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A ^(15)N NMR study of some azoles

Stefaniak, L. and Roberts, John D. and Witanowski, M. and Webb, G. A. (1984) A ^(15)N NMR study of some azoles. Organic Magnetic Resonance, 22 (4). pp. 215-220. ISSN 0030-4921. doi:10.1002/mrc.1270220404.

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^(15)N NMR data are reported for 42 azoles, taken mostly at a standard concentration and in a common solvent (0.5 M dimethyl sulfoxide with a 0.01 M increment of Cr(acac)_3 for each nitrogen atom present). Signal assignments were assisted by comparison with ^(14)N line widths, the use of ^2J(^(15)N^1H) couplings, and shielding calculations obtained by the INDO/S–SOS approach. The generally large differences in nitrogen-shielding changes permitted rather facile shift assignments.

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Additional Information:© 1984 Wiley Heyden Ltd. Received 21 April 1983; accepted 15 August 1983. Article first published online: 14 Apr 2005. The part of this research carried out at the California Institute of Technology was supported by the National Science Foundation, and by the Public Health Service, Research Grant No. GM 11072 from the Division of General Medical Sciences. The authors gratefully acknowledge the assistance of Ms B. T. Hamdi in performing the INDO/S-SOS shielding calculations. Financial assistance under project number MR.I. 9 from the Polish Academy of Sciences is gratefully recognized.
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Public Health ServiceGM 11072
Polish Academy of SciencesMR.I. 9
Issue or Number:4
Record Number:CaltechAUTHORS:20151002-123938046
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Official Citation:Stefaniak, L., Roberts, J. D., Witanowski, M. and Webb, G. A. (1984), A 15N NMR study of some azoles. Org. Magn. Reson., 22: 215–220. doi: 10.1002/mrc.1270220404
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:60720
Deposited By: Ruth Sustaita
Deposited On:02 Oct 2015 21:58
Last Modified:10 Nov 2021 22:38

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