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High Field Solid-State NMR Spectroscopy Investigation of ^(15)N-Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water

Fenniri, Hicham and Tikhomirov, Grigory A. and Brouwer, Darren H. and Bouatra, Souhaila and El Bakkari, Mounir and Yan, Zhimin and Cho, Jae-Young and Yamazaki, Takeshi (2016) High Field Solid-State NMR Spectroscopy Investigation of ^(15)N-Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water. Journal of the American Chemical Society, 138 (19). pp. 6115-6118. ISSN 0002-7863. http://resolver.caltech.edu/CaltechAUTHORS:20160610-130908380

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Abstract

^(15)N-labeled rosette nanotubes were synthesized and investigated using high-field solid-state NMR spectroscopy, X-ray diffraction, atomic force microscopy, and electron microscopy. The results established the H-bond network involved in the self-assembly of the nanostructure as well as bound water molecules in the nanotube’s channel.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1021/jacs.6b02420DOIArticle
http://pubs.acs.org/doi/abs/10.1021/jacs.6b02420PublisherArticle
http://pubs.acs.org/doi/suppl/10.1021/jacs.6b02420Related ItemSupporting Information
Additional Information:© 2016 American Chemical Society. Received: March 6, 2016. Publication Date (Web): May 04, 2016. Access to the 900 MHz NMR spectrometer was provided by the National Ultrahigh Field NMR Facility for Solids, a national research facility funded by the Canada Foundation for Innovation, the Natural Sciences and Engineering Research Council of Canada (NSERC), the Ontario Innovation Trust, Recherche Québec, the National Research Council Canada (NRC), and Bruker BioSpin and managed by the University of Ottawa. We thank NSERC, NRC, the University of Alberta, and Northeastern University for financial support. The authors declare no competing financial interest.
Funders:
Funding AgencyGrant Number
Canada Foundation for InnovationUNSPECIFIED
Natural Sciences and Engineering Research Council of Canada (NSERC)UNSPECIFIED
Ontario Innovation TrustUNSPECIFIED
Recherche QuébecUNSPECIFIED
National Research Council of CanadaUNSPECIFIED
Bruker BioSpinUNSPECIFIED
University of AlbertaUNSPECIFIED
Northeastern UniversityUNSPECIFIED
Record Number:CaltechAUTHORS:20160610-130908380
Persistent URL:http://resolver.caltech.edu/CaltechAUTHORS:20160610-130908380
Official Citation:High Field Solid-State NMR Spectroscopy Investigation of 15N-Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water Hicham Fenniri, Grigory A. Tikhomirov, Darren H. Brouwer, Souhaila Bouatra, Mounir El Bakkari, Zhimin Yan, Jae-Young Cho, and Takeshi Yamazaki Journal of the American Chemical Society 2016 138 (19), 6115-6118 DOI: 10.1021/jacs.6b02420
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:67843
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:10 Jun 2016 22:19
Last Modified:10 Jun 2016 22:19

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