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High-energy-resolution X-ray monochromator calibration using the detailed-balance principle

Zhao, J. Y. and Sturhahn, W. (2012) High-energy-resolution X-ray monochromator calibration using the detailed-balance principle. Journal of Synchrotron Radiation, 19 (4). pp. 602-608. ISSN 0909-0495. doi:10.1107/S0909049512022339. https://resolver.caltech.edu/CaltechAUTHORS:20160908-123949321

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Abstract

A new method is presented to calibrate an X-ray energy scale with sub-meV relative accuracy by using the detailed-balance principle of the phonon creation and annihilation. This method is conveniently used to define or verify the energy scale of high-energy-resolution monochromators that are used in inelastic X-ray scattering and nuclear resonant inelastic X-ray scattering instruments at synchrotron radiation facilities. This method does not rely on sample properties and its precision only depends on the statistical data quality. Well calibrated instruments are essential for reliable comparison of data sets obtained at different synchrotron radiation beamlines, of data with theoretical predictions, and of data from other techniques such as neutron or light scattering. The principle of the detailed-balance method is described in this paper and demonstrated experimentally.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1107/S0909049512022339DOIArticle
http://scripts.iucr.org/cgi-bin/paper?S0909049512022339PublisherArticle
ORCID:
AuthorORCID
Zhao, J. Y.0000-0002-0777-3626
Sturhahn, W.0000-0002-9606-4740
Additional Information:© 2012 International Union of Crystallography. This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. Received 18 November 2011; Accepted 16 May 2012. We thank Drs E. E. Alp, A. Alatas of APS, T. Sage, Y. Q. Zeng of Northeasten University, H. X. Wang of University of California at Davis, and Y. M. Xiao of HPCAT, APS, for fruitful discussions. This work was supported by the US Department of Energy, Office of Science, Office of Basic Energy Sciences, under Contract No. DE-AC02-06CH11357.
Funders:
Funding AgencyGrant Number
Department of Energy (DOE)DE-AC02-06CH11357
Subject Keywords:X-ray; monochromator; energy calibration; nuclear resonant scattering
Issue or Number:4
DOI:10.1107/S0909049512022339
Record Number:CaltechAUTHORS:20160908-123949321
Persistent URL:https://resolver.caltech.edu/CaltechAUTHORS:20160908-123949321
Official Citation:Zhao, J. Y. & Sturhahn, W. (2012). J. Synchrotron Rad. 19, 602-608.
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:70211
Collection:CaltechAUTHORS
Deposited By: Tony Diaz
Deposited On:09 Sep 2016 00:15
Last Modified:11 Nov 2021 04:26

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