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Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes

Hawkes, Geoffrey E. and Herwig, Klaus and Roberts, John D. (1974) Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes. Journal of Organic Chemistry, 39 (8). pp. 1017-1028. ISSN 0022-3263. https://resolver.caltech.edu/CaltechAUTHORS:20151008-153201653

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Abstract

The use of ^(13)C nmr (cmr) spectra for the determination of configurations of oximes is described. The problems of quantitative analysis of syn-anti mixtures of oximes by cmr, because of differential T_1 and Overhauser effects, are considered. Chemical shifts for the cmr resonances of a number of aldehydes and ketones are reported.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1021/jo00922a001DOIArticle
http://pubs.acs.org/doi/abs/10.1021/jo00922a001PublisherArticle
Additional Information:© 1974 American Chemical Society. Received August 28, 1973. Supported by the Public Health Service, Research Grant No. GM-11072 from the Division of General Medical Sciences, and by the National Science Foundation.
Funders:
Funding AgencyGrant Number
U.S. Public Health Service (USPHS)GM-11072
NSFUNSPECIFIED
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Caltech Gates and Crellin Laboratories of Chemistry4750
Issue or Number:8
Record Number:CaltechAUTHORS:20151008-153201653
Persistent URL:https://resolver.caltech.edu/CaltechAUTHORS:20151008-153201653
Official Citation:Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes Geoffrey E. Hawkes, Klaus Herwig, and John D. Roberts The Journal of Organic Chemistry 1974 39 (8), 1017-1028 DOI: 10.1021/jo00922a001
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:60932
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:10 Oct 2015 02:07
Last Modified:03 Oct 2019 09:02

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