data_x=2 _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common 'Europium Cadmium Antimonide/Arsenide' _chemical_melting_point 'Not Measured' _chemical_formula_moiety 'As2.41 Cd6 Eu11 Sb9.59' _chemical_formula_sum 'As4.82 Cd6 Eu11 Sb19.18' _chemical_formula_weight 3694.33 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cd' 'Cd' -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sb' 'Sb' -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Eu' 'Eu' -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting 'monoclinic' _symmetry_space_group_name_H-M 'C 1 2/m 1' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' _cell_length_a 32.1261(12) _cell_length_b 4.6788(2) _cell_length_c 12.2580(5) _cell_angle_alpha 90.00 _cell_angle_beta 109.5720(10) _cell_angle_gamma 90.00 _cell_volume 1736.06(12) _cell_formula_units_Z 2 _cell_measurement_temperature 89(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description 'needle like' _exptl_crystal_colour 'silver metalic' _exptl_crystal_size_max 0.045 _exptl_crystal_size_mid 0.043 _exptl_crystal_size_min 0.041 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_diffrn 7.067 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3099 _exptl_absorpt_coefficient_mu 32.691 _exptl_absorpt_correction_type 'Semi-Empirical Absorption Correction' _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details 'SADABS (Sheldrick, 2003)' _exptl_special_details ; ? ; _diffrn_ambient_temperature 89(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker Apex II' _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 12707 _diffrn_reflns_av_R_equivalents 0.0391 _diffrn_reflns_av_sigmaI/netI 0.0297 _diffrn_reflns_limit_h_min -43 _diffrn_reflns_limit_h_max 43 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 2.55 _diffrn_reflns_theta_max 29.13 _reflns_number_total 2599 _reflns_number_gt 2347 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 2008)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0134P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens "none" _refine_ls_hydrogen_treatment "none" _refine_ls_extinction_method SHELXL _refine_ls_extinction_coef 0.000298(9) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 2599 _refine_ls_number_parameters 94 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0252 _refine_ls_R_factor_gt 0.0213 _refine_ls_wR_factor_ref 0.0410 _refine_ls_wR_factor_gt 0.0399 _refine_ls_goodness_of_fit_ref 1.071 _refine_ls_restrained_S_all 1.071 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.001 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Eu1 Eu 0.018644(13) 0.0000 0.67999(3) 0.00727(9) Uani 1 2 d S . . Eu2 Eu 0.113194(13) 0.0000 0.50694(3) 0.00839(9) Uani 1 2 d S . . Eu3 Eu 0.125775(13) 0.0000 0.01143(3) 0.00845(9) Uani 1 2 d S . . Eu4 Eu 0.198969(13) 0.0000 0.33950(3) 0.00692(9) Uani 1 2 d S . . Eu5 Eu 0.281085(13) 0.0000 0.13458(3) 0.00779(9) Uani 1 2 d S . . Eu6 Eu 0.0000 0.0000 0.0000 0.00678(12) Uani 1 4 d S . . Sb1 Sb 0.090000(18) 0.0000 0.23216(5) 0.00566(18) Uani 0.711(7) 2 d SP . . As1 As 0.090000(18) 0.0000 0.23216(5) 0.00566(18) Uani 0.289(7) 2 d SP . . Sb2 Sb 0.14964(2) 0.0000 0.78146(5) 0.0057(2) Uani 0.396(6) 2 d SP . . As2 As 0.14964(2) 0.0000 0.78146(5) 0.0057(2) Uani 0.604(6) 2 d SP . . Sb3 Sb 0.309662(17) 0.0000 0.47187(4) 0.00605(11) Uani 1 2 d S . . Sb4 Sb 0.453371(17) 0.0000 0.11555(4) 0.00496(17) Uani 0.892(6) 2 d SP . . As4 As 0.453371(17) 0.0000 0.11555(4) 0.00496(17) Uani 0.108(6) 2 d SP . . Sb5 Sb 0.457077(18) 0.0000 0.49967(5) 0.00552(18) Uani 0.810(6) 2 d SP . . As5 As 0.457077(18) 0.0000 0.49967(5) 0.00552(18) Uani 0.190(6) 2 d SP . . Sb6 Sb 0.704329(16) 0.0000 0.13265(4) 0.00534(11) Uani 1 2 d S . . Cd1 Cd 0.219087(18) 0.0000 0.66638(5) 0.00728(12) Uani 1 2 d S . . Cd2 Cd 0.398094(19) 0.0000 0.25588(5) 0.00880(12) Uani 1 2 d S . . Cd3 Cd 0.548634(19) 0.0000 0.24563(5) 0.01032(13) Uani 1 2 d S . