Marsh, Richard E. (1994) On the structure of the mixed ligand complex of [VO]^(2+) with hydrotris(3,5-dimethylpyrazolyl)borato and 1,3-diphenyl-1,3-propanedionato ligands. Acta Crystallographica Section C, 50 (10). pp. 1596-1598. ISSN 0108-2701. https://resolver.caltech.edu/CaltechAUTHORS:20170123-155317741
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Abstract
The structure of (1,3-diphenyl-1,3-propanedionato,κ^2O,O')oxo[tris(3,5-dimethyl-1-pyrazolyl-κN^2)hydroborato] vanadium(IV) methyl cyanide, [VO(C_(15)H_(22)-BN_6)(C_(15)H_(11)O_2)].xCH_3CN, has recently been described and refined [Beddoes, Eardley, Mabbs, Moorcroft & Passand (1993). Acta Cryst. C49, 1923-1926] in space group Pna2_1 (orthorhombic; a = 15.960 (1), b = 12.447 (1), c = 17.044 (1) Å, z = 4). It is better described in Pnma (conventional setting of Pnam). Revised coordinates are given and the anomalous bond lengths reported earlier are revised.
Item Type: | Article | |||||||||
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Additional Information: | © 1994 International Union of Crystallography. Received 17 January 1994; accepted 19 April 1994. | |||||||||
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Issue or Number: | 10 | |||||||||
Record Number: | CaltechAUTHORS:20170123-155317741 | |||||||||
Persistent URL: | https://resolver.caltech.edu/CaltechAUTHORS:20170123-155317741 | |||||||||
Usage Policy: | No commercial reproduction, distribution, display or performance rights in this work are provided. | |||||||||
ID Code: | 73638 | |||||||||
Collection: | CaltechAUTHORS | |||||||||
Deposited By: | Tony Diaz | |||||||||
Deposited On: | 26 Jan 2017 20:39 | |||||||||
Last Modified: | 03 Oct 2019 16:29 |
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