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Nuclear Magnetic Resonance Spectroscopy. ^(13)C Spectra of Indole and Methylindoles

Parker, Richard Ghrist and Roberts, John D. (1970) Nuclear Magnetic Resonance Spectroscopy. ^(13)C Spectra of Indole and Methylindoles. Journal of Organic Chemistry, 35 (4). pp. 996-999. ISSN 0022-3263. https://resolver.caltech.edu/CaltechAUTHORS:20151013-111510823

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Abstract

The natural-abundance ^(13)C nmr spectra of indole, the seven monomethylindoles, and some di- and trimethylindoles have been determined at 15.1 MHz. The chemical shifts of the ring carbons in these compounds were found to range over 50 ppm, and with the aid of complete proton decoupling it was possible to resolve all of the carbon resonances. Single-frequency and off-resonance proton-decoupling techniques were employed to assign the resonances to specific carbons.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1021/jo00829a029DOIArticle
http://pubs.acs.org/doi/abs/10.1021/jo00829a029PublisherArticle
Additional Information:© 1970 American Chemical Society. Received September 8, 1969. Supported by the National Science Foundation and the Public Health Service, Research Grant GM-11072-07 from the Division of General Medical Sciences.
Funders:
Funding AgencyGrant Number
NSFUNSPECIFIED
U.S. Public Health Service (USPHS)GM-11072-07
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Caltech Gates and Crellin Laboratories of Chemistry3939
Issue or Number:4
Record Number:CaltechAUTHORS:20151013-111510823
Persistent URL:https://resolver.caltech.edu/CaltechAUTHORS:20151013-111510823
Official Citation:Nuclear magnetic resonance spectroscopy. 13C spectra of indole and methylindoles Richard Ghrist Parker and John D. Roberts The Journal of Organic Chemistry 1970 35 (4), 996-999 DOI: 10.1021/jo00829a029
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:61046
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:14 Oct 2015 23:36
Last Modified:03 Oct 2019 09:03

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