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Eu1 0.0103(2) 0.0052(2) 0.00555(19) 0.000 0.00159(15) 0.000 Eu2 0.00589(19) 0.0095(2) 0.0099(2) 0.000 0.00275(15) 0.000 Eu3 0.00637(19) 0.0077(2) 0.00947(19) 0.000 0.00031(15) 0.000 Eu4 0.00709(19) 0.0077(2) 0.00664(19) 0.000 0.00322(15) 0.000 Eu5 0.00763(19) 0.0081(2) 0.00823(19) 0.000 0.00338(15) 0.000 Eu6 0.0062(3) 0.0080(3) 0.0066(3) 0.000 0.0028(2) 0.000 Sb1 0.0051(3) 0.0059(3) 0.0056(3) 0.000 0.0013(2) 0.000 As1 0.0051(3) 0.0059(3) 0.0056(3) 0.000 0.0013(2) 0.000 Sb2 0.0059(3) 0.0052(4) 0.0063(3) 0.000 0.0026(3) 0.000 As2 0.0059(3) 0.0052(4) 0.0063(3) 0.000 0.0026(3) 0.000 Sb3 0.0067(2) 0.0045(3) 0.0068(2) 0.000 0.00201(19) 0.000 Sb4 0.0047(3) 0.0046(3) 0.0057(3) 0.000 0.0018(2) 0.000 As4 0.0047(3) 0.0046(3) 0.0057(3) 0.000 0.0018(2) 0.000 Sb5 0.0059(3) 0.0051(3) 0.0054(3) 0.000 0.0017(2) 0.000 As5 0.0059(3) 0.0051(3) 0.0054(3) 0.000 0.0017(2) 0.000 Sb6 0.0049(2) 0.0052(3) 0.0054(2) 0.000 0.00111(19) 0.000 Cd1 0.0073(3) 0.0062(3) 0.0062(3) 0.000 -0.0005(2) 0.000 Cd2 0.0061(3) 0.0117(3) 0.0084(3) 0.000 0.0022(2) 0.000 Cd3 0.0093(3) 0.0086(3) 0.0114(3) 0.000 0.0014(2) 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Eu1 As4 3.3246(5) 7_556 ? Eu1 Sb4 3.3246(5) 7_556 ? Eu1 As4 3.3246(5) 7_546 ? Eu1 Sb4 3.3246(5) 7_546 ? Eu1 As5 3.3677(5) 3_445 ? Eu1 Sb5 3.3677(5) 3_445 ? Eu1 As5 3.3677(5) 3_455 ? Eu1 Sb5 3.3677(5) 3_455 ? Eu1 Cd2 3.4405(5) 7_556 ? Eu1 Cd2 3.4405(5) 7_546 ? Eu1 As5 3.4759(5) 7_546 ? Eu1 Sb5 3.4759(5) 7_546 ? Eu2 Sb2 3.1710(8) . ? Eu2 Sb1 3.1967(7) . ? Eu2 As5 3.2332(5) 7_546 ? Eu2 Sb5 3.2332(5) 7_546 ? Eu2 As5 3.2331(5) 7_556 ? Eu2 Sb5 3.2331(5) 7_556 ? Eu2 Cd1 3.3073(7) . ? Eu2 Sb3 3.3543(5) 7_556 ? Eu2 Sb3 3.3543(5) 7_546 ? Eu2 Cd2 3.8422(6) 7_556 ? Eu3 As2 3.1596(8) 1_554 ? Eu3 Sb2 3.1596(8) 1_554 ? Eu3 Sb1 3.2749(7) . ? Eu3 Sb6 3.3967(5) 3_455 ? Eu3 Sb6 3.3966(5) 3_445 ? Eu3 As4 3.4218(5) 7_545 ? Eu3 Sb4 3.4218(5) 7_545 ? Eu3 As4 3.4218(5) 7 ? Eu3 Sb4 3.4218(5) 7 ? Eu3 Cd2 3.8878(6) 7_545 ? Eu3 Cd2 3.8878(6) 7 ? Eu4 Sb1 3.3016(7) . ? Eu4 Sb3 3.3653(5) 7_556 ? Eu4 Sb3 3.3653(5) 7_546 ? Eu4 Sb3 3.3783(6) . ? Eu4 Sb6 3.4963(5) 3_445 ? Eu4 Sb6 3.4963(5) 3_455 ? Eu4 Cd1 3.5406(5) 7_556 ? Eu4 Cd1 3.5406(5) 7_546 ? Eu4 Cd1 3.8390(7) . ? Eu5 As2 3.1544(5) 7_556 ? Eu5 Sb2 3.1544(5) 7_556 ? Eu5 As2 3.1544(5) 7_546 ? Eu5 Sb2 3.1544(5) 7_546 ? Eu5 Cd1 3.3815(5) 7_556 ? Eu5 Cd1 3.3815(5) 7_546 ? Eu5 Sb6 3.3934(5) 3_445 ? Eu5 Sb6 3.3934(5) 3_455 ? Eu5 Sb6 3.4610(7) 5_655 ? Eu5 Cd2 3.5492(7) . ? Eu5 Eu5 3.9915(6) 7_545 ? Eu5 Eu5 3.9915(6) 7 ? Eu6 Sb1 3.3085(5) . ? Eu6 As1 3.3085(5) 5 ? Eu6 Sb1 3.3085(5) 5 ? Eu6 As4 3.3384(4) 7 ? Eu6 As4 3.3384(4) 3_445 ? Eu6 Sb4 3.3384(4) 7 ? Eu6 Sb4 3.3384(4) 3_445 ? Eu6 As4 3.3384(4) 7_545 ? Eu6 As4 3.3384(4) 3_455 ? Eu6 Sb4 3.3384(4) 3_455 ? Eu6 Sb4 3.3384(4) 7_545 ? Sb1 Cd3 2.7227(4) 3_445 ? Sb1 Cd3 2.7227(4) 3_455 ? Sb2 Cd2 2.7502(5) 7_546 ? Sb2 Cd2 2.7502(5) 7_556 ? Sb2 Cd1 3.0127(9) . ? Sb2 Eu5 3.1545(5) 7_556 ? Sb2 Eu5 3.1545(5) 7_546 ? Sb2 Eu3 3.1595(8) 1_556 ? Sb3 Cd1 2.8546(4) 7_546 ? Sb3 Cd1 2.8546(4) 7_556 ? Sb3 Eu2 3.3543(5) 7_556 ? Sb3 Eu2 3.3543(5) 7_546 ? Sb3 Eu4 3.3654(5) 7_556 ? Sb3 Eu4 3.3654(5) 7_546 ? Sb4 Cd2 2.8565(8) . ? Sb4 Cd3 2.9393(8) . ? Sb4 Eu1 3.3246(5) 7_556 ? Sb4 Eu1 3.3246(5) 7_546 ? Sb4 Eu6 3.3384(4) 3 ? Sb4 Eu6 3.3384(4) 3_545 ? Sb4 Eu3 3.4219(5) 7_545 ? Sb4 Eu3 3.4219(5) 7 ? Sb5 As5 2.7552(11) 5_656 ? Sb5 Sb5 2.7552(11) 5_656 ? Sb5 Cd2 2.9542(8) . ? Sb5 Cd3 3.1882(8) 5_656 ? Sb5 Eu2 3.2331(5) 7_546 ? Sb5 Eu2 3.2331(5) 7_556 ? Sb5 Eu1 3.3677(5) 3 ? Sb5 Eu1 3.3677(5) 3_545 ? Sb5 Eu1 3.4759(5) 7_546 ? Sb5 Eu1 3.4758(5) 7_556 ? Sb6 Cd1 2.8392(7) 5_656 ? Sb6 Eu5 3.3933(5) 3 ? Sb6 Eu5 3.3933(5) 3_545 ? Sb6 Eu3 3.3966(5) 3_545 ? Sb6 Eu3 3.3966(5) 3 ? Sb6 Eu5 3.4610(7) 5_655 ? Sb6 Eu4 3.4962(5) 3 ? Sb6 Eu4 3.4962(5) 3_545 ? Cd1 Sb6 2.8392(7) 