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Nuclear Magnetic Resonance Spectroscopy. Application of Pulse and Fourier Transform Carbon-13 Nuclear Magnetic Resonance Techniques to Structure Elucidation. Rauwolfia Alkaloids

Levin, Ronald H. and Lallemand, J. Y. and Roberts, John D. (1973) Nuclear Magnetic Resonance Spectroscopy. Application of Pulse and Fourier Transform Carbon-13 Nuclear Magnetic Resonance Techniques to Structure Elucidation. Rauwolfia Alkaloids. Journal of Organic Chemistry, 38 (11). pp. 1983-1986. ISSN 0022-3263. doi:10.1021/jo00951a004. https://resolver.caltech.edu/CaltechAUTHORS:20151009-133523120

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Abstract

The natural-abundance pulse and Fourier transform ^(13)C nmr spectra of several Rauwolfia alkaloids have been recorded. Using noise-decoupling, partial single-frequency off-resonance deooupling (SFOR), and lanthanide chelate induced chemical-shift changes (lanthanide shifts), a self-consistent series of assignments have been made for the observed resonances.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1021/jo00951a004DOIArticle
http://pubs.acs.org/doi/abs/10.1021/jo00951a004PublisherArticle
Additional Information:© 1973 American Chemical Society. Received October 24, 1972. Supported by the Public Health Service, Research Grant No. GM-11072 from the Division of General Medical Sciences, and by the National Science Foundation. National Institutes of Health Postdoctoral Fellow, 1971-1972. NATO Postdoctoral Fellow, 1970-1971.
Funders:
Funding AgencyGrant Number
U.S. Public Health Service (USPHS)GM-11072
NSFUNSPECIFIED
NIH Postdoctoral FellowshipUNSPECIFIED
NATO Postdoctoral FellowshipUNSPECIFIED
Other Numbering System:
Other Numbering System NameOther Numbering System ID
Caltech Gates and Crellin Laboratories of Chemistry4503
Issue or Number:11
DOI:10.1021/jo00951a004
Record Number:CaltechAUTHORS:20151009-133523120
Persistent URL:https://resolver.caltech.edu/CaltechAUTHORS:20151009-133523120
Official Citation:Nuclear magnetic resonance spectroscopy. Application of pulse and Fourier transform carbon-13 nuclear magnetic resonance techniques to structure elucidation. Rauwolfia alkaloids Ronald H. Levin, J. Y. Lallemand, and John D. Roberts The Journal of Organic Chemistry 1973 38 (11), 1983-1986 DOI: 10.1021/jo00951a004
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:60944
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:16 Oct 2015 01:20
Last Modified:10 Nov 2021 22:42

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