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Die Struktur von DL-μ-hydroxo-di-μ-nitro-bis(triamminkobalt)(3+)-trichlorid-hydrat

Thewalt, Ulf (1970) Die Struktur von DL-μ-hydroxo-di-μ-nitro-bis(triamminkobalt)(3+)-trichlorid-hydrat. Acta crystallographica. Section B, Structural crystallography and crystal chemistry, 26 (1). pp. 81-88. ISSN 0567-7408. https://resolver.caltech.edu/CaltechAUTHORS:20161005-145312732

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Abstract

DL-μ-Hydroxo-di-μ-nitro-bis(triamminecobalt)(3 + )-trichloride hydrate, [(NH_3)_3Co(OH)(N0_2hCo(NH_3)_3]Cl_3. H_20, crystallizes in the monoclinic space group P2_1/c with ɑ = 9·70, b = 6-73, c = 24·57 Å and β = 104·3°; there are four formula units in the cell. The structure was determined by the heavy-atom method and refined by three-dimensional least-squares calculations. The final R index for 1397 observed reflections of non-zero weight is 0·067.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1107/S0567740870001954DOIArticle
http://scripts.iucr.org/cgi-bin/paper?a07341PublisherArticle
Additional Information:© 1970 International Union of Crystallography. Eingegangen am 5. Dezember 1968 und wiedereingereicht am 27. März 1969. This work was supported by Grant GP-5768 from the National Science Foundation.
Funders:
Funding AgencyGrant Number
NSFGP-5768
Other Numbering System:
Other Numbering System NameOther Numbering System ID
Arthur Amos Noyes Laboratory of Chemical Physics3769
Issue or Number:1
Record Number:CaltechAUTHORS:20161005-145312732
Persistent URL:https://resolver.caltech.edu/CaltechAUTHORS:20161005-145312732
Official Citation:Die Struktur von DL-μ-hydroxo-di-μ-nitro-bis­(triamminkobalt)(3+)-trichlorid-hydrat U. Thewalt Acta Cryst. (1970). B26, 81-88 doi: 10.1107/S0567740870001954
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:70885
Collection:CaltechAUTHORS
Deposited By: Ruth Sustaita
Deposited On:05 Oct 2016 22:10
Last Modified:03 Oct 2019 16:02

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