J 1400 15.08 4.23 34.77 0.20 0.12 -0.63 34.17 99.30 6.59 0.92 K 1650 25.92 7.18 73.93 0.09 0.07 -0.09 18.00 100.00 5.99 2.19 total gas age n=11 12.36 0.14 6.54 0.67 plateau n=5 steps G-K 12.20 0.14 98.72 6.71 0.06 "Table S2. continued 40Ar/39Ar step-heating results for groundmass concentrate, biotite and hornblende samples." ID Temp 40Ar/39Ar 37Ar/39Ar 36Ar/39Ar 39ArK K/Ca Cl/K 40Ar* 39Ar Age ±2s (°C) (x 10-3) (x 10-15 mol) (x 10-3) (%) (%) (Ma) (Ma) "3-87 hbl, A4:137, 14.71 mg hbl, J=0.0006937±0.11%, D=1.0069±0.001, NM-137, Lab#=52195-01" A 800 65.19 0.78 194.83 0.27 0.66 1.48 11.79 3.73 9.60 1.86 B 850 24.27 0.42 55.65 0.19 1.22 0.45 32.39 6.42 9.82 1.25 C 950 16.92 0.59 31.62 0.25 0.87 0.90 45.05 9.85 9.52 0.80 D 1020 29.85 0.78 47.12 0.14 0.66 0.43 53.57 11.78 19.92 1.40 E 1080 32.35 0.97 46.70 0.12 0.53 0.89 57.59 13.47 23.19 1.52 F 1120 37.79 2.37 96.60 0.18 0.22 -1.40 24.97 15.96 11.79 1.33 G 1160 16.71 3.79 50.51 0.99 0.13 0.78 12.54 29.68 2.63 0.38 H 1200 21.69 4.20 70.98 1.89 0.12 1.07 4.91 55.92 1.34 0.37 I 1300 6.41 4.81 14.59 2.69 0.11 1.18 38.92 93.31 3.13 0.14 J 1400 31.91 4.49 26.68 0.25 0.11 1.36 76.46 96.84 30.39 0.77 K 1650 31.08 1.04 20.88 0.23 0.49 0.90 80.43 100.00 31.04 0.79 total gas age n=11 7.21 0.22 5.96 0.47 plateau n=3 steps G-I 5.57 0.12 77.35 2.86 0.83 "3-88 hbl, A7:137, 12.78 mg hbl, J=0.0006918±0.11%, D=1.0069±0.001, NM-137, Lab#=52198-01" A 800 65.54 1.19 220.82 0.26 0.43 0.82 0.59 4.66 0.48 1.78 B 850 7.64 0.49 26.77 0.33 1.03 1.30 -2.98 10.51 -0.28 0.54 C 950 4.83 0.58 17.08 0.41 0.87 0.18 -3.61 17.72 -0.22 0.41 D 1020 8.04 0.86 24.45 0.25 0.60 1.41 11.05 22.12 1.11 0.63 E 1080 17.09 1.54 57.20 0.09 0.33 1.99 1.85 23.65 0.40 1.81 F 1120 24.57 2.28 87.56 0.05 0.22 3.59 -4.53 24.59 -1.39 2.56 G 1160 32.51 3.47 105.93 0.23 0.15 0.77 4.59 28.69 1.87 1.23 H 1200 25.11 4.06 86.25 0.85 0.13 0.37 -0.16 43.73 -0.05 0.59 I 1300 7.76 5.21 26.50 3.14 0.10 1.08 4.59 99.41 0.45 0.15 J 1400 82.65 24.96 284.75 0.02 0.02 -2.41 0.69 99.81 0.73 9.48 K 1650 138.10 14.42 493.24 0.01 0.04 1.57 -4.68 100.00 -8.19 24.86 total gas age n=11 5.65 0.26 0.34 0.53 plateau n=6 steps D-I 4.61 0.14 81.69 0.46 0.28 "BG-4 86-3 hbl, A2:137, 21.26 mg hbl, J=0.0006943±0.11%, D=1.0069±0.001, NM-137, Lab#=52193-01" A 800 428.65 1.67 1433.81 0.05 0.31 4.79 1.19 0.56 6.38 17.46 B 850 532.99 3.08 1838.25 0.01 0.17 -44.20 -1.87 0.62 -12.56 142.57 C 950 241.25 4.16 762.08 0.01 0.12 -9.50 6.80 0.70 20.50 48.60 D 1020 104.73 4.43 343.74 0.01 0.12 -1.00 3.36 0.79 4.42 23.52 E 1080 51.85 4.58 151.29 0.02 0.11 0.06 14.52 1.06 9.44 7.01 F 1120 24.32 4.75 64.39 0.06 0.11 -2.70 23.38 1.71 7.14 2.45 G 1160 10.05 4.77 17.54 0.31 0.11 0.80 52.35 5.35 6.60 0.42 H 1200 9.18 4.68 14.45 1.55 0.11 0.90 57.67 23.41 6.64 0.18 I 1300 6.21 4.73 4.31 6.37 0.11 0.81 85.81 97.47 6.69 0.05 J 1400 14.45 5.06 34.07 0.16 0.10 -0.54 33.24 99.36 6.03 1.06 K 1650 36.58 4.33 107.16 0.05 0.12 -2.47 14.41 100.00 6.62 2.81 total gas age n=11 8.60 0.11 6.67 0.40 plateau n=5 steps F-J 8.45 0.11 98.30 6.68 0.06 Notes: "Isotopic ratios corrected for blank, radioactive decay, and mass discrimination, not corrected for interferring reactions." Individual analyses show analytical error only; plateau and total gas age errors include error in J and irradiation parameters. Analyses in italics are excluded from final age calculations. Discrimination = 1.00684±0.00098 a.m.u. †=analyses excluded from plateau weighted mean age. ø=analyses excluded from inverse isochron age. K/Ca = molar ratio calculated from reactor produced 39ArK and 37ArCa. * 2s error ** MSWD outside of 95% confidence interval