5_656 ? Cd1 Sb3 2.8547(4) 7_546 ? Cd1 Sb3 2.8547(4) 7_556 ? Cd1 Eu5 3.3815(5) 7_556 ? Cd1 Eu5 3.3815(5) 7_546 ? Cd1 Eu4 3.5404(5) 7_556 ? Cd1 Eu4 3.5404(5) 7_546 ? Cd2 As2 2.7503(5) 7_546 ? Cd2 Sb2 2.7503(5) 7_546 ? Cd2 As2 2.7503(5) 7_556 ? Cd2 Sb2 2.7503(5) 7_556 ? Cd2 Eu1 3.4404(5) 7_556 ? Cd2 Eu1 3.4404(5) 7_546 ? Cd2 Eu2 3.8422(6) 7_556 ? Cd3 As1 2.7227(4) 3 ? Cd3 Sb1 2.7227(4) 3 ? Cd3 As1 2.7227(4) 3_545 ? Cd3 Sb1 2.7227(4) 3_545 ? Cd3 As5 3.1882(8) 5_656 ? Cd3 Sb5 3.1882(8) 5_656 ? Cd3 Eu1 3.5067(5) 7_546 ? Cd3 Eu1 3.5067(5) 7_556 ? Cd3 Eu6 3.7186(5) 3_545 ? Cd3 Eu6 3.7186(5) 3 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag As4 Eu1 Sb4 0.00(2) 7_556 7_556 ? As4 Eu1 As4 89.443(16) 7_556 7_546 ? Sb4 Eu1 As4 89.443(16) 7_556 7_546 ? As4 Eu1 Sb4 89.443(16) 7_556 7_546 ? Sb4 Eu1 Sb4 89.443(16) 7_556 7_546 ? As4 Eu1 Sb4 0.000(19) 7_546 7_546 ? As4 Eu1 As5 159.170(19) 7_556 3_445 ? Sb4 Eu1 As5 159.170(19) 7_556 3_445 ? As4 Eu1 As5 87.537(10) 7_546 3_445 ? Sb4 Eu1 As5 87.537(10) 7_546 3_445 ? As4 Eu1 Sb5 159.170(19) 7_556 3_445 ? Sb4 Eu1 Sb5 159.170(19) 7_556 3_445 ? As4 Eu1 Sb5 87.537(10) 7_546 3_445 ? Sb4 Eu1 Sb5 87.537(10) 7_546 3_445 ? As5 Eu1 Sb5 0.000(18) 3_445 3_445 ? As4 Eu1 As5 87.537(10) 7_556 3_455 ? Sb4 Eu1 As5 87.537(10) 7_556 3_455 ? As4 Eu1 As5 159.170(19) 7_546 3_455 ? Sb4 Eu1 As5 159.170(19) 7_546 3_455 ? As5 Eu1 As5 88.001(16) 3_445 3_455 ? Sb5 Eu1 As5 88.001(16) 3_445 3_455 ? As4 Eu1 Sb5 87.537(10) 7_556 3_455 ? Sb4 Eu1 Sb5 87.537(10) 7_556 3_455 ? As4 Eu1 Sb5 159.170(19) 7_546 3_455 ? Sb4 Eu1 Sb5 159.170(19) 7_546 3_455 ? As5 Eu1 Sb5 88.001(16) 3_445 3_455 ? Sb5 Eu1 Sb5 88.001(16) 3_445 3_455 ? As5 Eu1 Sb5 0.00(3) 3_455 3_455 ? As4 Eu1 Cd2 49.916(13) 7_556 7_556 ? Sb4 Eu1 Cd2 49.916(13) 7_556 7_556 ? As4 Eu1 Cd2 108.241(15) 7_546 7_556 ? Sb4 Eu1 Cd2 108.241(15) 7_546 7_556 ? As5 Eu1 Cd2 149.658(18) 3_445 7_556 ? Sb5 Eu1 Cd2 149.658(18) 3_445 7_556 ? As5 Eu1 Cd2 85.316(11) 3_455 7_556 ? Sb5 Eu1 Cd2 85.316(11) 3_455 7_556 ? As4 Eu1 Cd2 108.241(15) 7_556 7_546 ? Sb4 Eu1 Cd2 108.241(15) 7_556 7_546 ? As4 Eu1 Cd2 49.916(13) 7_546 7_546 ? Sb4 Eu1 Cd2 49.916(13) 7_546 7_546 ? As5 Eu1 Cd2 85.316(11) 3_445 7_546 ? Sb5 Eu1 Cd2 85.316(11) 3_445 7_546 ? As5 Eu1 Cd2 149.658(18) 3_455 7_546 ? Sb5 Eu1 Cd2 149.658(18) 3_455 7_546 ? Cd2 Eu1 Cd2 85.681(16) 7_556 7_546 ? As4 Eu1 As5 152.850(18) 7_556 7_546 ? Sb4 Eu1 As5 152.850(18) 7_556 7_546 ? As4 Eu1 As5 86.712(10) 7_546 7_546 ? Sb4 Eu1 As5 86.712(10) 7_546 7_546 ? As5 Eu1 As5 47.448(17) 3_445 7_546 ? Sb5 Eu1 As5 47.448(17) 3_445 7_546 ? As5 Eu1 As5 104.999(12) 3_455 7_546 ? Sb5 Eu1 As5 104.999(12) 3_455 7_546 ? Cd2 Eu1 As5 106.265(16) 7_556 7_546 ? Cd2 Eu1 As5 50.567(13) 7_546 7_546 ? As4 Eu1 Sb5 152.850(18) 7_556 7_546 ? Sb4 Eu1 Sb5 152.850(18) 7_556 7_546 ? As4 Eu1 Sb5 86.712(10) 7_546 7_546 ? Sb4 Eu1 Sb5 86.712(10) 7_546 7_546 ? As5 Eu1 Sb5 47.448(17) 3_445 7_546 ? Sb5 Eu1 Sb5 47.448(17) 3_445 7_546 ? As5 Eu1 Sb5 104.999(12) 3_455 7_546 ? Sb5 Eu1 Sb5 104.999(12) 3_455 7_546 ? Cd2 Eu1 Sb5 106.265(16) 7_556 7_546 ? Cd2 Eu1 Sb5 50.567(13) 7_546 7_546 ? As5 Eu1 Sb5 0.000(17) 7_546 7_546 ? Sb2 Eu2 Sb1 172.33(2) . . ? Sb2 Eu2 As5 91.897(15) . 7_546 ? Sb1 Eu2 As5 93.396(14) . 7_546 ? Sb2 Eu2 Sb5 91.897(15) . 7_546 ? Sb1 Eu2 Sb5 93.396(14) . 7_546 ? As5 Eu2 Sb5 0.00(3) 7_546 7_546 ? Sb2 Eu2 As5 91.897(15) . 7_556 ? Sb1 Eu2 As5 93.396(14) . 7_556 ? As5 Eu2 As5 92.700(17) 7_546 7_556 ? Sb5 Eu2 As5 92.700(17) 7_546 7_556 ? Sb2 Eu2 Sb5 91.897(15) . 7_556 ? Sb1 Eu2 Sb5 93.396(14) . 7_556 ? As5 Eu2 Sb5 92.700(17) 7_546 7_556 ? Sb5 Eu2 Sb5 92.700(17) 7_546 7_556 ? As5 Eu2 Sb5 0.000(15) 7_556 7_556 ? Sb2 Eu2 Cd1 55.378(16) . . ? Sb1 Eu2 Cd1 116.949(19) . . ? As5 Eu2 Cd1 125.887(12) 7_546 . ? Sb5 Eu2 Cd1 125.887(12) 7_546 . ? As5 Eu2 Cd1 125.887(12) 7_556 . ? Sb5 Eu2 Cd1 125.887(12) 7_556 . ? Sb2 Eu2 Sb3 85.253(14) . 7_556 ? Sb1 Eu2 Sb3 89.253(14) . 