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Nitrogen-15 Nuclear Magnetic Resonance Spectroscopy of Some Nucleosides and Nucleotides

Markowski, Volker and Sullivan, Glenn R. and Roberts, John D. (1977) Nitrogen-15 Nuclear Magnetic Resonance Spectroscopy of Some Nucleosides and Nucleotides. Journal of the American Chemical Society, 99 (3). pp. 714-718. ISSN 0002-7863. http://resolver.caltech.edu/CaltechAUTHORS:20151008-115812049

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Abstract

High-resolution nitrogen-15 NMR spectra of six nucleosides and six nucleotides have been obtained at the natural abundance level by high-resolution NMR spectroscopy. All of the nitrogen resonances have been assigned on the basis of comparison of their chemical shifts and nitrogen-hydrogen coupling constants with those of related compounds. Studies of the effect of protonation on the nitrogen chemical shifts of four of these compounds enabled the site of protonation to be detected directly.


Item Type:Article
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URLURL TypeDescription
http://dx.doi.org/10.1021/ja00445a009DOIArticle
http://pubs.acs.org/doi/abs/10.1021/ja00445a009PublisherArticle
Additional Information:© 1977 American Chemical Society. Received February 25, 1976. We are greatly indebted to Professor Nelson J. Leonard of the University of Illinois for labeled adenine samples and for valuable suggestions and encouragement. Supported by the Public Health Service, Research Grant No. GM 11072, from the Division of General Medicine Sciences, and by the National Science Foundation; (b) Deutscher Akademischer Austauschdienst Postdoctoral Fellow, 1974-75.
Funders:
Funding AgencyGrant Number
U.S. Public Health Service (USPHS)GM-11072
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Deutscher Akademischer Austauschdienst (DAAD)UNSPECIFIED
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Caltech Gates and Crellin Laboratories of Chemistry5260
Record Number:CaltechAUTHORS:20151008-115812049
Persistent URL:http://resolver.caltech.edu/CaltechAUTHORS:20151008-115812049
Official Citation:Nitrogen-15 nuclear magnetic resonance spectroscopy of some nucleosides and nucleotides Volker Markowski, Glenn R. Sullivan, and John D. Roberts Journal of the American Chemical Society 1977 99 (3), 714-718 DOI: 10.1021/ja00445a009
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:60914
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:10 Oct 2015 12:18
Last Modified:10 Oct 2015 12:18

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