Vaudry, Frédéric and Khodabandeh, Shervin and Davis, Mark E. (1996) Synthesis of Pure Alumina Mesoporous Materials. Chemistry of Materials, 8 (7). pp. 1451-1464. ISSN 0897-4756. doi:10.1021/cm9600337. https://resolver.caltech.edu/CaltechAUTHORS:20180319-152747571
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Abstract
Alumina mesophases have been synthesized by reacting aluminum alkoxides and carboxylic acids with controlled amounts of water in low-molecular-weight alcoholic solvents. Calcination of these materials yields aluminas that are thermally stable to 1073 K and contain randomly ordered pores. Specific surface areas as high as 710 m2/g and narrow pore size distributions centered at 20 Å that do not contain “zeolitic” micropores are exhibited by the calcined solids.
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Additional Information: | © 1996 American Chemical Society. Received January 18, 1996. Revised Manuscript Received April 29, 1996. Publication Date (Web): July 11, 1996. The authors thank Mr. Paul Wagner for carrying out variable-temperature XRD measurements and Dr. Larry Beck for helpful discussions concerning the interpretation of the NMR spectra. Akzo America is gratefully acknowledged for financial support. | |||||||||
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Issue or Number: | 7 | |||||||||
DOI: | 10.1021/cm9600337 | |||||||||
Record Number: | CaltechAUTHORS:20180319-152747571 | |||||||||
Persistent URL: | https://resolver.caltech.edu/CaltechAUTHORS:20180319-152747571 | |||||||||
Official Citation: | Synthesis of Pure Alumina Mesoporous Materials. Frédéric Vaudry, Shervin Khodabandeh, and Mark E. Davis. Chemistry of Materials 1996 8 (7), 1451-1464 DOI: 10.1021/cm9600337 | |||||||||
Usage Policy: | No commercial reproduction, distribution, display or performance rights in this work are provided. | |||||||||
ID Code: | 85365 | |||||||||
Collection: | CaltechAUTHORS | |||||||||
Deposited By: | Tony Diaz | |||||||||
Deposited On: | 26 Mar 2018 22:11 | |||||||||
Last Modified: | 15 Nov 2021 20:28 |
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