7_556 ? As5 Eu2 Sb3 176.539(17) 7_546 7_556 ? Sb5 Eu2 Sb3 176.539(17) 7_546 7_556 ? As5 Eu2 Sb3 89.364(10) 7_556 7_556 ? Sb5 Eu2 Sb3 89.364(10) 7_556 7_556 ? Cd1 Eu2 Sb3 50.742(10) . 7_556 ? Sb2 Eu2 Sb3 85.253(14) . 7_546 ? Sb1 Eu2 Sb3 89.253(14) . 7_546 ? As5 Eu2 Sb3 89.364(10) 7_546 7_546 ? Sb5 Eu2 Sb3 89.364(10) 7_546 7_546 ? As5 Eu2 Sb3 176.539(17) 7_556 7_546 ? Sb5 Eu2 Sb3 176.539(17) 7_556 7_546 ? Cd1 Eu2 Sb3 50.742(10) . 7_546 ? Sb3 Eu2 Sb3 88.443(16) 7_556 7_546 ? Sb2 Eu2 Cd2 44.920(10) . 7_556 ? Sb1 Eu2 Cd2 138.547(9) . 7_556 ? As5 Eu2 Cd2 102.559(15) 7_546 7_556 ? Sb5 Eu2 Cd2 102.559(15) 7_546 7_556 ? As5 Eu2 Cd2 48.419(12) 7_556 7_556 ? Sb5 Eu2 Cd2 48.419(12) 7_556 7_556 ? Cd1 Eu2 Cd2 83.799(14) . 7_556 ? Sb3 Eu2 Cd2 76.781(12) 7_556 7_556 ? Sb3 Eu2 Cd2 128.362(16) 7_546 7_556 ? As2 Eu3 Sb2 0.00(2) 1_554 1_554 ? As2 Eu3 Sb1 173.91(2) 1_554 . ? Sb2 Eu3 Sb1 173.91(2) 1_554 . ? As2 Eu3 Sb6 91.347(15) 1_554 3_455 ? Sb2 Eu3 Sb6 91.347(15) 1_554 3_455 ? Sb1 Eu3 Sb6 93.067(14) . 3_455 ? As2 Eu3 Sb6 91.347(15) 1_554 3_445 ? Sb2 Eu3 Sb6 91.347(15) 1_554 3_445 ? Sb1 Eu3 Sb6 93.067(14) . 3_445 ? Sb6 Eu3 Sb6 87.061(15) 3_455 3_445 ? As2 Eu3 As4 87.684(15) 1_554 7_545 ? Sb2 Eu3 As4 87.684(15) 1_554 7_545 ? Sb1 Eu3 As4 87.872(14) . 7_545 ? Sb6 Eu3 As4 178.963(17) 3_455 7_545 ? Sb6 Eu3 As4 93.331(9) 3_445 7_545 ? As2 Eu3 Sb4 87.684(15) 1_554 7_545 ? Sb2 Eu3 Sb4 87.684(15) 1_554 7_545 ? Sb1 Eu3 Sb4 87.872(14) . 7_545 ? Sb6 Eu3 Sb4 178.963(17) 3_455 7_545 ? Sb6 Eu3 Sb4 93.331(9) 3_445 7_545 ? As4 Eu3 Sb4 0.00(3) 7_545 7_545 ? As2 Eu3 As4 87.684(15) 1_554 7 ? Sb2 Eu3 As4 87.684(15) 1_554 7 ? Sb1 Eu3 As4 87.872(14) . 7 ? Sb6 Eu3 As4 93.331(9) 3_455 7 ? Sb6 Eu3 As4 178.963(17) 3_445 7 ? As4 Eu3 As4 86.262(15) 7_545 7 ? Sb4 Eu3 As4 86.262(15) 7_545 7 ? As2 Eu3 Sb4 87.684(15) 1_554 7 ? Sb2 Eu3 Sb4 87.684(15) 1_554 7 ? Sb1 Eu3 Sb4 87.872(14) . 7 ? Sb6 Eu3 Sb4 93.331(9) 3_455 7 ? Sb6 Eu3 Sb4 178.963(17) 3_445 7 ? As4 Eu3 Sb4 86.262(15) 7_545 7 ? Sb4 Eu3 Sb4 86.262(15) 7_545 7 ? As4 Eu3 Sb4 0.000(15) 7 7 ? As2 Eu3 Cd2 44.463(10) 1_554 7_545 ? Sb2 Eu3 Cd2 44.463(10) 1_554 7_545 ? Sb1 Eu3 Cd2 132.193(12) . 7_545 ? Sb6 Eu3 Cd2 133.711(16) 3_455 7_545 ? Sb6 Eu3 Cd2 82.076(11) 3_445 7_545 ? As4 Eu3 Cd2 45.454(12) 7_545 7_545 ? Sb4 Eu3 Cd2 45.454(12) 7_545 7_545 ? As4 Eu3 Cd2 96.966(14) 7 7_545 ? Sb4 Eu3 Cd2 96.966(14) 7 7_545 ? As2 Eu3 Cd2 44.463(10) 1_554 7 ? Sb2 Eu3 Cd2 44.463(10) 1_554 7 ? Sb1 Eu3 Cd2 132.193(12) . 7 ? Sb6 Eu3 Cd2 82.076(11) 3_455 7 ? Sb6 Eu3 Cd2 133.711(16) 3_445 7 ? As4 Eu3 Cd2 96.966(14) 7_545 7 ? Sb4 Eu3 Cd2 96.966(14) 7_545 7 ? As4 Eu3 Cd2 45.454(12) 7 7 ? Sb4 Eu3 Cd2 45.454(12) 7 7 ? Cd2 Eu3 Cd2 73.988(13) 7_545 7 ? Sb1 Eu4 Sb3 87.329(14) . 7_556 ? Sb1 Eu4 Sb3 87.329(14) . 7_546 ? Sb3 Eu4 Sb3 88.078(16) 7_556 7_546 ? Sb1 Eu4 Sb3 175.149(18) . . ? Sb3 Eu4 Sb3 89.184(13) 7_556 . ? Sb3 Eu4 Sb3 89.185(14) 7_546 . ? Sb1 Eu4 Sb6 90.815(13) . 3_445 ? Sb3 Eu4 Sb6 177.202(15) 7_556 3_445 ? Sb3 Eu4 Sb6 93.930(9) 7_546 3_445 ? Sb3 Eu4 Sb6 92.789(13) . 3_445 ? Sb1 Eu4 Sb6 90.815(13) . 3_455 ? Sb3 Eu4 Sb6 93.930(9) 7_556 3_455 ? Sb3 Eu4 Sb6 177.202(15) 7_546 3_455 ? Sb3 Eu4 Sb6 92.789(13) . 3_455 ? Sb6 Eu4 Sb6 83.997(14) 3_445 3_455 ? Sb1 Eu4 Cd1 133.492(10) . 7_556 ? Sb3 Eu4 Cd1 77.739(12) 7_556 7_556 ? Sb3 Eu4 Cd1 134.932(16) 7_546 7_556 ? Sb3 Eu4 Cd1 48.665(10) . 7_556 ? Sb6 Eu4 Cd1 102.108(15) 3_445 7_556 ? Sb6 Eu4 Cd1 47.587(12) 3_455 7_556 ? Sb1 Eu4 Cd1 133.492(10) . 7_546 ? Sb3 Eu4 Cd1 134.932(16) 7_556 7_546 ? Sb3 Eu4 Cd1 77.739(12) 7_546 7_546 ? Sb3 Eu4 Cd1 48.665(10) . 