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The Synthesis of Asymmetrically Labeled 5-Norbornene-2,3-endo-dicarboxylic Anhydride

Scheidegger, Ulrich and Baldwin, John E. and Roberts, John D. (1967) The Synthesis of Asymmetrically Labeled 5-Norbornene-2,3-endo-dicarboxylic Anhydride. Journal of the American Chemical Society, 89 (4). pp. 894-898. ISSN 0002-7863. http://resolver.caltech.edu/CaltechAUTHORS:20151014-144941782

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Abstract

Procedures are described for a synthesis of 5-norbornene-2,3-endo-dicarboxylica nhydride stereospecifically labeled with ^(14)C in one carbonyl group and for the degradation of the anhydride to determine which carbonyl group was labeled. The particular method of synthesis was found to give the labeled anhydride with ^(14)C in that carbonyl group which corresponds in position to the carboxyl group of the levorotatory 2-endo-norbornanecarboxylic acid.


Item Type:Article
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http://dx.doi.org/10.1021/ja00980a027DOIArticle
http://pubs.acs.org/doi/abs/10.1021/ja00980a027PublisherArticle
Additional Information:© 1967 American Chemical Society. Received May 23, 1966. Supported by the National Science Foundation.
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Caltech Gates and Crellin Laboratories of Chemistry3370
Record Number:CaltechAUTHORS:20151014-144941782
Persistent URL:http://resolver.caltech.edu/CaltechAUTHORS:20151014-144941782
Official Citation:The Synthesis of Asymmetrically Labeled 5-Norbornene-2,3-endo-dicarboxylic Anhydride Ulrich Scheidegger, John E. Baldwin, and John D. Roberts Journal of the American Chemical Society 1967 89 (4), 894-898 DOI: 10.1021/ja00980a027
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:61116
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:15 Oct 2015 17:26
Last Modified:15 Oct 2015 17:26

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