Zieger, Herman E. and Roberts, John D. (1969) Nuclear Magnetic Resonance Spectroscopy. Low-Temperature Studies of Diallylmagnesium. Journal of Organic Chemistry, 34 (6). pp. 1976-1977. ISSN 0022-3263. https://resolver.caltech.edu/CaltechAUTHORS:20151013-145413050
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Abstract
Allylic organoalkali metal compounds have been observed to exhibit reversible changes in nmr spectra (e.g., AA'BB'C → AB_4 for allyllithium) over the temperature range from -100 to + 110º. In contrast, allymagnesium bromide is reported to display a simple AB_4 spectrum at -80º and diallylmagnesiurn to behave similarly from -60 to +37º in tetrahydrofuran.
| Item Type: | Article | |||||||||
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| Additional Information: | © 1969 American Chemical Society. Received July 9, 1968. Supported in part by the National Science Foundation. | |||||||||
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| Issue or Number: | 6 | |||||||||
| Record Number: | CaltechAUTHORS:20151013-145413050 | |||||||||
| Persistent URL: | https://resolver.caltech.edu/CaltechAUTHORS:20151013-145413050 | |||||||||
| Official Citation: | Nuclear magnetic resonance spectroscopy. Low temperature studies of diallylmagnesium Herman E. Zieger and John D. Roberts The Journal of Organic Chemistry 1969 34 (6), 1976-1977 DOI: 10.1021/jo01258a104 | |||||||||
| Usage Policy: | No commercial reproduction, distribution, display or performance rights in this work are provided. | |||||||||
| ID Code: | 61075 | |||||||||
| Collection: | CaltechAUTHORS | |||||||||
| Deposited By: | Ruth Sustaita | |||||||||
| Deposited On: | 14 Oct 2015 19:26 | |||||||||
| Last Modified: | 03 Oct 2019 09:04 |
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