7_546 ? Sb6 Eu4 Cd1 47.587(12) 3_445 7_546 ? Sb6 Eu4 Cd1 102.108(15) 3_455 7_546 ? Cd1 Eu4 Cd1 82.713(15) 7_556 7_546 ? Sb1 Eu4 Cd1 101.610(16) . . ? Sb3 Eu4 Cd1 46.108(8) 7_556 . ? Sb3 Eu4 Cd1 46.108(8) 7_546 . ? Sb3 Eu4 Cd1 73.539(14) . . ? Sb6 Eu4 Cd1 136.465(8) 3_445 . ? Sb6 Eu4 Cd1 136.465(8) 3_455 . ? Cd1 Eu4 Cd1 98.911(13) 7_556 . ? Cd1 Eu4 Cd1 98.911(13) 7_546 . ? Sb1 Eu4 Eu3 53.100(13) . . ? Sb3 Eu4 Eu3 123.071(11) 7_556 . ? Sb3 Eu4 Eu3 123.071(11) 7_546 . ? Sb3 Eu4 Eu3 131.751(15) . . ? Sb6 Eu4 Eu3 54.151(9) 3_445 . ? Sb6 Eu4 Eu3 54.151(9) 3_455 . ? Cd1 Eu4 Eu3 100.003(13) 7_556 . ? Cd1 Eu4 Eu3 100.003(13) 7_546 . ? Cd1 Eu4 Eu3 154.710(15) . . ? Sb1 Eu4 Eu2 51.376(13) . . ? Sb3 Eu4 Eu2 53.877(10) 7_556 . ? Sb3 Eu4 Eu2 53.877(10) 7_546 . ? Sb3 Eu4 Eu2 123.773(15) . . ? Sb6 Eu4 Eu2 126.113(11) 3_445 . ? Sb6 Eu4 Eu2 126.113(11) 3_455 . ? Cd1 Eu4 Eu2 131.578(10) 7_556 . ? Cd1 Eu4 Eu2 131.578(10) 7_546 . ? Cd1 Eu4 Eu2 50.234(11) . . ? Eu3 Eu4 Eu2 104.476(12) . . ? As2 Eu5 Sb2 0.00(2) 7_556 7_556 ? As2 Eu5 As2 95.74(2) 7_556 7_546 ? Sb2 Eu5 As2 95.74(2) 7_556 7_546 ? As2 Eu5 Sb2 95.74(2) 7_556 7_546 ? Sb2 Eu5 Sb2 95.74(2) 7_556 7_546 ? As2 Eu5 Sb2 0.00(3) 7_546 7_546 ? As2 Eu5 Cd1 54.759(15) 7_556 7_556 ? Sb2 Eu5 Cd1 54.759(15) 7_556 7_556 ? As2 Eu5 Cd1 116.689(18) 7_546 7_556 ? Sb2 Eu5 Cd1 116.689(18) 7_546 7_556 ? As2 Eu5 Cd1 116.689(18) 7_556 7_546 ? Sb2 Eu5 Cd1 116.689(18) 7_556 7_546 ? As2 Eu5 Cd1 54.759(15) 7_546 7_546 ? Sb2 Eu5 Cd1 54.759(15) 7_546 7_546 ? Cd1 Eu5 Cd1 87.548(17) 7_556 7_546 ? As2 Eu5 Sb6 160.937(19) 7_556 3_445 ? Sb2 Eu5 Sb6 160.937(19) 7_556 3_445 ? As2 Eu5 Sb6 85.560(11) 7_546 3_445 ? Sb2 Eu5 Sb6 85.560(11) 7_546 3_445 ? Cd1 Eu5 Sb6 107.766(16) 7_556 3_445 ? Cd1 Eu5 Sb6 49.553(12) 7_546 3_445 ? As2 Eu5 Sb6 85.560(11) 7_556 3_455 ? Sb2 Eu5 Sb6 85.560(11) 7_556 3_455 ? As2 Eu5 Sb6 160.937(19) 7_546 3_455 ? Sb2 Eu5 Sb6 160.937(19) 7_546 3_455 ? Cd1 Eu5 Sb6 49.553(12) 7_556 3_455 ? Cd1 Eu5 Sb6 107.766(16) 7_546 3_455 ? Sb6 Eu5 Sb6 87.166(15) 3_445 3_455 ? As2 Eu5 Sb6 90.253(15) 7_556 5_655 ? Sb2 Eu5 Sb6 90.253(15) 7_556 5_655 ? As2 Eu5 Sb6 90.253(15) 7_546 5_655 ? Sb2 Eu5 Sb6 90.253(15) 7_546 5_655 ? Cd1 Eu5 Sb6 135.755(9) 7_556 5_655 ? Cd1 Eu5 Sb6 135.755(9) 7_546 5_655 ? Sb6 Eu5 Sb6 108.778(12) 3_445 5_655 ? Sb6 Eu5 Sb6 108.778(12) 3_455 5_655 ? As2 Eu5 Cd2 47.999(10) 7_556 . ? Sb2 Eu5 Cd2 47.999(10) 7_556 . ? As2 Eu5 Cd2 47.999(10) 7_546 . ? Sb2 Eu5 Cd2 47.999(10) 7_546 . ? Cd1 Eu5 Cd2 87.431(14) 7_556 . ? Cd1 Eu5 Cd2 87.431(14) 7_546 . ? Sb6 Eu5 Cd2 131.920(10) 3_445 . ? Sb6 Eu5 Cd2 131.920(10) 3_455 . ? Sb6 Eu5 Cd2 86.350(15) 5_655 . ? As2 Eu5 Eu5 143.84(2) 7_556 7_545 ? Sb2 Eu5 Eu5 143.84(2) 7_556 7_545 ? As2 Eu5 Eu5 86.445(11) 7_546 7_545 ? Sb2 Eu5 Eu5 86.445(11) 7_546 7_545 ? Cd1 Eu5 Eu5 151.711(19) 7_556 7_545 ? Cd1 Eu5 Eu5 93.993(9) 7_546 7_545 ? Sb6 Eu5 Eu5 55.179(11) 3_445 7_545 ? Sb6 Eu5 Eu5 103.716(16) 3_455 7_545 ? Sb6 Eu5 Eu5 53.599(11) 5_655 7_545 ? Cd2 Eu5 Eu5 120.848(15) . 7_545 ? As2 Eu5 Eu5 86.445(11) 7_556 7 ? Sb2 Eu5 Eu5 86.445(11) 7_556 7 ? As2 Eu5 Eu5 143.84(2) 7_546 7 ? Sb2 Eu5 Eu5 143.84(2) 7_546 7 ? Cd1 Eu5 Eu5 93.993(9) 7_556 7 ? Cd1 Eu5 Eu5 151.711(19) 7_546 7 ? Sb6 Eu5 Eu5 103.716(16) 3_445 7 ? Sb6 Eu5 Eu5 55.179(11) 3_455 7 ? Sb6 Eu5 Eu5 53.599(11) 5_655 7 ? Cd2 Eu5 Eu5 120.848(15) . 7 ? Eu5 Eu5 Eu5 71.761(13) 7_545 7 ? Sb1 Eu6 As1 180.0 . 5 ? Sb1 Eu6 Sb1 180.0 . 5 ? As1 Eu6 Sb1 0.00(3) 5 5 ? Sb1 Eu6 As4 88.733(11) . 7 ? As1 Eu6 As4 91.267(11) 5 7 ? Sb1 Eu6 As4 91.267(11) 5 7 ? Sb1 Eu6 As4 91.267(11) . 3_445 ? As1 Eu6 As4 88.733(11) 5 3_445 ? Sb1 Eu6 As4 88.733(11) 5 3_445 ? As4 Eu6 As4 180.000(18) 7 3_445 ? Sb1 Eu6 Sb4 88.733(11) . 7 ? As1 Eu6 Sb4 91.267(11) 5 7 ? Sb1 Eu6 Sb4 91.267(11) 5 7 ? As4 Eu6 Sb4 0.000(18) 7 7 ? As4 Eu6 Sb4 180.000(15) 3_445 7 ? Sb1 Eu6 Sb4 91.267(11) . 3_445 ? As1 Eu6 Sb4 88.733(11) 5 3_445 ? Sb1 Eu6 Sb4 88.733(11) 5 3_445 ? As4 Eu6 Sb4 180.000(18) 7 3_445 ? As4 Eu6 Sb4 0.000(15) 3_445 3_445 ? Sb4 Eu6 Sb4 180.000(18) 7 3_445 ? Sb1 Eu6 As4 88.733(11) . 7_545 ? As1 Eu6 As4 91.267(11) 5 7_545 ? Sb1 Eu6 As4 91.267(11) 5 7_545 ? As4 Eu6 As4 88.977(13) 7 7_545 ? As4 Eu6 As4 91.023(13) 3_445 7_545 ? Sb4 Eu6 As4 88.977(13) 7 7_545 ? Sb4 Eu6 As4 91.023(13) 3_445 7_545 ? Sb1 Eu6 As4 91.267(11) . 