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A preliminary crystallographic investigation of 1-phenylhydantoin and three derivatives of uracil

Gerdil, Raymond (1960) A preliminary crystallographic investigation of 1-phenylhydantoin and three derivatives of uracil. Acta Crystallographica, 13 (2). pp. 165-166. ISSN 0365-110X. http://resolver.caltech.edu/CaltechAUTHORS:20161005-161231415

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Abstract

A preliminary investigation has been made of the crystallographic data of 4-methyl-5-ethyluracil (I), 4-methyluracil-5-acetic acid (II), 4-methyl-5-methylaminouracil (III), and 1-phenyLhydantoin (IV). The lattice constants and space-group data were obtained from rotation and Weissenberg photographs; the determinations were made on the basis of one crystal setting for each species, and the measurements were corrected for film shrinkage. The angular constants of the direct cells were determined by the method of angular lag (Buerger, 1942): from measurements on (1) an equi-inclination photograph of the first layer in monoclinic cases, (2) a composite anti-equi-inclination photograph (of the zero and first layers, respectively) in triclinic cases. The crystal densities were determined by flotation. The errors are estimated to be about ± 0.05 Å for the linear constants and about ± 0 ° 20' for the angular constants.


Item Type:Article
Related URLs:
URLURL TypeDescription
http://dx.doi.org/10.1107/S0365110X60000364DOIArticle
http://scripts.iucr.org/cgi-bin/paper?S0365110X60000364PublisherArticle
Additional Information:© 1960 International Union of Crystallography. (Received 6 October 1959) Contribution No. 2516 from the Gates and Crellin Laboratories of Chemistry. Aided by a grant from The National Foundation.
Funders:
Funding AgencyGrant Number
National FoundationUNSPECIFIED
Other Numbering System:
Other Numbering System NameOther Numbering System ID
Gates and Crellin Laboratories of Chemistry2516
Record Number:CaltechAUTHORS:20161005-161231415
Persistent URL:http://resolver.caltech.edu/CaltechAUTHORS:20161005-161231415
Official Citation:Gerdil, R. (1960). Acta Cryst. 13, 165-166.
Usage Policy:No commercial reproduction, distribution, display or performance rights in this work are provided.
ID Code:70902
Collection:CaltechAUTHORS
Deposited By: George Porter
Deposited On:14 Oct 2016 22:24
Last Modified:13 Feb 2019 18:03

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