Hawkes, Geoffrey E. and Herwig, Klaus and Roberts, John D. (1974) Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes. Journal of Organic Chemistry, 39 (8). pp. 1017-1028. ISSN 0022-3263. doi:10.1021/jo00922a001. https://resolver.caltech.edu/CaltechAUTHORS:20151008-153201653
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Abstract
The use of ^(13)C nmr (cmr) spectra for the determination of configurations of oximes is described. The problems of quantitative analysis of syn-anti mixtures of oximes by cmr, because of differential T_1 and Overhauser effects, are considered. Chemical shifts for the cmr resonances of a number of aldehydes and ketones are reported.
Item Type: | Article | |||||||||
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Additional Information: | © 1974 American Chemical Society. Received August 28, 1973. Supported by the Public Health Service, Research Grant No. GM-11072 from the Division of General Medical Sciences, and by the National Science Foundation. | |||||||||
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Issue or Number: | 8 | |||||||||
DOI: | 10.1021/jo00922a001 | |||||||||
Record Number: | CaltechAUTHORS:20151008-153201653 | |||||||||
Persistent URL: | https://resolver.caltech.edu/CaltechAUTHORS:20151008-153201653 | |||||||||
Official Citation: | Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes Geoffrey E. Hawkes, Klaus Herwig, and John D. Roberts The Journal of Organic Chemistry 1974 39 (8), 1017-1028 DOI: 10.1021/jo00922a001 | |||||||||
Usage Policy: | No commercial reproduction, distribution, display or performance rights in this work are provided. | |||||||||
ID Code: | 60932 | |||||||||
Collection: | CaltechAUTHORS | |||||||||
Deposited By: | Ruth Sustaita | |||||||||
Deposited On: | 10 Oct 2015 02:07 | |||||||||
Last Modified: | 10 Nov 2021 22:41 |
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