3_455 ? As1 Eu6 As4 88.733(11) 5 3_455 ? Sb1 Eu6 As4 88.733(11) 5 3_455 ? As4 Eu6 As4 91.023(13) 7 3_455 ? As4 Eu6 As4 88.977(13) 3_445 3_455 ? Sb4 Eu6 As4 91.023(13) 7 3_455 ? Sb4 Eu6 As4 88.977(13) 3_445 3_455 ? As4 Eu6 As4 180.000(18) 7_545 3_455 ? Sb1 Eu6 Sb4 91.267(11) . 3_455 ? As1 Eu6 Sb4 88.733(11) 5 3_455 ? Sb1 Eu6 Sb4 88.733(11) 5 3_455 ? As4 Eu6 Sb4 91.023(13) 7 3_455 ? As4 Eu6 Sb4 88.977(13) 3_445 3_455 ? Sb4 Eu6 Sb4 91.023(13) 7 3_455 ? Sb4 Eu6 Sb4 88.977(13) 3_445 3_455 ? As4 Eu6 Sb4 180.000(18) 7_545 3_455 ? As4 Eu6 Sb4 0.000(18) 3_455 3_455 ? Sb1 Eu6 Sb4 88.733(11) . 7_545 ? As1 Eu6 Sb4 91.267(11) 5 7_545 ? Sb1 Eu6 Sb4 91.267(11) 5 7_545 ? As4 Eu6 Sb4 88.977(13) 7 7_545 ? As4 Eu6 Sb4 91.023(13) 3_445 7_545 ? Sb4 Eu6 Sb4 88.977(13) 7 7_545 ? Sb4 Eu6 Sb4 91.023(13) 3_445 7_545 ? As4 Eu6 Sb4 0.000(18) 7_545 7_545 ? As4 Eu6 Sb4 180.000(18) 3_455 7_545 ? Sb4 Eu6 Sb4 180.000(18) 3_455 7_545 ? Cd3 Sb1 Cd3 118.46(3) 3_445 3_455 ? Cd3 Sb1 Eu2 83.242(17) 3_445 . ? Cd3 Sb1 Eu2 83.242(17) 3_455 . ? Cd3 Sb1 Eu3 111.322(17) 3_445 . ? Cd3 Sb1 Eu3 111.322(17) 3_455 . ? Eu2 Sb1 Eu3 148.00(2) . . ? Cd3 Sb1 Eu4 116.726(16) 3_445 . ? Cd3 Sb1 Eu4 116.726(16) 3_455 . ? Eu2 Sb1 Eu4 74.830(15) . . ? Eu3 Sb1 Eu4 73.174(15) . . ? Cd3 Sb1 Eu6 75.435(16) 3_445 . ? Cd3 Sb1 Eu6 75.435(16) 3_455 . ? Eu2 Sb1 Eu6 137.26(2) . . ? Eu3 Sb1 Eu6 74.739(14) . . ? Eu4 Sb1 Eu6 147.91(2) . . ? Cd2 Sb2 Cd2 116.56(3) 7_546 7_556 ? Cd2 Sb2 Cd1 112.404(19) 7_546 . ? Cd2 Sb2 Cd1 112.404(19) 7_556 . ? Cd2 Sb2 Eu5 168.03(2) 7_546 7_556 ? Cd2 Sb2 Eu5 73.537(12) 7_556 7_556 ? Cd1 Sb2 Eu5 66.455(15) . 7_556 ? Cd2 Sb2 Eu5 73.537(12) 7_546 7_546 ? Cd2 Sb2 Eu5 168.03(2) 7_556 7_546 ? Cd1 Sb2 Eu5 66.455(15) . 7_546 ? Eu5 Sb2 Eu5 95.74(2) 7_556 7_546 ? Cd2 Sb2 Eu3 81.959(19) 7_546 1_556 ? Cd2 Sb2 Eu3 81.959(19) 7_556 1_556 ? Cd1 Sb2 Eu3 148.97(3) . 1_556 ? Eu5 Sb2 Eu3 93.696(16) 7_556 1_556 ? Eu5 Sb2 Eu3 93.696(16) 7_546 1_556 ? Cd2 Sb2 Eu2 80.576(18) 7_546 . ? Cd2 Sb2 Eu2 80.576(18) 7_556 . ? Cd1 Sb2 Eu2 64.607(18) . . ? Eu5 Sb2 Eu2 108.395(17) 7_556 . ? Eu5 Sb2 Eu2 108.395(17) 7_546 . ? Eu3 Sb2 Eu2 146.42(2) 1_556 . ? Cd1 Sb3 Cd1 110.07(2) 7_546 7_556 ? Cd1 Sb3 Eu2 134.53(2) 7_546 7_556 ? Cd1 Sb3 Eu2 63.777(13) 7_556 7_556 ? Cd1 Sb3 Eu2 63.777(13) 7_546 7_546 ? Cd1 Sb3 Eu2 134.53(2) 7_556 7_546 ? Eu2 Sb3 Eu2 88.442(16) 7_556 7_546 ? Cd1 Sb3 Eu4 153.23(2) 7_546 7_556 ? Cd1 Sb3 Eu4 75.727(12) 7_556 7_556 ? Eu2 Sb3 Eu4 71.990(10) 7_556 7_556 ? Eu2 Sb3 Eu4 131.333(18) 7_546 7_556 ? Cd1 Sb3 Eu4 75.727(12) 7_546 7_546 ? Cd1 Sb3 Eu4 153.23(2) 7_556 7_546 ? Eu2 Sb3 Eu4 131.333(18) 7_556 7_546 ? Eu2 Sb3 Eu4 71.990(10) 7_546 7_546 ? Eu4 Sb3 Eu4 88.076(16) 7_556 7_546 ? Cd1 Sb3 Eu4 68.636(15) 7_546 . ? Cd1 Sb3 Eu4 68.636(15) 7_556 . ? Eu2 Sb3 Eu4 131.972(10) 7_556 . ? Eu2 Sb3 Eu4 131.972(10) 7_546 . ? Eu4 Sb3 Eu4 90.814(14) 7_556 . ? Eu4 Sb3 Eu4 90.814(14) 7_546 . ? Cd2 Sb4 Cd3 114.69(2) . . ? Cd2 Sb4 Eu1 67.148(14) . 7_556 ? Cd3 Sb4 Eu1 67.764(13) . 7_556 ? Cd2 Sb4 Eu1 67.148(14) . 7_546 ? Cd3 Sb4 Eu1 67.764(13) . 7_546 ? Eu1 Sb4 Eu1 89.442(16) 7_556 7_546 ? Cd2 Sb4 Eu6 135.510(6) . 3 ? Cd3 Sb4 Eu6 72.332(13) . 3 ? Eu1 Sb4 Eu6 77.310(8) 7_556 3 ? Eu1 Sb4 Eu6 140.042(18) 7_546 3 ? Cd2 Sb4 Eu6 135.510(6) . 3_545 ? Cd3 Sb4 Eu6 72.332(13) . 3_545 ? Eu1 Sb4 Eu6 140.042(18) 7_556 3_545 ? Eu1 Sb4 Eu6 77.310(8) 7_546 3_545 ? Eu6 Sb4 Eu6 88.977(13) 3 3_545 ? Cd2 Sb4 Eu3 75.925(15) . 7_545 ? Cd3 Sb4 Eu3 136.617(8) . 7_545 ? Eu1 Sb4 Eu3 142.754(19) 7_556 7_545 ? Eu1 Sb4 Eu3 80.441(9) 7_546 7_545 ? Eu6 Sb4 Eu3 131.053(17) 3 7_545 ? Eu6 Sb4 Eu3 72.458(8) 3_545 7_545 ? Cd2 Sb4 Eu3 75.925(15) . 7 ? Cd3 Sb4 Eu3 136.617(8) . 