Takahashi, Masaaki and Davis, Donald R. and Roberts, John D. (1962) Nuclear Magnetic Resonance Spectroscopy. Long-Range H-F Spin-Spin Coupling in 1,1-Difluoro-2,2-dichloro-3-phenyl-3-methylcyclobutane. Journal of the American Chemical Society, 84 (15). pp. 2935-2938. ISSN 0002-7863. doi:10.1021/ja00874a018. https://resolver.caltech.edu/CaltechAUTHORS:20151020-073602006
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Abstract
A 2 C.P.S. long-range H-F spin-spin coupling has been observed over fire saturated bonds in 1,1-difluoro-2,2-dichloro-3-phenyl-3-metliylcyclobutane, involving one of the fluorines at the 1-position and the protons of the 3-methyl group. Comparison of the spectrum with that of stereospecifically labeled 4-deuterio derivatives suggests that the fluorine involved in the long-range coupling is the one cis to the methyl group.
| Item Type: | Article | |||||||||
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| Additional Information: | © 1962 American Chemical Society. Received March 7, 1962. Supported in part by the Kureha Chemical Ind. Co. (Japan) and the Office of Naval Research. | |||||||||
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| Issue or Number: | 15 | |||||||||
| DOI: | 10.1021/ja00874a018 | |||||||||
| Record Number: | CaltechAUTHORS:20151020-073602006 | |||||||||
| Persistent URL: | https://resolver.caltech.edu/CaltechAUTHORS:20151020-073602006 | |||||||||
| Official Citation: | Nuclear Magnetic Resonance Spectroscopy. Long-Range H-F Spin-Spin Coupling in 1,1-Difluoro-2,2-dichloro-3-phenyl-3-methylcyclobutane Masaaki Takahashi, Donald R. Davis, and John D. Roberts Journal of the American Chemical Society 1962 84 (15), 2935-2938 DOI: 10.1021/ja00874a018 | |||||||||
| Usage Policy: | No commercial reproduction, distribution, display or performance rights in this work are provided. | |||||||||
| ID Code: | 61298 | |||||||||
| Collection: | CaltechAUTHORS | |||||||||
| Deposited By: | Ruth Sustaita | |||||||||
| Deposited On: | 20 Oct 2015 18:52 | |||||||||
| Last Modified: | 10 Nov 2021 22:47 |
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