7 ? Eu1 Sb4 Eu3 80.441(9) 7_556 7 ? Eu1 Sb4 Eu3 142.754(19) 7_546 7 ? Eu6 Sb4 Eu3 72.458(8) 3 7 ? Eu6 Sb4 Eu3 131.053(17) 3_545 7 ? Eu3 Sb4 Eu3 86.259(15) 7_545 7 ? As5 Sb5 Sb5 0.00(2) 5_656 5_656 ? As5 Sb5 Cd2 107.77(3) 5_656 . ? Sb5 Sb5 Cd2 107.77(3) 5_656 . ? As5 Sb5 Cd3 112.52(3) 5_656 5_656 ? Sb5 Sb5 Cd3 112.52(3) 5_656 5_656 ? Cd2 Sb5 Cd3 139.71(2) . 5_656 ? As5 Sb5 Eu2 133.622(9) 5_656 7_546 ? Sb5 Sb5 Eu2 133.622(9) 5_656 7_546 ? Cd2 Sb5 Eu2 76.630(15) . 7_546 ? Cd3 Sb5 Eu2 75.865(14) 5_656 7_546 ? As5 Sb5 Eu2 133.622(9) 5_656 7_556 ? Sb5 Sb5 Eu2 133.622(9) 5_656 7_556 ? Cd2 Sb5 Eu2 76.630(15) . 7_556 ? Cd3 Sb5 Eu2 75.865(14) 5_656 7_556 ? Eu2 Sb5 Eu2 92.702(17) 7_546 7_556 ? As5 Sb5 Eu1 68.335(16) 5_656 3 ? Sb5 Sb5 Eu1 68.335(16) 5_656 3 ? Cd2 Sb5 Eu1 134.475(9) . 3 ? Cd3 Sb5 Eu1 64.605(13) 5_656 3 ? Eu2 Sb5 Eu1 140.42(2) 7_546 3 ? Eu2 Sb5 Eu1 76.436(10) 7_556 3 ? As5 Sb5 Eu1 68.335(16) 5_656 3_545 ? Sb5 Sb5 Eu1 68.335(16) 5_656 3_545 ? Cd2 Sb5 Eu1 134.475(9) . 3_545 ? Cd3 Sb5 Eu1 64.605(13) 5_656 3_545 ? Eu2 Sb5 Eu1 76.436(10) 7_546 3_545 ? Eu2 Sb5 Eu1 140.42(2) 7_556 3_545 ? Eu1 Sb5 Eu1 88.000(16) 3 3_545 ? As5 Sb5 Eu1 64.216(16) 5_656 7_546 ? Sb5 Sb5 Eu1 64.216(16) 5_656 7_546 ? Cd2 Sb5 Eu1 64.095(13) . 7_546 ? Cd3 Sb5 Eu1 135.986(9) 5_656 7_546 ? Eu2 Sb5 Eu1 78.468(10) 7_546 7_546 ? Eu2 Sb5 Eu1 140.722(19) 7_556 7_546 ? Eu1 Sb5 Eu1 132.551(17) 3 7_546 ? Eu1 Sb5 Eu1 75.000(12) 3_545 7_546 ? As5 Sb5 Eu1 64.216(16) 5_656 7_556 ? Sb5 Sb5 Eu1 64.216(16) 5_656 7_556 ? Cd2 Sb5 Eu1 64.095(13) . 7_556 ? Cd3 Sb5 Eu1 135.986(9) 5_656 7_556 ? Eu2 Sb5 Eu1 140.722(19) 7_546 7_556 ? Eu2 Sb5 Eu1 78.468(10) 7_556 7_556 ? Eu1 Sb5 Eu1 75.000(12) 3 7_556 ? Eu1 Sb5 Eu1 132.551(17) 3_545 7_556 ? Eu1 Sb5 Eu1 84.605(15) 7_546 7_556 ? Cd1 Sb6 Eu5 65.007(13) 5_656 3 ? Cd1 Sb6 Eu5 65.007(13) 5_656 3_545 ? Eu5 Sb6 Eu5 87.168(15) 3 3_545 ? Cd1 Sb6 Eu3 132.880(10) 5_656 3_545 ? Eu5 Sb6 Eu3 155.442(19) 3 3_545 ? Eu5 Sb6 Eu3 87.700(8) 3_545 3_545 ? Cd1 Sb6 Eu3 132.880(10) 5_656 3 ? Eu5 Sb6 Eu3 87.700(8) 3 3 ? Eu5 Sb6 Eu3 155.442(19) 3_545 3 ? Eu3 Sb6 Eu3 87.063(15) 3_545 3 ? Cd1 Sb6 Eu5 117.93(2) 5_656 5_655 ? Eu5 Sb6 Eu5 71.222(12) 3 5_655 ? Eu5 Sb6 Eu5 71.222(12) 3_545 5_655 ? Eu3 Sb6 Eu5 84.392(13) 3_545 5_655 ? Eu3 Sb6 Eu5 84.392(13) 3 5_655 ? Cd1 Sb6 Eu4 67.023(14) 5_656 3 ? Eu5 Sb6 Eu4 75.276(10) 3 3 ? Eu5 Sb6 Eu4 131.947(17) 3_545 3 ? Eu3 Sb6 Eu4 124.630(17) 3_545 3 ? Eu3 Sb6 Eu4 69.302(10) 3 3 ? Eu5 Sb6 Eu4 137.865(7) 5_655 3 ? Cd1 Sb6 Eu4 67.023(14) 5_656 3_545 ? Eu5 Sb6 Eu4 131.947(17) 3 3_545 ? Eu5 Sb6 Eu4 75.276(10) 3_545 3_545 ? Eu3 Sb6 Eu4 69.302(10) 3_545 3_545 ? Eu3 Sb6 Eu4 124.630(17) 3 3_545 ? Eu5 Sb6 Eu4 137.865(7) 5_655 3_545 ? Eu4 Sb6 Eu4 83.998(14) 3 3_545 ? Sb6 Cd1 Sb3 121.943(14) 5_656 7_546 ? Sb6 Cd1 Sb3 121.943(14) 5_656 7_556 ? Sb3 Cd1 Sb3 110.07(2) 7_546 7_556 ? Sb6 Cd1 Sb2 98.98(2) 5_656 . ? Sb3 Cd1 Sb2 97.753(18) 7_546 . ? Sb3 Cd1 Sb2 97.753(18) 7_556 . ? Sb6 Cd1 Eu2 159.00(2) 5_656 . ? Sb3 Cd1 Eu2 65.481(14) 7_546 . ? Sb3 Cd1 Eu2 65.481(14) 7_556 . ? Sb2 Cd1 Eu2 60.014(18) . . ? Sb6 Cd1 Eu5 65.439(13) 5_656 7_556 ? Sb3 Cd1 Eu5 156.48(2) 7_546 7_556 ? Sb3 Cd1 Eu5 77.467(11) 7_556 7_556 ? Sb2 Cd1 Eu5 58.782(13) . 7_556 ? Eu2 Cd1 Eu5 100.162(15) . 7_556 ? Sb6 Cd1 Eu5 65.439(13) 5_656 7_546 ? Sb3 Cd1 Eu5 77.467(11) 7_546 7_546 ? Sb3 Cd1 Eu5 156.48(2) 7_556 7_546 ? Sb2 Cd1 Eu5 58.782(13) . 7_546 ? Eu2 Cd1 Eu5 100.161(15) . 7_546 ? Eu5 Cd1 Eu5 87.549(17) 7_556 7_546 ? Sb6 Cd1 Eu4 65.390(13) 5_656 7_556 ? Sb3 Cd1 Eu4 128.63(2) 7_546 7_556 ? Sb3 Cd1 Eu4 62.698(13) 7_556 7_556 ? Sb2 Cd1 Eu4 132.987(12) . 7_556 ? Eu2 Cd1 Eu4 127.777(13) . 7_556 ? Eu5 Cd1 Eu4 74.840(10) 7_556 7_556 ? Eu5 Cd1 Eu4 130.749(18) 7_546 7_556 ? Sb6 Cd1 Eu4 65.390(13) 5_656 7_546 ? Sb3 Cd1 Eu4 62.698(13) 7_546 7_546 ? Sb3 Cd1 Eu4 128.63(2) 7_556 7_546 ? Sb2 Cd1 Eu4 132.987(12) . 7_546 ? Eu2 Cd1 Eu4 127.777(13) . 7_546 ? Eu5 Cd1 Eu4 130.749(18) 7_556 7_546 ? Eu5 Cd1 Eu4 74.840(10) 7_546 7_546 ? Eu4 Cd1 Eu4 82.716(15) 7_556 7_546 ? Sb6 Cd1 Eu4 134.39(2) 5_656 . ? Sb3 Cd1 Eu4 58.164(13) 7_546 . ? Sb3 Cd1 Eu4 58.164(13) 7_556 . ? Sb2 Cd1 Eu4 126.63(2) . . ? Eu2 Cd1 Eu4 66.611(13) . . ? Eu5 Cd1 Eu4 135.454(9) 7_556 . ? Eu5 Cd1 Eu4 135.454(9) 7_546 . ? Eu4 Cd1 Eu4 81.089(13) 7_556 . ? Eu4 Cd1 Eu4 81.089(13) 7_546 . ? As2 Cd2 Sb2 0.00(4) 7_546 7_546 ? As2 Cd2 As2 116.56(3) 7_546 7_556 ? Sb2 Cd2 As2 116.56(3) 7_546 7_556 ? As2 Cd2 Sb2 116.56(3) 7_546 7_556 ? Sb2 Cd2 Sb2 116.56(3) 7_546 7_556 ? As2 Cd2 Sb2 0.00(2) 7_556 7_556 ? As2 Cd2 Sb4 108.920(19) 7_546 . ? Sb2 Cd2 Sb4 108.920(19) 7_546 . ? As2 Cd2 Sb4 108.921(19) 7_556 . ? Sb2 Cd2 Sb4 108.921(19) 7_556 . ? As2 Cd2 Sb5 107.538(19) 7_546 . ? Sb2 Cd2 Sb5 107.538(19) 7_546 . ? As2 Cd2 Sb5 107.538(19) 7_556 . ? Sb2 Cd2 Sb5 107.538(19) 7_556 . ? Sb4 Cd2 Sb5 106.96(2) . . ? As2 Cd2 Eu1 164.56(2) 7_546 7_556 ? Sb2 Cd2 Eu1 164.56(2) 7_546 7_556 ? As2 Cd2 Eu1 78.880(13) 7_556 7_556 ? Sb2 Cd2 Eu1 78.880(13) 7_556 7_556 ? Sb4 Cd2 Eu1 62.936(13) . 7_556 ? Sb5 Cd2 Eu1 65.337(13) . 7_556 ? As2 Cd2 Eu1 78.880(13) 7_546 7_546 ? Sb2 Cd2 Eu1 78.880(13) 7_546 7_546 ? As2 Cd2 Eu1 164.56(2) 7_556 7_546 ? Sb2 Cd2 Eu1 164.56(2) 7_556 7_546 ? Sb4 Cd2 Eu1 62.936(13) . 7_546 ? Sb5 Cd2 Eu1 65.337(13) . 7_546 ? Eu1 Cd2 Eu1 85.683(16) 7_556 7_546 ? As2 Cd2 Eu5 58.465(15) 7_546 . ? Sb2 Cd2 Eu5 58.465(15) 7_546 . ? As2 Cd2 Eu5 58.465(15) 7_556 . ? Sb2 Cd2 Eu5 58.465(15) 7_556 . ? Sb4 Cd2 Eu5 122.18(2) . . ? Sb5 Cd2 Eu5 130.86(2) . . ? Eu1 Cd2 Eu5 136.801(8) 7_556 . ? Eu1 Cd2 Eu5 136.801(8) 7_546 . ? As2 Cd2 Eu2 117.08(2) 7_546 7_556 ? Sb2 Cd2 Eu2 117.08(2) 7_546 7_556 ? As2 Cd2 Eu2 54.503(16) 7_556 7_556 ? Sb2 Cd2 Eu2 54.503(16) 7_556 7_556 ? Sb4 Cd2 Eu2 133.706(13) . 7_556 ? Sb5 Cd2 Eu2 54.950(12) . 7_556 ? Eu1 Cd2 Eu2 71.113(10) 7_556 7_556 ? Eu1 Cd2 Eu2 120.286(17) 7_546 7_556 ? Eu5 Cd2 Eu2 87.814(14) . 7_556 ? As1 Cd3 Sb1 0.00(3) 3 3 ? As1 Cd3 As1 118.46(3) 3 3_545 ? Sb1 Cd3 As1 118.46(3) 3 3_545 ? As1 Cd3 Sb1 118.46(3) 3 3_545 ? Sb1 Cd3 Sb1 118.46(3) 3 3_545 ? As1 Cd3 Sb1 0.00(3) 3_545 3_545 ? As1 Cd3 Sb4 114.065(16) 3 . ? Sb1 Cd3 Sb4 114.065(16) 3 . ? As1 Cd3 Sb4 114.065(17) 3_545 . ? Sb1 Cd3 Sb4 114.065(17) 3_545 . ? As1 Cd3 As5 104.404(18) 3 5_656 ? Sb1 Cd3 As5 104.404(18) 3 5_656 ? As1 Cd3 As5 104.404(18) 3_545 5_656 ? Sb1 Cd3 As5 104.404(18) 3_545 5_656 ? Sb4 Cd3 As5 98.06(2) . 5_656 ? As1 Cd3 Sb5 104.404(18) 3 5_656 ? Sb1 Cd3 Sb5 104.404(18) 3 5_656 ? As1 Cd3 Sb5 104.404(18) 3_545 5_656 ? Sb1 Cd3 Sb5 104.404(18) 3_545 5_656 ? Sb4 Cd3 Sb5 98.06(2) . 5_656 ? As5 Cd3 Sb5 0.000(19) 5_656 5_656 ? As1 Cd3 Eu1 160.89(2) 3 7_546 ? Sb1 Cd3 Eu1 160.89(2) 3 7_546 ? As1 Cd3 Eu1 78.373(12) 3_545 7_546 ? Sb1 Cd3 Eu1 78.373(12) 3_545 7_546 ? Sb4 Cd3 Eu1 61.352(13) . 7_546 ? As5 Cd3 Eu1 60.177(13) 5_656 7_546 ? Sb5 Cd3 Eu1 60.177(13) 5_656 7_546 ? As1 Cd3 Eu1 78.373(12) 3 7_556 ? Sb1 Cd3 Eu1 78.373(12) 3 7_556 ? As1 Cd3 Eu1 160.89(2) 3_545 7_556 ? Sb1 Cd3 Eu1 160.89(2) 3_545 7_556 ? Sb4 Cd3 Eu1 61.352(13) . 7_556 ? As5 Cd3 Eu1 60.177(13) 5_656 7_556 ? Sb5 Cd3 Eu1 60.177(13) 5_656 7_556 ? Eu1 Cd3 Eu1 83.692(16) 7_546 7_556 ? As1 Cd3 Eu6 124.94(2) 3 3_545 ? Sb1 Cd3 Eu6 124.94(2) 3 3_545 ? As1 Cd3 Eu6 59.442(13) 3_545 3_545 ? Sb1 Cd3 Eu6 59.442(13) 3_545 3_545 ? Sb4 Cd3 Eu6 58.804(11) . 3_545 ? As5 Cd3 Eu6 130.278(13) 5_656 3_545 ? Sb5 Cd3 Eu6 130.278(13) 5_656 3_545 ? Eu1 Cd3 Eu6 70.272(9) 7_546 3_545 ? Eu1 Cd3 Eu6 120.122(17) 7_556 3_545 ? As1 Cd3 Eu6 59.442(13) 3 3 ? Sb1 Cd3 Eu6 59.442(13) 3 3 ? As1 Cd3 Eu6 124.94(2) 3_545 3 ? Sb1 Cd3 Eu6 124.94(2) 3_545 3 ? Sb4 Cd3 Eu6 58.804(11) . 3 ? As5 Cd3 Eu6 130.278(13) 5_656 3 ? Sb5 Cd3 Eu6 130.278(13) 5_656 3 ? Eu1 Cd3 Eu6 120.122(17) 7_546 3 ? Eu1 Cd3 Eu6 70.272(9) 7_556 3 ? Eu6 Cd3 Eu6 77.969(11) 3_545 3 ? _diffrn_measured_fraction_theta_max 0.997 _diffrn_reflns_theta_full 29.13 _diffrn_measured_fraction_theta_full 0.997 _refine_diff_density_max 1.467 _refine_diff_density_min -1.332 _refine_diff_density_rms 0.314